Tasumatrols P – T,Five New Taxoids from Taxus sumatrana

The phytochemical investigation of the more polar fractions from the leaves and twigs of Taxus sumatrana (Taxaceae) afforded five new taxane diterpene esters, tasumatrols P–T ( 1 – 5 ) possessing an 11(15→1),11(10→9)‐diabeotaxane skeleton. Compounds 1, 4 , and 5 contain an α‐hydroxy group at C(14), while 3 has no OH group at either C(13) or C(14). Compound 2 is a natural 4,5‐acetonide derivative, while 4 has an unusual spiro‐connected 2‐hydroxy‐2‐phenyl‐1,3‐dioxolane ring. Ten known taxoids, were also isolated in the course of the chromatographic fractionation. Five additional new O‐acetyl derivatives 3a, 4a, 4b, 5a , and 5b were prepared from the taxanes 3 – 5 . The structures of all new compounds were established on the basis of their spectroscopic analyses. Compound 1 showed mild cytotoxic activity against human Hela and Daoy tumor cells.     

教学录象带的计算机辅助制作

常规教具的计算机辅助制作是计算机辅助教学的一项新内容．本文通过对实际操作方法的叙述,较为详细地介绍了在办公室条件下,利用多媒体微机及普通录象机制作教学录象带的过程．这些方法具有较高的实用价值．     

Optimization of the extraction of paclitaxel from Taxus baccata L. by the use of microwave energy

A simple and rapid microwave-assisted extraction (MAE) procedure was developed and optimized for the extraction of paclitaxel (Taxol) from the needles of yew trees Taxus baccata L. grown in Iranian habitats. The samples, immersed in a methanol-water mixture, were irradiated with microwaves in a closed-vessel system. The method was evaluated using a factorial design approach based on parameters such as extraction time, temperature, methanol concentration in water (v/v), and the ratio of grams of sample to 10 mL of solvent. Statistical treatment of the results revealed that the selected parameters were all significant except the extraction time. Optimum conditions would be 1.5 g samples in 10 mL solvent (90% methanol), an extraction temperature of 95 degrees C, and an extraction time of 7 min. The extracts has been analyzed by reverse-phase high-performance liquid chromatography with UV detection (LC/UV) at 227 nm for quantification. Liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for confirmation. The main advantage of the proposed MAE method versus conventional solvent extraction (CSE) are the considerable reductions in time (7 min versus 16 h) and in solvent consumption (20 mL versus 150 mL). The MAE procedure yielded extracts that could be analyzed directly without any preliminary clean-up or solvent exchange steps. Both extraction methods show RSDs lower than 10% and lead to comparable recoveries of paclitaxel (87-92%).     

JMF技术在网络多媒体教学系统中的应用研究

 网络多媒体教学与一般的网络多媒体应用的主要差别在于同时包括了视频流、音频流和课件板书数据流等,本文讨论了JMF(Java Media Framework)应用于网络多媒体教学系统开发研究中的几个问题,给出了其中的2个主要部分:JMF API和JMF RTP API的实现方式,在网络课堂实录系统的开发中取得了较好的效果.     

多媒质区域介质子网格时域有限差分法

介绍了应用于多媒质区域电磁问题的介质子网格时域有限差分法．该方法在保证精度的前提下，节省了大量计算时间及计算机内存，尤其在处理多媒质界面方面具有很大的优势．     

采用工艺巷防止高瓦斯易自燃综放面上隅角瓦斯积聚的探讨

上隅角瓦斯积聚是采用综呆放顶煤技术开采高瓦斯易自燃煤层必须面对的难题。文章提出了利用工艺巷防止综放面上隅角瓦斯积聚的方法。并且,根据计算流体力学理论建立数学物理模型,模拟计算了综放工作面及采空区内空气、瓦斯流动的规律,有力地论证了该方法的可行性和有效性,为我国高瓦斯易自燃煤层综放工作面的瓦斯防治工作提供了新的思路。     

流媒体应用层组播实现的探讨

本文根据应用层组播的原理和协议,对基于数据驱动的流媒体应用层组播的实现方法进行探讨．     

山西天然南方红豆杉林及群落特点的研究

本文对南方红豆杉的地理分布和以它为优势种的森林植被在山西省的生态环境、植物区系组成及群落结构进行了初步研究并建议加强保护和发展.     

变温层积处理对南方红豆杉种子生理生化特性的影响

脱除外被蜡质层的南方红豆杉种子,经低-暖-低变温层积结合植物生长调节剂及微量元素处理,120 d休眠解除.未层积处理的种子可供胚呼吸直接利用的可溶性糖等含量低.变温层积处理后,种子蛋白质、氨基酸和可溶性糖含量分别比对照提高了27.6%、80.0%和107.1%,脂肪含量降低了16.4%;种子脱氢酶、过氧化物酶和多酚氧化酶活性分别比对照提高了7.6%、129.3%和119.6%,蛋白酶活性降低了13.3%;解剖学特征表明,经变温层积处理,种子胚的发育渐进完善.实验结果提示种子贮藏物质特别是脂类物质的分解、转化和利用可能是南方红豆杉种子休萌解除的关键.     

流媒体技术概述

通过对网络连续媒体实时传输的分析，着重对流媒体技术进行了较为深入的研究和比较，并结合网络教学的要求，设计了一套基于Microsoft的wmv流文件格式的实施方案。