A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS |
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| Authors: | Amoureux Jean-Paul Flambard Alexandrine Delevoye Laurent Montagne Lionel |
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| Institution: | LCPS, CNRS-8012, Université de Lille-1, Villeneuve d'Ascq, F-59652, France. jean-paul.amoureux@univ-lille1.fr |
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| Abstract: | We show that by combining the intrinsically larger (with respect to MQMAS) efficiency of Double-Quantum Filtered Satellite-Transition MAS (DQF-STMAS), with the large S/N gain of the Soft-Pulse Added Mixing (SPAM) concept, a new very sensitive high-resolution solid-state NMR method can be obtained for semi-integer quadrupolar nuclei. |
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