全文获取类型
收费全文 | 838篇 |
免费 | 38篇 |
国内免费 | 36篇 |
专业分类
化学 | 622篇 |
晶体学 | 4篇 |
力学 | 10篇 |
综合类 | 19篇 |
数学 | 55篇 |
物理学 | 100篇 |
无线电 | 102篇 |
出版年
2023年 | 12篇 |
2022年 | 57篇 |
2021年 | 45篇 |
2020年 | 27篇 |
2019年 | 33篇 |
2018年 | 35篇 |
2017年 | 52篇 |
2016年 | 41篇 |
2015年 | 40篇 |
2014年 | 42篇 |
2013年 | 52篇 |
2012年 | 46篇 |
2011年 | 38篇 |
2010年 | 35篇 |
2009年 | 33篇 |
2008年 | 42篇 |
2007年 | 52篇 |
2006年 | 31篇 |
2005年 | 28篇 |
2004年 | 19篇 |
2003年 | 20篇 |
2002年 | 23篇 |
2001年 | 20篇 |
2000年 | 16篇 |
1999年 | 9篇 |
1998年 | 11篇 |
1997年 | 7篇 |
1996年 | 8篇 |
1995年 | 9篇 |
1994年 | 7篇 |
1993年 | 4篇 |
1992年 | 3篇 |
1991年 | 1篇 |
1990年 | 1篇 |
1988年 | 4篇 |
1987年 | 2篇 |
1986年 | 3篇 |
1985年 | 1篇 |
1984年 | 1篇 |
1982年 | 1篇 |
1978年 | 1篇 |
排序方式: 共有912条查询结果,搜索用时 15 毫秒
1.
2.
Summary The aim of this investigation was to obtain qualitative and quantitative profiles of the flavonoid and biflavonoid composition
of six cypress species—Cupressus funebris L.,Cupressus sempervirens L.,Cupressus glabra L.,Cupressus arizonica L.,Cupressus goveniana L., andCupressus lusitanica L. HPLC-diode-array detection (DAD), HPLC-MS, and HPTLC were used to identify the individual compounds. A chromatographic
method was optimized for identification and quantification of the main flavonoid glycosides and biflavonoids. The flavonoids
identified and calibrated were: rutin, quercetin glucoside, quercetin rhamnoside, and kaempferol 3-O-rhamnoside. The biflavonoids identified and calibrated were: cupressuflavone, amentoflavone, robustaflavone, hinokiflavone,
methylrobustaflavone, methylamentoflavone, and dimethylcupressuflavone. 相似文献
3.
4.
5.
6.
近年来,国内外数据泄露事件频发,大量企业的商业利益、声誉受损。数据安全法律法规相继颁布,监管力度不断升级,企业逐渐意识到数据安全治理的重要性与紧迫性。通过对2021年开展的企业数据安全治理能力评估现状进行整理,总结企业数据安全治理工作在组织建设、人才培养、技术工具等方面的现状与趋势,提供能力提升思路,以供业界参考。 相似文献
7.
A new extraction method for ginsenosides from ginseng roots, ginseng leaves and ginseng drug preparations by Sep-Pak C18 cartridges has been studied. Ginsenoside extraction by Sep-Pak cartridges is a rapid, efficient, reproducible method. In addition, the extracts were analyzed by high performance thin layer chromatography (HPTLC) and reverse phase high performance liquid chromatography (HPLC). The major components of ginseng saponins were effectively separated using an ODS-120T column. 相似文献
8.
Four myrosinase (β-thioglucosidase EC. 3.2.3.1) and seven disaccharase (β-fructofuranosidase, EC. 3.2.1.26) isoenzymes were isolated from turnip leaves. The most active enzymes were isolated in pure
form. Myrosinase and disaccharase mol wt was 62.0 × 103 and 69.5 × 103 dalton, respectively, on the basis of gel filtration on Sephadex G-200.
Myrosinase pH profile showed high activity between pH 5 and 7 with the optimum at pH 5.5. The purified enzyme was heat-stable
for 60 min at 30°C with only loss of 24% of activity. Its activity is strongly inhibited (100%) by Pb2+, Ba2+, Cu2+ and Ca2+ ions, and activated (70%) by EDTA at 0.04M. The pure enzyme failed to hydrolyze amylose, glycogen, lactose, maltose, and
sucrose. TheK
m andV
max values of myrosinase using sinigrin as specific substrate was 0.045 mM and 2.5 U, respectively.
The maximal activity of disaccharase enzyme was obtained at pH 4–5 and 35–37°C. The enzyme was heat-stable at 30°C for 30
min with only 10% loss of its activity. Its activity is strongly activated (70–240%) by Ca2+, Ba2+, Cu2+, and EDTA at 0.01M. The enzyme activity is specific to the disaccharide sucrose and failed to hydrolyze other disaccharides (maltose and lactose).
TheK
m andV
max of disaccharase were 0.123 mM and 3.33 U, respectively. 相似文献
9.
烟草三维荧光特征和品质评吸的关系 总被引:2,自引:0,他引:2
研究不同品种烟草石油醚冷萃取物的三维荧光光谱,包括烟草所共在的荧光性质和各自的荧光特性,寻找它们与烟草香味,颈头等吃味之间的关系,选择合适的量值指标,为烟草品质的 观感官评估提供了一个实用的对照方法。 相似文献
10.
Sansei Nishibe Kumiko Mitsui-Saitoh Junichi Sakai Takahiko Fujikawa 《Molecules (Basel, Switzerland)》2021,26(8)
Forsythia fruit (Forsythia suspensa Vahl (Oleaceae)) is a common component of Kampo medicines for treating the common cold, influenza, and allergies. The main polyphenolic compounds in the leaves of F. suspensa are pinoresinol β-d-glucoside, phillyrin and forsythiaside, and their levels are higher in the leaves of the plant than in the fruit. It is known that polyphenolic compounds stimulate lipid catabolism in the liver and suppress dyslipidemia, thereby attenuating diet-induced obesity and polyphenolic anti-oxidants might attenuate obesity in animals consuming high-fat diets. Recently, phillyrin was reported as a novel cyclic AMP phosphodiesterase 4 (PDE4) inhibitor derived from forsythia fruit. It was expected that the leaves of F. suspensa might display anti-obesity effects and serve as a health food material. In this review, we summarized our studies on the biological effects of forsythia leaves containing phillyrin and other polyphenolic compounds, particularly against obesity, atopic dermatitis, and influenza A virus infection, and its potential as a phytoestrogen. 相似文献