| 质谱在线连续检测系统的建立及应用实例 |
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| 引用本文： | 郭耘,张兵,李树本,牛建中,高玲. 质谱在线连续检测系统的建立及应用实例[J]. 分析测试技术与仪器, 1999, 5(4): 230-233 |
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| 作者姓名： | 郭耘 张兵 李树本 牛建中 高玲 |
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| 作者单位： | [1]中国科学院兰州化学物理研究所羰基合成与选择氧化国家重点 [2]中国科学院大型仪器功能开发 |
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| 基金项目： | 中国科学院大型仪器功能开发基金 |
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| 摘 要： | 设计和建立了一种质谱在线连续检测系统。该系统响应迅速，操作灵活。可直接与反应系统或与色谱等联机使用，对所有的气相反应和有可挥发组分的液相反应进行在线检测。在ＺｒＯ２－Ａ１２Ｏ３上进行了ＮＨ３吸脱附和ＣＯ脉冲反应的研究，获得了重现性很好的结果。
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| 关 键 词： | 质谱 在线检测 程序升温脱附 多催化反应 |
| 收稿时间： | 1999-10-07 |
| 修稿时间： | 1999-11-02 |
Establishment and Application of a System for On line Detection Based on Mass Spectrometer |
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| GUO Yun,ZHANG Bing,LI Shuben,NIU Jianzhong and GAO Ling. Establishment and Application of a System for On line Detection Based on Mass Spectrometer[J]. Analysis and Testing Technology and Instruments, 1999, 5(4): 230-233 |
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| Authors: | GUO Yun ZHANG Bing LI Shuben NIU Jianzhong GAO Ling |
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| Affiliation: | State Key Laboratory for Oxo Synthesis and Selective Oxidation, the Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000;State Key Laboratory for Oxo Synthesis and Selective Oxidation, the Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000;State Key Laboratory for Oxo Synthesis and Selective Oxidation, the Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000;State Key Laboratory for Oxo Synthesis and Selective Oxidation, the Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000;State Key Laboratory for Oxo Synthesis and Selective Oxidation, the Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000 |
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| Abstract: | The design and establishment of a system for on line detection based on mass spectrometer were described, by which gases and volatile liquid components can be detected continuously. The system can be adjusted conveniently according to different reaction conditions, and connected with GS etc.. The system has been successfully used for the investigation of NH3 TPD and CO pulse reaction over ZrO-2 Al-2O-3. |
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| Keywords: | mass spectrometer on line temperature programmed desorption pulse reaction |
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