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排序方式: 共有1124条查询结果,搜索用时 652 毫秒
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Elnaz Marzi Khosrowshahi Behnaz Limuie Khosrowshahi Mir Ali Farajzadeh Abolghasem Jouyban Mustafa Tuzen Mohammad Reza Afshar Mogaddam Mahboob Nemati 《Biomedical chromatography : BMC》2022,36(7):e5371
A dispersive solid-phase extraction method based on a new sorbent has been performed on plasma and wastewater samples to determine metoprolol by high-performance liquid chromatography–tandem mass spectrometry. In this study, the analyte was adsorbed from the samples onto microcrystalline cellulose as a green and efficient sorbent and then eluted for use in the determination step. In the mass spectrometer, the analyte was detected in the positive mode and selectivity of the analysis was increased by sequential mass analysis through multiple reaction monitoring. All of the effective parameters in the extraction of metoprolol from plasma and wastewater were optimized. Under optimal conditions the method was linear in the ranges of 1–1,000 and 0.1–1,000 ng/ml in plasma and wastewater samples, respectively. The detection limits of the method were 0.30 and 0.03 ng/ml in plasma and wastewater samples, respectively. The data showed that the method provides low detection limit, wide linear range, good precision and high extraction recovery. Finally several plasma and wastewater samples were successfully analyzed using the method. The use of a small amount of a green and inexpensive sorbent and a low volume of plasma without the need for further pretreatment steps are the main advantages of the method. 相似文献
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S. P. Popov 《Computational Mathematics and Mathematical Physics》2006,46(6):983-994
Numerical solutions to three systems of integrable evolutionary equations from the Toda lattice hierarchy are analyzed. These are the classical Toda lattice, the second local dispersive flow, and the second extended dispersive flow. Special attention is given to the properties of soliton solutions. For the equations of the second local flow, two types of solitons interacting in a special manner are found. Solutions corresponding to various initial data are qualitatively outlined. 相似文献
5.
R. S. Kaler 《Fiber and Integrated Optics》2006,25(1):41-57
In this article, the comparison of large signal theory and small signal theory has been done with dispersive propagation of optical signal with IMDD (Intensity Modulation Direct Detection) systems for semiconductor lasers with higher-order dispersion terms. The expressions for an exact large signal theory and small signal theory including higher-order dispersion terms for propagation of an optical wave with sinusoidal amplitude and frequency modulation in a dispersive fiber have been derived. It is observed that small signal theory is more sensitive compared to large signal theory in terms of intensity modulation/direct detection systems. Also, it is reported that for large signal analysis the higher-order effects of dispersion can be ignored, whereas for small signal theory, the higher-order effects can be ignored for lower modulation frequencies only. The variation in the transfer function for various values of modulation indices are greater for small signal analysis than for large signal analysis. Also, as the intensity modulation index is increased, there is a decrease in the value of transfer function. The large signal model approximates the small signal model for lower values of the intensity modulation index. 相似文献
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CDMA时变色散信道的两级盲辨识算法 总被引:1,自引:0,他引:1
本文通过对时变信道的扩展函数在时频域进行正则采样,得到了CDMA时变系统的离散正则模型。针对该模型提出了一种具有较低运算量的两级盲辨识算法。为避免两级算法产生的误差传播效应,文章将理想SIMO模型等效为加性噪声模型来处理。与基展开模型方法相比,该算法具有不需利用观测数据的高阶统计量估计展开基频率的优点。文章通过仿真验证了该算法是可行的。 相似文献
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It is shown that the condition υ > υp (ω), which is necessary in order to trigger the Vavilov-Cherenkov effect, determines the interval of radiated frequencies
and it alone cannot establish a strong restriction to the velocity of the particle. It is exhibited that it is possible to
define a general lower bound for the velocity of the particle, which does not depend on the frequency when both, a specific
response of the medium is taken into account and the mentioned condition is considered. The minimum value of the phase velocity
of light in the medium determines the existence of such general lower bound. 相似文献
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利用相位共轭技术补偿光纤中色散效应的条件 总被引:1,自引:0,他引:1
利用相位共轭器的频率反转特性的,补偿光纤中的色散效应,在理论上和实验上得到了证明.由色散脉冲的傅里叶交换确定了光纤中二次色散效应可以被忽略的条件,得到了共轭器的反射率和带宽与非线性介质的长度L,参数|K|L之间的关系曲线,找到了影响补偿效果的主要因素. 相似文献
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Recent X-ray diffraction studies on α-quartz (SiO2) by Kingmaet al [1], have shown the occurrence of a reversible, crystalline-to-crystalline, phase transition just prior to amorphization
at ≈ 21 GPa. This precursor transition has also been confirmed by our recent molecular dynamics simulation study [2]. In order
to investigate the possibility of a similar behaviour in other isostructural compounds, which also undergo pressure induced
amorphization, α-GeO2 and α-AlPO4 (berlinite form) were studied using energy dispersive X-ray diffraction. In either of these materials, no such phase transition
is detected prior to amorphization. The onset of amorphization and its reversal is found to be time dependent in GeO2. 相似文献
10.
Cu-12.7(wt)%Al合金从900℃高温淬至365℃~500℃温度范围等温不同时间(30秒至15分钟)的试样中形成了大量树枝状的γ_2相沉淀粒子。应用配有X线能谱仪(XEDS)和电子能量损失谱仪(EELS)的分析电子显微镜(JEOL JEM-2000FX型)对上还试样研究,结果表明:这些γ_2相粒子具有富铝的“核心”,长大到粒子线度大于约800nm后以不稳定方式生长成“花朵”状。生长过程中伴随着溶质元素Al由基体向γ_2相内的富集。而且在γ_2相粒子内部呈现出Spinodal分解组织的形貌特征,表明γ_2粒子内形成了化学成分调幅。EELS分析表明试样含氧。 相似文献