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Micro-interferometry for measurement of thermal displacements at fiber/matrix interfaces
Authors:N. R. Sottos  W. R. Scott  R. L. McCullough
Affiliation:(1) 216 Talbot Laboratory, University of Illinois, 104 S. Wright Street, 61801 Urbana, IL;(2) Naval Air Development Center, Code 6063, 18974 Warminster, PA;(3) Department of Chemical Engineering, University of Delaware, 19716 Newark, DE
Abstract:A micro-interferometric technique for measuring out-of-plane thermal displacements on a scale commensurate with the dimensions of the fiber/matrix unit cell is described. A scanning micro-interferometer is used to image surface displacements of samples containing a single-pitch-based carbon fiber embedded in an epoxy matrix. The interferometer design gives the necessary resolution to detect small changes in thermal displacements in the fiber/matrix interface region. The samples were heated electrically through the fiber to create radially symmetric temperature and displacement fields. Repeatable displacement measurements were obtained on a radial line across the interface region with an accuracy of ±25 Å. A sharp expansion of the matrix surrounding the fiber was observed with each heating. Overall, the experiments demonstrate the utility of micro-interferometry for measuring submicron displacements.
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