基于多材质复合管柱的裸眼井壁支撑工艺及应用

已完钻超深裸眼水平井侧钻技术是经济、高效开发油藏剩余油的主要手段之一，传统的磨铣钢套管开窗侧钻技术存在下入摩阻大、磨铣耗时长导致开窗失败等问题。为此，提出了基于多材质复合管柱的超深水平井裸眼井壁支撑工艺，结合中国西北油田已完钻超深裸眼水平井井况，首先，提出了基于“铝合金+碳钢”的多材质复合管柱组合及设计方法；其次，开展了基于管柱实物屈曲实验数据的管柱临界屈曲载荷计算模型适用性评价，并优选出了适合于“铝合金+碳钢”多材质复合管柱的屈曲临界载荷计算模型；最后，研究了综合考虑管柱扭矩、摩阻、刚性、井眼条件、管柱强度及材质的多材质复合管柱下入性分析方法，并利用下入性分析软件对西北油田顺北X1井、X2井、X3井、X4井复合管柱进行了下入可行性评价。该方法在X1井和X2井得到成功应用，进一步论证了该工艺现场应用的可行性。研究成果可为超深水平井裸眼井壁支撑的复合管柱设计和下入可行性评价提供理论参考。     

Effect of heat treatment on microstructures and properties of a novel Al-Zn-Mg-Cu alloy for oil drilling

In view of the special requirements for strength, heat resistance and corrosion resistance of Al-Zn-Mg-Cu alloy for oil drilling, the Al-6.2 Zn-2.5 Mg-1.6 Cu alloy was prepared by increasing Cu content on basis of Russian Series 1953 alloy. The effect of heat treatment on the microstructures and properties of the alloy was characterized by optical microscope(OM), scanning electron microscope(SEM) and transmission electron microscope(TEM), and investigated by tensile test at room temperature, thermal exposure test and corrosion test. The results show that the strength after T6 aging treatment exhibit a decrease trend as an increase of the solution temperature from465 °C to 480 °C. After the solution treated by the rate of 470 °C/1 h, second phases dissolve into the matrix very well and the strength property reaches optimum. The alloy has better comprehensive properties treated by a solution treatment of 470 °C/1 h and then followed by an aging treatment of 120 °C/24 h + 170 °C/1 h + 120 °C/24 h. Under the aging state, the precipitated phases inside the grains are suitable in size, while on the grain boundary distribute discontinuously and the precipitate-free zone is obvious. Besides, the alloy still maintain high tensile properties. The yield strength, tensile strength and elongation are 650 MPa, 686 MPa,12.0%, respectively. The yield strength retention after heat exposure is 92%. The alloy has good corrosion resistance and the exfoliation corrosion degree. The average corrosion rate in the H_2S and CO_2 environment is 0.0024 mm/a, which is far less than the required 0.12 mm/a. It is insensitive to H_2S and CO_2 environments.     

Formation of low-temperature deformation-induced segregations of nickel in Fe–Ni-based austenitic alloys

ABSTRACT

The authors present the results of an investigation in Fe–Ni-Cr austenitic alloys of the low-temperature deformation-induced segregations of nickel that form in the micro regions being (i) located close to grain- and subgrain boundaries and (ii) characteristic of the concentration and magnetic inhomogeneities indicated by the appearance of a dark diffraction contrast at the electron diffraction patterns taken from these regions typical (at the same time) of an enhanced value of Curie temperature. The observed effects were connected with the micro distortions caused by the local change of lattice parameter because of an increase in nickel concentration, as well as in the result of a magnetostriction dilatation. Using methods of the X-ray energy dispersive spectroscopy (XEDS) and atomic-probe body-section radiography (tomography – APT) has made it possible to determine the borders of those regions of austenite that were characteristic of an enhanced concentration of nickel in the fields of the localisation of a deformation-induced segregation of nickel in the vicinity of grain (subgrain) boundaries of austenitic alloys of the types Fe–13Cr–30Ni and Fe–37Ni–3Ti.     

激光快速成型TC4合金显微组织及力学性能

采用金相显微镜、扫描电镜、电子拉伸机等，研究了激光快速成型TC4合金沉积态在平行沉积方向和垂直沉积方向的组织和力学性能.结果表明:激光快速成型TC4合金沉积态宏观组织沿沉积方向生长的粗大β柱状晶呈明暗相间的条带状结构，具备典型的魏氏组织特征;垂直沉积方向的强度比平行沉积方向的强度高，但塑性低;合金断口为韧窝状断口，垂直沉积方向的断口韧窝尺寸比平行沉积方向的小.     

运用试验设计法优化某军品压铸弹尾工艺

根据某军品部件出现的问题，应用试验设计法成功地找出了最优组合，提高了该部件的强度，解决了该强度问题，使生产得以正常进行。     

铅锡合金沉积物的显微组织

将离子浓度比为5∶5的铅锡电沉积分形生长沉积物制备成金相样品，用金相显微镜观察了它们的显微组织。结果表明，在此情况下，铅锡电沉积生成物由两相组成，即铅锡共晶相和铅基固溶相，两相呈交替层状分布。     

High index of refraction via quantum interference in a three-level system of Er^3＋-doped yttrium aluminium garnet crystal

A simple three-level system is proposed to produce high index of refraction with zero absorption in an Er^3＋-doped yttrium aluminium garnet （YAG） crystal, which is achieved for a probe field between the excited state 4I13/2 and ground state 4I15/2 by adjusting a strong coherent driving field between the upper excited state 4I11/2 and 4I15/2. It is found that the changes of the frequency of the coherent driving field and the concentration of Er^3＋ ions in the YAG crystal can maximize the index of refraction accompanied by vanishing absorption. This result could be useful for the dispersion compensation in fibre communication, laser particle acceleration, high precision magnetometry and so on.     

93W合金有关力学参量的综合选评

 对93W合金材料进行了超声测量实验，并结合原有的超声测量结果进行了分析比较，提出了可以直接用冲击波速度关系式的三个系数c₀ 、λ和λ′来对钨合金的有关力学参量，如G₀、K₀、G₀′、K₀′等进行综合选评的方法。得到了一组对93W合金较为合理的力学参量推荐值。     

铝电解中的阴极过程

对铝电解中的阴极反应、阴极过电压、阴极表面的双电层结构等阴极过程进行了研究,发现在+005～-005V(相对于铝阴极)电位区有一个还原电流峰和一个氧化电流峰,它们是Al3++3e→Al和Al-3e→Al3+·与阳极相比,阴极过电压较小,在001～3A/cm2的Taffel区,约为01V·在阴极表面的双电层中,第一层为Ca2+,Mg2+,Li+和Al3+离子,没有Na+离子,这说明,阴极过电压是因为Mg2+,Ca2+等离子形成的电化学双电层阻力所引起,同时也说明别略耶夫猜想基本是正确的·     

Chronoamperometric studies in an ammonia citrate electrolyte for the deposition of a nickel-molybdenum alloy

Dependences of the current and the chemical composition of cathodic deposits on the electrolysis time are studied in an ammonia-citrate electrolyte for the deposition of a nickel-molybdenum alloy in potentiostatic conditions. At potentials less negative than ?0.93 V, no nickel-molybdenum alloy deposition occurs and in the course of electrolysis there is observed a decrease in the current, which is connected with the blocking of the electrode surface by the formed molybdenum oxides. In the region of potentials of deposition of a nickel-molybdenum alloy there is realized the following shape of a time dependence of the current. Within the first few seconds of the electrolysis process, the current somewhat decreases. Then there occurs its increase, which is connected with the alloy deposition on the cathode. In the course of electrolysis there occurs a decrease in the molybdenum content in the cathodic deposit.