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1.
A sensitive and efficient method for trace analysis of some phenolic compounds using simultaneous derivatization and air‐assisted liquid–liquid microextraction from human urine and plasma samples followed by gas chromatography–nitrogen phosphorous detection
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Mir Ali Farajzadeh Mohammad Reza Afshar Mogaddam Ali Akbar Alizadeh Nabil 《Biomedical chromatography : BMC》2015,29(12):1921-1931
In present study, a simultaneous derivatization and air‐assisted liquid–liquid microextraction method combined with gas chromatography–nitrogen phosphorous detection has been developed for the determination of some phenolic compounds in biological samples. The analytes are derivatized and extracted simultaneously by a fast reaction with 1‐flouro‐2,4‐dinitrobenzene under mild conditions. Under optimal conditions low limits of detection in the range of 0.05–0.34 ng mL?1 are achievable. The obtained extraction recoveries are between 84 and 97% and the relative standard deviations are less than 7.2% for intraday (n = 6) and interday (n = 4) precisions. The proposed method was demonstrated to be a simple and efficient method for the analysis of phenols in biological samples. Copyright © 2015 John Wiley & Sons, Ltd. 相似文献
2.
室外空气污染和污染空气中的颗粒物是一类致癌物,而近年中国的大气颗粒物污染仍然维持在较高浓度水平。通过综述中国近年大气颗粒物污染现状和开展的颗粒物致癌机制研究,分析中国研究中颗粒物有关实验动物致癌性的证据和颗粒物致癌的人群流行病学线索,阐述大气颗粒物与癌症的关系,提出中国亟需开展相关研究。 相似文献
3.
随着经济快速发展,化石燃料已被大量开发和使用,一方面人类面临能源日渐匮乏的危机,另一方面能源大量浪费也引起全球环境问题.本文以环保和节能为目标,提出一种综合利用风力发电技术、热泵技术和低温地板辐射采暖技术的新型采暖模式,对使用可再生风能进行采暖,进行了可行性探讨. 相似文献
4.
文章在分析矩形型钢弯曲变形过程及应力与应变等方面的关系的基础上,推导出工件曲率半径与工件回弹后曲率半径之间的关系,从而确定了凸模半径。 相似文献
5.
Sensitivity analysis is a mathematical tool, first developed for optimization methods, which aim is to characterize a system response through the variations of its output parameters following modifications imposed on the input parameters of the system. Such an analysis may quickly become laborious when the thermal model under consideration is complex or the number of input parameters is high. In this paper, we develop a mathematical model to analyse the heat exchanges in four different types of solar air collectors. When building this thermal model we show that for each collector, at quasi-steady state, the energy balance equations of the components of the collector cascade into a single first-order non-linear differential equation that is able to predict the thermal behaviour of the collector. Our heat transfer model clearly demonstrates the existence of an important dimensionless parameter, referred to as the thermal performance factor of the collector, that compares the useful thermal energy which can be extracted from the heater to the overall thermal losses of that collector for a given set of input parameters. A sensitivity analysis of our thermal model has been performed for the most significant input parameters such as the incident solar irradiation, the inlet fluid temperature, the air mass flow rate, the depth of the fluid channel, the number and nature of the transparent covers in order to measure the impact of each of these parameters on our model. An important result which can be drawn from this study is that the heat transfer model developed is robust enough to be used for thermal design studies of most known flat plate solar air heaters, but also of flat plate solar water collectors and linear solar concentrators. 相似文献
6.
太阳能空调的可行性研究 总被引:3,自引:0,他引:3
对太阳能空调系统进行了定性分析 ,从环保、节能角度阐述了发展太阳能空调的优势所在。提出了太阳能空调将具有广阔的市场前景。 相似文献
7.
8.
气垫导轨在刚体转动惯量测定实验中的应用 总被引:1,自引:0,他引:1
本文介绍了一种测量刚体转动惯量的新方法。即把气垫导轨和刚体转动仪结合起来来测量刚体的转动惯量,使传统的气垫导轨实验和刚体转动惯量测定实验得以更新,提高了实验测量的精度,拓展了实验内容。 相似文献
9.
连铸坯角部传热过程的数值模拟 总被引:1,自引:0,他引:1
在连铸理论与实践研究的基础上,提出了系数法铸坯角部热通量模型,为准确研究铸坯角部传热、应力和角部缺陷的产生提供了条件。 相似文献
10.
The design guideline for the air suction drawing system with auxiliary air was analyzed, a spunbonding nonwoven system named PADHL1 - 3200 was designed and polypropylene (PP) spunbonded nonwoven fabrics with excellent properties were achieved after many trial runs. On the other hand, the suction air velocity (VA) was calculated and the influence of VA on the bonding strengh of PP nonwoven fabrics was Studied as well. It was found that VA is 1.5 - 2.5 times of the spinning velocity. With the increase of VA, PP fibers become finer and the bonding strength of PP nonwoven fabrics increases as well. 相似文献