An efficient synthesis of enol phosphates via organic base-promoted addition of phosphites to 4-oxo-enoates |
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| Authors: | Xiao-Yu Zhu Jia-Rong Chen Liang-Qiu Lu Wen-Jing Xiao |
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| Institution: | Key Laboratory of Pesticide & Chemical Biology, Ministry of Education, College of Chemistry, Central China Normal University, 152 Luoyu Road, Wuhan, Hubei 430079, China |
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| Abstract: | A TMG catalyzed, practical and efficient hydrophosphorylation of 4-oxo-enoates by diethyl or diphenyl phosphite has been described. This protocol allows a convenient access to a variety of enol phosphates under mild conditions in good yield with excellent stereoselectivity. |
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