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1.
Mu-Shih Lin Kuen-Tay Jeng 《Journal of polymer science. Part A, Polymer chemistry》1992,30(9):1941-1951
Poly(ethylene glycol) diacrylate was synthesized from poly(ethylene glycol) of molecular weight 600 with acryloyl chloride in a molar ratio of 1:2. Poly(ethylene glycol) diacrylate (PEGDA) was then blended with diglycidyl ether of bisphenol A (DGEBA) in various ratios, followed by curing with 2,2′-azobisisobutyronitrile (AIBN) and isophronediamine (IPDA) simultaneously. Viscosity changes before and during IPN formation were examined with a Brookfield viscometer. Formation of H-bonding and functional group changes were investigated with FTIR. Exothermic curing thermograms were recorded with dynamic DSC. Optically clear IPNs thus obtained were characterized with rheometric dynamic spectroscopy (RDS) and scanning electron microscopy (SEM) to check possible compatibility of the two networks. Experimental results revealed that during IPN formation hydrogen bonds between PEGDA and DGEBA and interlock of networks had profound effect on viscosity change and pot-life. Complete compatibility of the IPNs was found as DGEBA content was higher than 50% by weight. The compatibility between PEGDA and DGEBA networks was evidenced from inner shift of a single damping peak in RDS. In the meantime, SEM micrographs confirmed the coincidence with the result of RDS © 1992 John Wiley &Sons, Inc. 相似文献
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钱建华 《科技情报开发与经济》2005,15(2):182-183
介绍了炉膛爆炸的原因及防止措施,分析了传统炉膛压力控制系统的缺点,从高压保护回路、压力控制系统、运行程序、联锁系统等方面论述了新型炉膛防爆控制系统。 相似文献
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Mu-Shih Lin Kuen-Tay Jeng Kun-Yui Huang Yen-Fong Shih 《Journal of polymer science. Part A, Polymer chemistry》1993,31(13):3317-3325
Simultaneous interpenetrating polymer networks (SINs) based on diglycidyl ether of bis-phenol A (DGEBA) and poly(ethylene glycol) diacrylate (PEGDA) in weight ratios of 100/0, 50/50, and 0/100 were blended and cured simultaneously by using benzoyl peroxide (BPO) and m-xylenediamine (MXDA) as curing agents. A kinetic study during SIN formation was carried out at 45, 55, 63, and 70°C. Concentration changes for both the epoxide and C?C bond were monitored with FTIR. A rate expression for DGEBA cure kinetics was established with a model reaction of phenyl glycidyl ether (PGE) and benzylamine. Experimental results revealed that lower rate constants and higher activation energy for the SIN were found, compared with those for the constituent DGEBA and PEGDA network formation. A model of network interlock was proposed to account for this phenomenon. During simultaneous cure of DGEBA and PEGDA, the interlock (mutual entanglement) between DGEBA and PEGDA networks provided a sterically hindered environment, which subsequently increased the activation energy and reduced cure rates for both DGEBA and PEGDA. © 1993 John Wiley & Sons, Inc. 相似文献
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齐广 《内蒙古民族大学学报(自然科学版)》2007,22(6):642-647
农牧交错地带经济基础薄弱,生态环境脆弱,发展生产必须科学、可持续.否则会造成恶性循环,给人类带来灾难.笔者认为在农牧交错带开发草业是首选的产业,因为开发草业既可以保护环境,又可以解决养殖业中的饲草源,具有一定的经济效益和生态效益. 相似文献
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赵隽生 《河北科技大学学报》1995,(2)
重点介绍杜邦干法腈纶装置中的一个核心部分──聚合釜的工艺特点,及为实现此特殊的工艺要求,是如何配置自动控制系统和联锁的。 相似文献
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文章介绍了火焰检测器在制硫燃烧炉上的应用,包括其工作原理、工作过程以及在安装调试过程中所存在的问题和解决方案。实现了制硫燃烧炉的SIS顺控点火逻辑和紧急停车逻辑。双探头火焰检测器的应用提高了火焰检测的可靠性,对于降低故障率、安全生产具有现实意义。 相似文献
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通过预裂再生混凝土push-off试件的裂缝处剪力传递性能试验,研究了再生混凝土裂缝处骨料咬合及剪力传递性能.结果表明:再生混凝土裂缝处剪力传递性能总体上与普通混凝土较为接近;约束刚度越大,试件的剪力传递强度越高;再生混凝土强度越高,试件的剪力传递强度有一定的提高;相同混凝土强度下,随着再生粗骨料取代率的提高,试件剪力传递强度略有降低.借鉴Walraven的理论,并考虑再生混凝土的细微观结构与再生粗骨料的几何特点,得到了再生混凝土中的骨料咬合模型.试验中各试件的剪力传递强度值与相关理论计算值吻合良好. 相似文献