| Decarboxylative bromination of α,β-unsaturated carboxylic acids via an anodic oxidation |
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| 引用本文： | Mei-Xiang Bi,Peng Qian,Yu-Kang Wang,Zheng-Gen Zha,Zhi-Yong Wang. Decarboxylative bromination of α,β-unsaturated carboxylic acids via an anodic oxidation[J]. 中国化学快报, 2017, 28(6): 1159-1162. DOI: 10.1016/j.cclet.2017.04.030 |
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| 作者姓名： | Mei-Xiang Bi Peng Qian Yu-Kang Wang Zheng-Gen Zha Zhi-Yong Wang |
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| 作者单位： | Hefei National Laboratory for Physical Sciences at Microscale, CAS Key Laboratory of Soft Matter Chemistry and Department of Chemistry & Collaborative Innovation Center of Suzhou Nano Science and Technology, University of Science and Technology of China, Hefei 230026, China |
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| 基金项目： | The authors are grateful to the National Nature Science Foundation of China (Nos. 21472177, 21672200, 21432009, J1310010) and the Strategic Priority Research Program of the Chinese Academy of Sciences (No. XDB20000000). |
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| 摘 要： | A novel bromination of α,β-unsaturated carboxylic acids was developed via a decarboxylation by virtue of a direct anodic electro-oxidation.In this method,ammonium bromide was employed as a bromine source and the reaction features transition-metal-free,short time,and no additional supporting electrolyte.
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| 关 键 词： | Decarboxylative bromination &alpha &beta -Unsaturated carboxylic acids Ammonium bromide Anodic oxidation Electro-oxidation |
Decarboxylative bromination of α,β-unsaturated carboxylic acids via an anodic oxidation |
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| Mei-Xiang Bi,Peng Qian,Yu-Kang Wang,Zheng-Gen Zha,Zhi-Yong Wang. Decarboxylative bromination of α,β-unsaturated carboxylic acids via an anodic oxidation[J]. Chinese Chemical Letters, 2017, 28(6): 1159-1162. DOI: 10.1016/j.cclet.2017.04.030 |
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| Authors: | Mei-Xiang Bi Peng Qian Yu-Kang Wang Zheng-Gen Zha Zhi-Yong Wang |
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| Affiliation: | Hefei National Laboratory for Physical Sciences at Microscale, CAS Key Laboratory of Soft Matter Chemistry and Department of Chemistry & Collaborative Innovation Center of Suzhou Nano Science and Technology, University of Science and Technology of China, Hefei 230026, China |
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| Abstract: | A novel bromination of α,β-unsaturated carboxylic acids was developed via a decarboxylation by virtue of a direct anodic electro-oxidation. In this method, ammonium bromide was employed as a bromine source and the reaction features transition-metal-free, short time, and no additional supporting electrolyte. |
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| Keywords: | Decarboxylative bromination α β-Unsaturated carboxylic acids Ammonium bromide Anodic oxidation Electro-oxidation |
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