| Synthesis and Crystal Structure of 1,4-Dimethyl-2,5-di{[2’-(3-pyridylmethylamino-formyl)phenoxyl]methyl}benzene Perchlorate |
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| 作者单位： | State Key Laboratory of Applied Organic Chemistry College of Chemistry and Chemical Engineering Lanzhou University，State Key Laboratory of Applied Organic Chemistry College of Chemistry and Chemical Engineering Lanzhou University，State Key Laboratory of Applied Organic Chemistry College of Chemistry and Chemical Engineering Lanzhou University，State Key Laboratory of Applied Organic Chemistry College of Chemistry and Chemical Engineering Lanzhou University，State Key Laboratory of Applied Organic Chemistry College of Chemistry and Chemical Engineering Lanzhou University，Lanzhou 730000 China，Lanzhou 730000 China，Lanzhou 730000 China，Lanzhou 730000 China，Lanzhou 730000 China |
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| 摘 要： | The title compound, 1,4-dimethyl-2,5-di{[2’-(3-pyridylmethylaminoformyl)phenoxyl]- methyl}benzene perchlorate (C36H36Cl2N4O12, Mr = 787.59), has been synthesized and structurally determined by single-crystal X-ray diffraction. The crystal crystallizes in the orthorhombic system, space group Pbca with a = 14.366(4), b = 15.159(4), c = 16.443(5), V = 3580.9(17)3, Z = 4, Dc = 1.461 g/cm3, μ = 0.253 mm-1, F(000) = 1640, R = 0.0618 and wR = 0.1525 for 1615 observed reflections (I > 2σ(I)). In the structure of the title compound, a two-dimensional supramolecular layer is formed via intermolecular hydrogen bonding interactions.
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| 关 键 词： | 2 5-dimethyl-1 4-di{[2’-(3-pyridylmethylaminoformyl)phenoxyl]methyl}benzene synthesis spectral characterization crystal structure |
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