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Synthesis of 1,3,4-thiadiazines,bis-1,3,4-thiadiazoles, [1,2,4]triazino[3,4-b][1,3,4]thiadiazine,thiazolines from carbonothioic dihydrazide
Authors:Abdelwahed R Sayed
Institution:1. Department of Chemistry, Faculty of Science, University of Beni Suef, Egypt;2. Department of Chemistry, Faculty of Science, KFU, Saudi Arabia
Abstract:A novel and efficient synthesis of 1,3,4-thiadiazines, bis-1,3,4-thiadiazoles, 1,2,4]triazino3,4-b]1,3,4]thiadiazine, and thiazolines is reported from the reaction of α-haloketo hydrazonoyl halides with carbonothioic dihydrazide or its analogues. The structures were elucidated on the basis of their elemental analysis, spectral data and an alternative synthetic route.
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