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排序方式: 共有138条查询结果,搜索用时 15 毫秒
1.
地方时与区时在电离层研究中的差异 总被引:2,自引:0,他引:2
本文指出混淆地时与区时两个时间概念在电离层研究中带来的差异的严重性,建议使用地方与区时这两个名词,而抛弃“本地时”和“当地时”等容易引起混淆的名词。 相似文献
2.
《Journal of separation science》2003,26(8):647-652
The use of a poly(methylmethacrylate) capillary electrophoresis chip, provided with a high sample load capacity separation system (a 8500 nL separation channel combined with a 500 nL sample injection channel) and a pair of on‐chip conductivity detectors, for zone electrophoresis (ZE) determination of oxalate in beer was studied. Hydrodynamic and electroosmotic flows of the solution in the separation compartment of the chip were suppressed and electrophoresis was a dominant transport process in the separations performed on the chip. A low pH of the carrier electrolyte (3.8), implemented by aspartic acid and bis‐tris propane, provided an adequate selectivity in the separation of oxalate from anionic beer constituents and, at the same time, also a sufficient sensitivity in its conductivity detection. Under our working conditions, this anion could be detected at a 0.5 μmol/L concentration also in samples containing chloride (a major anionic constituent of beer) at a 1800 higher concentration. Such a favorable analyte/matrix concentration ratio made possible accurate and reproducible [typically, 2–5% relative standard deviation (RSD) values of the peak areas of the analyte in dependence on its concentration in the sample] determination of oxalate in 500 nL volumes of 20–50‐fold diluted beer samples. Short analysis times (about 200 s), minimum sample preparation, and reproducible migration times of this analyte (0.5–1.0% RSD values) were characteristic for ZE on the chip. 相似文献
3.
To develop a low cost and highly effective metallurgical route for solar-grade Si production, we investigated the zone melting directional solidification method. In this method, bulk crystalline Si is successfully produced from Si-Sn solvent; this bulk crystalline Si demonstrates a steady growth interface and excellent compositional uniformity. Moreover, the growth rate of bulk crystalline Si along the axial direction increases because the remaining MG-Si serves as Si source to keep the Si-Sn solution saturated with Si atoms, and it is approximately three times larger than that of Si by using the Si-based alloy directional solidification method without Si source. In this work, the evolution of impurity phases segregated in different regions along the axial direction is extensively discussed. The distribution and amount of impurities, including Ca, Al, B, and P, are effectively controlled by this refining method, further improving the quality of bulk crystalline Si. 相似文献
4.
C. J. Toussaint F. Bo 《International journal of environmental analytical chemistry》2013,93(1-2):55-67
Abstract In the framework of remote sensing studies concerning coastal transport of pollution in the Northern Adriatic Sea, a method has been developed for the quantitative determination of sulphur, iron, titanium, calcium, phosphorus, silicon, aluminium, magnesium in suspended matter of sea water. The suspended material was collected by filtering on millipore membrane filters with pore width of 0.45 μ and directly analysed by X-ray spectroscopy. For calibration dried solution and particulate standard samples were used. Limits of sensitivity and precision of the method are reported. Correlations between the concentration of these elements and the total suspended matter/chlorophyll are discussed. The aim is to study the geochemical composition of particulate matter and its variations within the geographical site of the sea basin and the seasonal conditions. The approach is to consider aluminium and the other elements normalized on Al. On the basis of a matrix correlation analyses of some sets of data chosen in the restricted area for investigation, some hypothesis on superficial distribution of clay, carbonate, iron hydrous oxides and other mineral detrites, are taken into account. The results confirm the complex situation existing in the offshore area of the Venice lagoon from a geochemical point of view. The suspended matter seem to be argillaceous in the Southern part of the investigated area and semi-argillaceous with hydrous oxides and carbonates in the Northern part which is influenced by the Piave river. 相似文献
5.
Simultaneous and Fast Detection of Anions in Snow Using Short Tube by Capillary Zone Electrophoresis
Weiping Yang Zhujun Zhang 《International journal of environmental analytical chemistry》2013,93(6):353-360
A capillary zone electrophoresis (CZE) method applied short-effective length of capillary (11 cm) and low separation voltage (5 kV) was developed for the fast and quantitative determination of Cl m , $ {\rm NO}_2^ - $ , $ {\rm SO}_4^{2 - } $ , $ {\rm NO}_3^ - $ , $ {\rm HCO}_3^ - $ in snow sample. Baseline separation of inorganic anions and organic anions was achieved within 55 s. Indirect absorbance detection of anions was accomplished with a chromate - based background electrolyte modified with cetyltrimethylammonium bromide (CTAB) and acetonitrile at pH 9.5. The effect of the pH, the concentration of electrolyte and modifiers on the resolution was investigated. The application of electrokinetic injection using butyric acid as internal standard created the described method fast, sensitive, and quantitative, with good relative standard deviation (RSD), for migration times from 0.1 to 0.3% and for peak areas from 1.8 to 4.0%. The limits of detection (LOD) were 0.03 mg L m 1 Cl m , 0.1 mg L m 1 $ {\rm NO}_2^ - $ , 0.07 mg L m 1 $ {\rm SO}_4^{2 - } $ , 0.08 mg L m 1 $ {\rm NO}_3^ - $ , 0.05 mg L m 1 F m , and 0.2 mg L m 1 $ {\rm HCO}_3^ - $ , respectively. Standard addition recoveries of Cl m , $ {\rm NO}_2^ - $ , $ {\rm SO}_4^{2 - } $ , $ {\rm NO}_3^ - $ , F m , and $ {\rm HCO}_3^ - $ in snow sample were between 91 and 104%. This method has been shown promising results for the determination of small anions in snow sample. 相似文献
6.
Yacine Boulfrad Antti Haarahiltunen Hele Savin Eivind J.
vrelid Lars Arnberg 《Progress in Photovoltaics: Research and Applications》2015,23(1):30-36
The deteriorated area of the multicrystalline silicon (mc‐Si) ingots grown by directional solidification, commonly known as the Red Zone, is usually removed before wafering. This area, characterized by poor minority carrier lifetime, is located on the sides, at the top, and the bottom of the mc‐Si ingots. In this study, the effect of internal gettering by oxygen precipitates and structural defects has been investigated on the bottom zone of a mc‐Si ingot. Nucleation and growth of oxygen precipitates as well as low temperature annealing were studied. Photoluminescence imaging, lifetime mapping, and interstitial iron measurements performed by μ‐PCD reveal a considerable reduction of the bottom Red Zone. An improvement of lifetime from below 1 µs to about 20 µs and a reduction of interstitial iron concentration from 1.32 × 1013 at/cm3 to 8.4 × 1010 at/cm3 are demonstrated in this paper. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
7.
Wang Jinsong Qi Wenfeng 《电子科学学刊(英文版)》2007,24(3):301-304
In an Approximately Synchronized Code Division Multiple Access (AS-CDMA) communication system, a family with large number of Zero Correlation Zone (ZCZ) sequences is desired, which can satisfy the rapid increase of users. This paper presents a method to generate a (2L,2M, ZCZ')-ZCZ sequence family from an original (L,M,ZCZ)-ZCZ sequence family, where ZCZ' = ZCZ if ZCZ is even and ZCZ' =ZCZ - 1 if ZCZ is odd. This method can also recursively act on a ZCZ sequence family to construct a series of ZCZ sequence families with large sequence number and zero correlation zone length identical to or one less than that of original ZCZ sequences. 相似文献
8.
9.
基于菲涅尔区修正结构的多波束自适应天线 总被引:8,自引:3,他引:8
菲涅尔区相位修正结构具有类似于二次曲面的聚焦特性和更好的偏轴扫描特性,将该结构与馈源阵列相组合,并通过用改进的LMS算法对馈源阵列输出的自适应信号处理,实现了对来波方向的估计和数字波束形成,从而构成了一类新型的多波束自适应天线。计算机模拟的有关结果证实了其可行性。 相似文献
10.
LIGA技术制作Fresnel波带片的研究 总被引:2,自引:0,他引:2
简要介绍了利用LIGA技术中同步辐射光刻、微电铸技术制作α粒子编码成像波带片的研究,讨论了编码波带片的结构和影响波带片的平面和层析分辨率的参数。根据实验要求设计和研制了一种α粒子编码成像波带片。 相似文献