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Nickel(II) complexes based on products of condensation of aroyl(perfluoroacyl)methanes with benzoylhydrazine |
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| Authors: | K G Avezov S I Yakimovich B B Umarov V V Pakal’nis G G Aleksandrov T N Niyazkhanov N G Sevinchov N A Parpiev |
| Institution: | 1. Bukhara State University, Bukhara, Uzbekistan 2. St. Petersburg State University, St. Petersburg, Russia 3. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii pr. 31, Moscow, 119991, Russia |
| Abstract: | A series of novel complexes NiL n · NH3 were obtained by reactions of equimolar amounts of the ligands H2L n (prepared by condensation of aroyl(perfluoroacyl)methanes with benzoylhydrazine) as solutions in ethanol and nickel(II) acetate as a solution in aqueous ammonia. The empirical formulas and square planar structures of the complexes obtained were determined using elemental analysis, IR and 1H NMR spectroscopy, and X-ray diffraction. |
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