A simple,rapid and sensitive method based on modified multiwalled carbon nanotube for preconcentration and determination of lead ions in aqueous media in natural pHs

In this study, multiwalled carbon nanotube (MWCNT) was modified by the pyridine group using a silane agent and characterized by infrared spectroscopy (IR), thermal analysis (TG/DTA), and elemental analysis (CHN) and scanning electron microscopy (SEM). The application of this sorbent was investigated in determination of lead ions in aqueous samples, using flame atomic absorption spectrometry (FAAS). Through this study, different parameters such as pH and sample flow rate on adsorption process and eluent concentration, volume and flow rate were optimized. The limit of detection (LOD), the relative standard deviation and the recovery of the method were 2 ng mL^?1, 1.3% and 99.7%, respectively. Two standard reference materials (NIST 1571 and NIST 1572) were used to verify accuracy of this method. Finally, the sorbent was successfully applied for extraction and determination of low levels of Pb(II) ions in aqueous samples.     

Gas-phase 21Ne NMR studies and the nuclear magnetic dipole moment of neon-21

Gas-phase ²¹Ne nuclear magnetic resonance spectra were measured at the natural abundance of ²¹Ne isotope for samples consisting of pressurized neon up to 60 bar at room temperature and applying the magnetic field of the strength B₀ = 11.7574 T. It showed that the nuclear magnetic resonance frequency is linearly dependent on the density of gaseous neon. The resonance frequency was extrapolated to the zero-density point, and it permitted the determination of the ²¹Ne nuclear magnetic moment, μ(²¹Ne) = 0.6617774(10) μ_N. The present value of μ(²¹Ne) is not influenced by the bulk magnetic susceptibility of neon and interactions between neon atoms; therefore, it is more precise and reliable than the previous result obtained for μ(²¹Ne).     

码流分析仪在有线数字电视系统中的应用

论述数字电视系统的关键技术，对传输码流参数进行分析，提出码流分析仪在有线数字电视系统中的应用方法。     

基于MPEG-2文件的合并

介绍了具有相同音频、视频编码方式的MPEG - 2节目流如何合并成一个节目流。合并后的文件播放流畅并且时间显示正确 ,它包括PATPMT表的重写 ,系统头部分相关字段的更改 ,PCR值的修改 ,解码时间标签 (DTS)和显示时间标签 (PTS)的重新确定 ,传送速率的修改以及添加相应的空包     

MPEG-4 AAC解码器在NIOS Ⅱ平台上的实现和优化

给出了MEPG-4AAC实时解码器在NIOSⅡ平台的实现方案，介绍了MPEG-4AAC—LC解码算法及各关键模块优化算法。在完成实时解码要求下，结合NIOSⅡ平台特性，对解码器在软件代码与处理器上进行优化。实验结果表明CPU时钟为80MHz时能达到实时解码要求。     

HE-AAC V2编码原理及其应用

在保证优秀的音频质量下,提高音频编码的压缩效率是数字音频技术一直追求的目标,简单介绍目前最先进的音频编码HE-AAC V2的原理及应用,着重介绍其中用到的两种新技术频带复制(SBR)技术和参数立体声(PS)技术.     

实时硬件系统中控制方法的研究

由于实时硬件系统的规模和复杂度不断增大，系统结构的模块化设计已成为硬件系统开发的发展趋势。研究了硬件系统中模块控制的方法和特点。结合MPEG2电视编码器中各功能模块的特点，提出了适合该硬件系统的模块控制方案，说明了控制模块的硬件设计思想和软件实现。实践证明，该方案满足系统实时性和可靠性的设计要求。     

基于ADSP21XXC运行环境下FFT的实现

介绍了数字信号处理器ADSP21XX芯片的特点以及实现FFT(快速离散付里叶变换)的方法，给出了ADSP21XX的C和汇编混合编程的特点及技巧。     

MPEG-4视频编码技术及其在多媒体通信中的应用

本文较为详细地介绍了MPEG－4视频编码的主要技术及其功能与特点，并基于此标准提出了一个基于Internet网络的多媒体通信系统的设计方案。     

基于PNX1300系列多媒体处理器的MPEG-4视频压缩卡设计

介绍了一种基于MPEG—4视频压缩标准和PNX1300系列多媒体处理器的MPEG—4视频压缩卡的设计方案，给出了该视频压缩卡的硬件结构框图，详细分析了其软件编码器的设计流程。