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排序方式: 共有1084条查询结果,搜索用时 418 毫秒
1.
R. Bairava Ganesh Hitoshi Matsuo Takahiro Kawamura Yoshihiro Kangawa Koji Arafune Yoshio Ohshita Masafumi Yamaguchi Koichi Kakimoto 《Journal of Crystal Growth》2008,310(11):2697-2701
Multicrystalline silicon was grown by unidirectional solidification method using the accelerated crucible rotation technique. The application of the accelerated crucible rotation technique in unidirectional solidification method induced growth striations across the axial direction of the grown crystal. This striation pattern was observed from carbon concentration distribution, obtained by using Fourier transform infrared spectroscopy. The generated striation pattern was found to be weak and discontinuous. Some striations were absent, probably due to back melting, caused during each crucible rotation. From the growth striations and applied time period in crucible rotation, the growth rate was estimated by using Fourier transformation analysis. 相似文献
2.
The growth mechanism of the peritectic η phase involving the peritectic reaction and peritectic transformation in Cu-70%Sn alloy was investigated under directional
solidification. The results show that a major growth mechanism in thickening of the peritectic η-layer is not the peritectic reaction but the peritectic transformation. The transformation temperature and isothermal time
play crucial roles in determining the volume fraction and the thickness of the peritectic η phase. With the increase of the temperature and isothermal time, the volume fraction of the peritectic η phase increases. The regressed data show that the relationship between the thickness of η phase (Δx) and the transformation temperature (T) meets the following equation In Δx=6.5−1673 1 / T. Additionally, there exists a relationship between the thickness of the η phase (Δx) and the isothermal time (t) at the 9 mm solidification distance below the peritectic reaction interface, Δx=0.72t
1/2, which is consistent with the theoretical model.
Supported by the National Science Foundation of China (Grant No. 50395102) 相似文献
3.
The specific heat and related thermophysical properties of liquid Fe77.5Cu13Mo9.5 monotectic alloy were investigated by an electromagnetic levitation drop calorimeter over a wide temperature range from 1482 to 1818 K. A maximum undercooling of 221 K (0.13 Tm) was achieved and the specific heat was determined as 44.71 J·mol-1·K-1. The excess specific heat, enthalpy change, entropy change and Gibbs free energy difference of this alloy were calculated on the basis of experimental results. It was found that the calculated results by traditional estimating methods can only describe the solidification process under low undercooling conditions. Only the experimental results can reflect the reality under high undercooling conditions. Meanwhile, the thermal diffusivity, thermal conductivity, and sound speed were derived from the present experimental results. Furthermore, the solidified microstructural morphology was examined, which consists of (Fe) and (Cu) phases. The calculated interface energy was applied to exploring the correlation between competitive nucleation and solidification microstructure within monotectic alloy. 相似文献
4.
MicrostructureEvolutioninLaserRSCo-baseMetastableAlloyWANGAnan;CHENGShunqi;GUOZhiyao(KunmingUniversityofScienceandTechnology,... 相似文献
5.
The hot cracking of the continuous casting bullit is connected with its macrostructure and mechanical property burnt. The macrostructure and the mechanical property of 0. 13 wt- %C continuous casting bullit was investigated. The results are as follows: 1) the classical representation of the casting bullit shows three distinct zones, a peripherial region of small equiaxed grains, a columnar zone, and a central equiaxed zone. The rapid increase of the under cooling layer thickness is the criterion of the transformation from the columnar zone to central equiaxed zone; 2) The hardness decreases with the reducing of the solidification speed; 3) The tensile strength decreases gradually from the peripherial equiaxed maximum principal strain zone to central equiaxed zone ,and increases with the drop of the temperature. 相似文献
6.
The dendrite growth process of transparent NaBi(WO4)2 with small prandtl and high melting point was studied by using the in-situ observation system. According to the dynamic images and detailed information, there are two kinds of restriction effect on
the dendrite growth, the competition between arms and branches and the convection in the melt. The dendrite growth rate was
time dependent, and the rate of arm growth reached the maximum 5.8 mm/s in the diffusive-advective region and rapidly decreased
in the diffusive-convective region. The growth rate of branch had the same change trends as the arm’s. Based on the EPMA-EDS
data of solidification structure of quenched NaBi(WO4)2 melt, it was found that there were component differences from stoichiometric concentration in the melt near the interface
during the growth process.
Supported by the National Natural Science Foundation of China (Grant No. 50331040) and the Innovation Funds from Shanghai
Institute of Ceramics, Chinese Academy of Sciences (Grant No. SCX0623) 相似文献
7.
本文对液化气罐体焊缝和热影响区在高温冶金反应、结晶动力学及热循环的作用下,产生的一次结晶和二次结晶的组织形态、性能特征作了分析。实践表明,焊接夹杂和气孔是引起罐体焊缝裂纹或导致爆炸的主要原因。为此,作者提出,为了保证液化气罐焊接质量,必须从冶金和工艺两方面采取有效措施,迅速建立焊接质量监控系统,对焊接检验手段要进一步完善。 相似文献
8.
9.
往复挤压准晶增强快速凝固Mg92.5Zn6.4Y1.1合金 总被引:1,自引:0,他引:1
采用往复挤压工艺将快速凝固Mg92.5Zn6.4Y1.1合金薄带在330℃挤压2道次和4道次,然后正挤压制成Φ10 mm的棒材。用OM,TEM,XRD及DTA研究了往复挤压过程中准晶相I-Mg3YZn6弥散析出及对力学性能的影响。研究表明,往复挤压有利于快速凝固Mg92.5Zn6.4Y1.1合金薄带的焊合,获得组织致密、均匀、高强韧合金。往复挤压2道次,相组成为-αMg和准晶I-Mg3YZn6,脱溶析出纳米准晶相较少;4道次相组成为-αMg和准晶I-Mg3YZn6及MgZn相,脱溶弥散析出的纳米I-Mg3YZn6准晶相及MgZn相较多。往复挤压提高材料的拉伸性能,其主要原因是细晶强化和析出强化。 相似文献
10.
Differential scanning calorimetry and the advanced solidification processing of metals and alloys 总被引:2,自引:0,他引:2
B. Cantor 《Journal of Thermal Analysis and Calorimetry》1994,42(4):647-665
This paper describes some examples of the use of differential scanning calorimetry (DSC) in providing information for advanced solidification processing of metals and alloys. Spray forming, squeeze casting, grain refinement and crystallization of amorphous alloys are all discussed. DSC measurements are shown to be valuable for testing kinetic theories of nucleation and growth, and validating solidification process models. 相似文献