Effect of heat treatment on microstructures and properties of a novel Al-Zn-Mg-Cu alloy for oil drilling

In view of the special requirements for strength, heat resistance and corrosion resistance of Al-Zn-Mg-Cu alloy for oil drilling, the Al-6.2 Zn-2.5 Mg-1.6 Cu alloy was prepared by increasing Cu content on basis of Russian Series 1953 alloy. The effect of heat treatment on the microstructures and properties of the alloy was characterized by optical microscope(OM), scanning electron microscope(SEM) and transmission electron microscope(TEM), and investigated by tensile test at room temperature, thermal exposure test and corrosion test. The results show that the strength after T6 aging treatment exhibit a decrease trend as an increase of the solution temperature from465 °C to 480 °C. After the solution treated by the rate of 470 °C/1 h, second phases dissolve into the matrix very well and the strength property reaches optimum. The alloy has better comprehensive properties treated by a solution treatment of 470 °C/1 h and then followed by an aging treatment of 120 °C/24 h + 170 °C/1 h + 120 °C/24 h. Under the aging state, the precipitated phases inside the grains are suitable in size, while on the grain boundary distribute discontinuously and the precipitate-free zone is obvious. Besides, the alloy still maintain high tensile properties. The yield strength, tensile strength and elongation are 650 MPa, 686 MPa,12.0%, respectively. The yield strength retention after heat exposure is 92%. The alloy has good corrosion resistance and the exfoliation corrosion degree. The average corrosion rate in the H_2S and CO_2 environment is 0.0024 mm/a, which is far less than the required 0.12 mm/a. It is insensitive to H_2S and CO_2 environments.     

基于Sinc插值与相关谱的纵横波速度比扫描方法

在多分量地震技术中，准确地求取出纵、横波速比（γ）是多分量资料处理、反演、解释各环节中的一个重要步骤。由于地下同一层位具有相同的波阻抗比，因此该层位的反射纵波和反射转换波相互关联，纵横波速比与时间比存在相互转化关系。基于Sinc插值算法与相关系数谱分析的纵横波速比扫描方法是通过设置一系列γ，利用Sinc插值算法将纵波拉伸后与转换波进行互相关，当互相关系数达到最大时即可求出相应的γ。理论数据和实际资料的测试，验证了该方法的有效性、准确性和实用性。     

Metabolomics techniques applied in the investigation of phenolic acids from the agro-industrial by-product of Carapa guianensis Aubl

Processing of Carapa guianensis seeds to obtain oil on an industrial scale generates a significant amount of by-product, approximately 66% w/w, which is called cake and is a potential source of biomolecules, including simple phenolic structures. For this reason, studies were carried out on the chemical profiles of hydrolyzed extract from this agro-industrial by-product through High Performance Thin-Layer Chromatography (HPTLC) and Gas Chromatography coupled to Mass Spectrometry (GC–MS). These techniques were used to detect metabolic classes and/or groups, and to identify, for the first time, thirteen simple phenolic acids in this by-product. The sample antioxidant capacity was determined by methods of 2,2-diphenyl-1-picrylhydrazyl (DPPH)and 2,2′-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) diammonium salt (ABTS⁺) radicals direct sequestration. The hydrolyzed fraction showed a total of 63.47% in the relative abundance of the total of compounds, standing out: p-hydroxybenzoic acid (39.19%) and protocatechuic acid (3,4-dihydroxybenzoic acid) (5.62%), both from hydroxybenzoic acids and 3-(3,4-dihydroxyphenyl)lactic acid, (7.76%) hydroxycinnamic acids derivatives. In these results, the fraction rich in simple phenolic acids was obtained, attributing the prominent behavior of this matrix antioxidant activity, expressed by (IC₅₀: of 16.42 µg/mL and 6.52 µg/mL for DPPH and ABTS⁺ radicals, respectively). The research demonstrated an alternative to applicability that involves sustainability from agro-industrial. These techniques were used to detect metabolic classes and/or groups, and to identify, for the first time, thirteen simple phenolic acids in this by-product, generating a process capable of converting biomass into a bioproduct, consisting of bioactive compounds, in addition to adding value to the industrial chain.     

基于串联两阶段网络DEA模型的供应链规模收益分析

数据包络分析(DEA)是评价供应链系统(Supply chain system)间相对有效性的一种重要的工具,但是传统的DEA不考虑供应链的内部结构,对系统效率评价偏高;而本文所研究两阶段串联供应链系统,考虑把部分中间产品作为最终产品输出,增加额外中间投入的情形.基于所提出的供应链系统结构,本文建立相应的串联结构下的网络DEA模型,并针对所建立模型进行相关理论的研究,给出了串联结构下的生产可能集和规模收益情况判定方法.最后,进行数值实验,以验证我们提出的结论.     

论家庭教育中儿童人格的塑造与培养

父母及家庭环境对儿童人格形成与发展具有十分重要的影响。父母要以身示范,营造和睦、健康、向上的家庭氛围。在儿童人格塑造和培养中,要十分重视智力因素的培养,特别注意早期智力与创造力的开发,重视社会适应能力的培养,包括融入集体生活的能力、人际适应能力和环境适应能力等。     

NIPA类共聚温敏水凝胶中水的状态和耐热性

用N-异丙基丙烯酰胺（NIPA）与丙烯酸钠（SA）及甲基丙烯酸钠（SMA）共聚合成了两个系列的水凝胶，研究了共聚组成与水凝胶基本性质的关系，并用示差扫描量热法（DSC）和热失重法（TG）研究了此类水凝胶中水的状态和耐热性。     

待定系数法在无理函数积分中的应用

在教学过程中通过对练习题: 的求解、分析、综合和归纳得: (1) 式中P_n(X)_9 Q_n(x)均为n次多项式,其中Q_n(x)的各项系数待定。 (2) 式中P_n(x)为n次多项式,f_(n-1)(x)为各项系数待定的(n-1)次多项式,μ_n为待定常数。     

Necessary Conditions for Differentiability of Distance Functions

Necessary conditions for the Gâteaux differentiability of the distance function to a set are considered. A series of characterizing results is obtained.     

Coxeter Transformation and Quasiquivers

Mathematical Notes -