排序方式: 共有76条查询结果,搜索用时 7 毫秒
1.
NSRL-XAFS光束线弧矢聚焦双晶单色器设计 总被引:1,自引:1,他引:0
针对XAFS光束线能量动态扫描的实验特点,介绍了弧矢聚焦双晶单色器的物理设计:包括晶体光学结构、性能参数计算、晶体热载分析和弧矢弯曲原理.弧矢缩比选择为1:4.88,水平接收角由原来的1mrad拓宽到3mrad,在不改变基本配置的情况下,获得了样品上束癍缩小、光子通量高达半个量级以上的增益. 相似文献
2.
NSRL光电子能谱实验控制软件设计及其应用 总被引:1,自引:0,他引:1
介绍一种同步辐射光电子能谱实验的软件.软件对光束线的控制由罗兰圆模式改为DRAGON模式[1],光通过率提高2~3倍.软件不仅可以做以X射线枪为激发源的X射线激发谱(XPS),还可以做以同步辐射光为激发源的能量分布曲线谱(EDC)、固定终态谱(CFS)和固定初态谱(CIS).软件使用图形的菜单界面,可视化操作,运行稳定,满足科学实验的要求 相似文献
3.
Upgrade of beamline BL08B at Taiwan Light Source from a photon‐BPM to a double‐grating SGM beamline
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Jih‐Young Yuh Shan‐Wei Lin Liang‐Jen Huang Hok‐Sum Fung Long‐Life Lee Yu‐Joung Chen Chiu‐Ping Cheng Yi‐Ying Chin Hong‐Ji Lin 《Journal of synchrotron radiation》2015,22(5):1312-1318
During the last 20 years, beamline BL08B has been upgraded step by step from a photon beam‐position monitor (BPM) to a testing beamline and a single‐grating beamline that enables experiments to record X‐ray photo‐emission spectra (XPS) and X‐ray absorption spectra (XAS) for research in solar physics, organic semiconductor materials and spinel oxides, with soft X‐ray photon energies in the range 300–1000 eV. Demands for photon energy to extend to the extreme ultraviolet region for applications in nano‐fabrication and topological thin films are increasing. The basic spherical‐grating monochromator beamline was again upgraded by adding a second grating that delivers photons of energy from 80 to 420 eV. Four end‐stations were designed for experiments with XPS, XAS, interstellar photoprocess systems (IPS) and extreme‐ultraviolet lithography (EUVL) in the scheduled beam time. The data from these experiments show a large count rate in core levels probed and excellent statistics on background normalization in the L‐edge adsorption spectrum. 相似文献
4.
Thierry Moreno 《Journal of synchrotron radiation》2015,22(5):1163-1169
Synchrotron infrared beamlines are powerful tools on which to perform spectroscopy on microscopic length scales but require working with large bending‐magnet source apertures in order to provide intense photon beams to the experiments. Many infrared beamlines use a single toroidal‐shaped mirror to focus the source emission which generates, for large apertures, beams with significant geometrical aberrations resulting from the shape of the source and the beamline optics. In this paper, an optical layout optimized for synchrotron infrared beamlines, that removes almost totally the geometrical aberrations of the source, is presented and analyzed. This layout is already operational on the IR beamline of the Brazilian synchrotron. An infrared beamline design based on a SOLEIL bending‐magnet source is given as an example, which could be useful for future IR beamline improvements at this facility. 相似文献
5.
A low-cost optical feedback system using dynamic mirrors has been developed at the NSLS for stabilizing the position and direction of an infrared synchrotron beam against thermal drift and mechanical noise. The system design has some unique features that potentially simplify installation into an existing infrared beamline. We describe the system and its features along with some performance results. 相似文献
6.
André Rothkirch G. Diego Gatta Mathias Meyer Sébastien Merkel Marco Merlini Hanns‐Peter Liermann 《Journal of synchrotron radiation》2013,20(5):711-720
Fast detectors employed at third‐generation synchrotrons have reduced collection times significantly and require the optimization of commercial as well as customized software packages for data reduction and analysis. In this paper a procedure to collect, process and analyze single‐crystal data sets collected at high pressure at the Extreme Conditions beamline (P02.2) at PETRA III, DESY, is presented. A new data image format called `Esperanto' is introduced that is supported by the commercial software package CrysAlisPro (Agilent Technologies UK Ltd). The new format acts as a vehicle to transform the most common area‐detector data formats via a translator software. Such a conversion tool has been developed and converts tiff data collected on a Perkin Elmer detector, as well as data collected on a MAR345/555, to be imported into the CrysAlisPro software. In order to demonstrate the validity of the new approach, a complete structure refinement of boron‐mullite (Al5BO9) collected at a pressure of 19.4 (2) GPa is presented. Details pertaining to the data collections and refinements of B‐mullite are presented. 相似文献
7.
XDS: a flexible beamline for X‐ray diffraction and spectroscopy at the Brazilian synchrotron
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F. A. Lima M. E. Saleta R. J. S. Pagliuca M. A. Eleotério R. D. Reis J. Fonseca Júnior B. Meyer E. M. Bittar N. M. Souza-Neto E. Granado 《Journal of synchrotron radiation》2016,23(6):1538-1549
The majority of the beamlines at the Brazilian Synchrotron Light Source Laboratory (LNLS) use radiation produced in the storage‐ring bending magnets and are therefore currently limited in the flux that can be used in the harder part of the X‐ray spectrum (above ~10 keV). A 4 T superconducting multipolar wiggler (SCW) was recently installed at LNLS in order to improve the photon flux above 10 keV and fulfill the demands set by the materials science community. A new multi‐purpose beamline was then installed at the LNLS using the SCW as a photon source. The XDS is a flexible beamline operating in the energy range between 5 and 30 keV, designed to perform experiments using absorption, diffraction and scattering techniques. Most of the work performed at the XDS beamline concentrates on X‐ray absorption spectroscopy at energies above 18 keV and high‐resolution diffraction experiments. More recently, new setups and photon‐hungry experiments such as total X‐ray scattering, X‐ray diffraction under high pressures, resonant X‐ray emission spectroscopy, among others, have started to become routine at XDS. Here, the XDS beamline characteristics, performance and a few new experimental possibilities are described. 相似文献
8.
Calibration of a compact XUV soft X‐ray monochromator with a digital autocollimator in situ
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Jih-Young Yuh Shang-Wei Lin Liang-Jen Huang Long-Life Lee 《Journal of synchrotron radiation》2016,23(5):1232-1236
A digital autocollimator of resolution 0.1 µrad (0.02 arcsec) serves as a handy correction tool for calibrating the angular uncertainty during angular and lateral movements of gratings inside a monochromator chamber under ultra‐high vacuum. The photon energy dispersed from the extreme ultraviolet (XUV) to the soft X‐ray region of the synchrotron beamline at the Taiwan Light Source was monitored using molecular ionization spectra at high resolution as energy references that correlate with the fine angular steps during grating rotation. The angular resolution of the scanning mechanism was <0.3 µrad, which results in an energy shift of 80 meV at 867 eV. The angular uncertainties caused by the lateral movement during a grating exchange were decreased from 2.2 µrad to 0.1 µrad after correction. The proposed method provides a simple solution for on‐site beamline diagnostics of highly precise multi‐axis optical manipulating instruments at synchrotron facilities and in‐house laboratories. 相似文献
9.
Wantana Klysubun Pinit Kidkhunthod Pongjakr Tarawarakarn Panidtha Sombunchoo Chanapa Kongmark Sukit Limpijumnong Saroj Rujirawat Rattikorn Yimnirun Gamolwan Tumcharern Kajornsak Faungnawakij 《Journal of synchrotron radiation》2017,24(3):707-716
The SUT‐NANOTEC‐SLRI beamline was constructed in 2012 as the flagship of the SUT‐NANOTEC‐SLRI Joint Research Facility for Synchrotron Utilization, co‐established by Suranaree University of Technology (SUT), National Nanotechnology Center (NANOTEC) and Synchrotron Light Research Institute (SLRI). It is an intermediate‐energy X‐ray absorption spectroscopy (XAS) beamline at SLRI. The beamline delivers an unfocused monochromatic X‐ray beam of tunable photon energy (1.25–10 keV). The maximum normal incident beam size is 13 mm (width) × 1 mm (height) with a photon flux of 3 × 108 to 2 × 1010 photons s?1 (100 mA)?1 varying across photon energies. Details of the beamline and XAS instrumentation are described. To demonstrate the beamline performance, K‐edge XANES spectra of MgO, Al2O3, S8, FeS, FeSO4, Cu, Cu2O and CuO, and EXAFS spectra of Cu and CuO are presented. 相似文献
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