Efficiency of composite vs. conically shaped chromatographic columns

The theory of composite chromatographic columns has been re-examined and general equations relating their efficiency to those of individual columns were derived. The derivations were based on elementary principles without reference to the principle of variance additivity. Derived also, were general equations for the efficiency of columns with continuously varying diameters, HETP and other properties from which formulae for special cases of practical interest were deduced. An example comparing the efficiencies of two columns, one conical and the other composite was given. The calculations show clearly that the conical column is superior in efficiency for the same total length and total retention volume.     

An investigation of glasses for capillary chromatography

An investigation was conducted of various glasses, other than soda lime or borosilicate, for use in glass capillary gas chromatography. The work has uncovered some unique chromatographic qualities in the use of potash soda lead and fused silica glasses as materials for making glass capillary columns. The fused silica proved to be an ideal material for capillary column construction, being inherently more inert than glass containing metal oxides. It has been shown that through the use of thin wall capillary tubing of high flexibility many of the mechanical problems associated with glass capillary columns, such as fragility and column straightening, can be avoided.     

多芯片LED与恒流源一体化混合集成设计

将多芯片LED与恒流源电路进行一体化混合集成电路工艺设计,保证了3～10W的多芯片集成LED在低于100mA的驱动电流下正常工作.恒流源采用跟随浮压技术进行设计,使集成LED的工作电压在2～200V,恒定工作电流在10～100mA选择.其恒流温度漂移小于5μA/℃,发光效率大于17Lm/W,同时简化了工频驱动电源电路的设计,减少远距离供电线路损耗.     

茶刺蛾[Darna trima(more)]颗粒体病毒鉴定及核酸与蛋白质特性的初步研究

1985年从四川珙县分离到的茶刺蛾病原物,经感染试验,组织病理研究,包涵体及病毒粒子超微结构研究,核酸类型鉴别等,定名该病原物为茶刺蛾颗粒体病毒.另对该病毒核酸作了限制性内切酶分析和热变性试验,测得该病毒核酸为双链DNA分子,分子量为64.11×10~6d,93.87kb,Tm值为67.3℃,(G+C)含量为32.7％,包涵体蛋白的氨基酸组分中Asp、Glu和Arg含量高,占氨基酸总量的34.12％,His,Cys和Met含量很少。该病毒对茶刺蛾幼虫有很强的感染力,氨基酸在生物防治上有潜在应用前景.     

Preconcentration of samples in sandwich tanks for continuous thin-layer chromatography

It is demonstrated that horizontai sandwich tank with two cover plates can be used to preconcentrate sample solutions. Narrow sharply-defined starting zones are obtained just outside the smaller cover plate when the series of spots of the sample solution are applied on the thin layer and predeveloped with a volatile solvent. After evaporation of the solvent, the whole area of the TLC-plate is covered with two plates and developed with a suitable solvent.     

竖轴式离心粉碎机的功耗确定

多碎少磨是国内外选矿界公认的节能降耗的有效方法,而超细粉碎又是降低入磨粒度、实现多碎少磨的最直接手段．本文在动力学研究的基础上,分析了竖轴式离心粉碎机的功耗计算,并推导出功耗与粉碎机的结构及主轴的回转速度有关,为竖轴式离心粉碎机的实际生产应用提供了理论基础。     

Uniformly More Powerful, Two-Sided Tests for Hypotheses about Linear Inequalities

Let Xhave a multivariate, p-dimensional normal distribution (p 2) with unknown mean and known, nonsingular covariance . Consider testing H ₀ : b _i 0, for some i = 1,..., k, and b _i 0, for some i = 1,..., k, versus H ₁ : b _i < 0, for all i = 1,..., k, or b _i < 0, for all i = 1,..., k, where b ₁,..., b _k , k 2, are known vectors that define the hypotheses and suppose that for each i = 1,..., k there is an j {1,..., k} (j will depend on i) such that b _i b _j 0. For any 0 < < 1/2. We construct a test that has the same size as the likelihood ratio test (LRT) and is uniformly more powerful than the LRT. The proposed test is an intersection-union test. We apply the result to compare linear regression functions.     

求解背包问题的并行混合遗传算法

针对基本遗传算法在求解大规模问题时，收敛速度缓慢、容易早熟的现象，借鉴生物区域性进化的原理，设计了一种基于星型迁移策略的并行混合遗传算法（Parallel Hybrid Genetic Algorithm，简称PHGA）．该算法采用高效的超贪心算子进行解码，使遗传进化过程从多个平均适应度较高的文明群体开始进化，并采用定期将各群体的最优个体输出给其他群体，使得最优个体共享，促进所有群体共同进化的共产主义迁移策略．在PVM环境下，对背包问题进行求解的实验，已取得超线性的加速比，并改进了解质量．     

浅议汉语中“字母词”的研究

从19世纪下半叶汉语中出现“字母词”的身影到近年来“字母词”的使用频率不断增加和使用领域逐步扩展,学者们对“字母词”的研究兴趣也与日俱增.和对其他语言现象的研究一样,学者们对汉语中“字母词”的研究也经历了萌芽、发展和成熟这三个不同阶段.与此同时,学者们对“字母词”的研究也经历了从最初只是对个别感兴趣的“字母词”进行研究,到后来逐步开始对字母词的名称、分类等各个方面的较为理论性的研究.当然,“字母词”的研究并非尽善尽美,有些方面的研究还有待完善.