ICP-AES测定钛基复合材料中镍、钕和铁的研究

采用ICP－AES法对钛基复合材料中的合金元素镍、钕、铁的测定进行了研究，着重进行了基体元素及待测元素镍、钕、铁之间干扰试验及各元素在测定浓度范围内的线性相关性试验，进行了酸度试验，测定了钛基复合材料中3种元素的含量，得到了较好的精密度和准确度。方法简便、可靠，获得满意的分析结果。     

Structural optimization design for large mirror

The system design must be started from the concept with low cost and high performance. In this point, the topological shape of the structure is very important in the view of the structural rigidities and light-weight design.In this paper, the optimization methodology is presented in the design stage of the large optical mirror. We obtain the optimal layout through the topology optimization and then design the details through the size or shape optimization for structural rigidity.     

GaAlInP发光材料计算的经验公式

根据已经发表的实验数据，针对镓铝铟磷发光材料的提出了一组经验公式及相应的曲线，作为ＧａＡｌＩｎＰ可见光材料设计的依据或参考。     

The analysis of thermal stresses in thermopiezoelastic semi-infinite body with an edge crack

Summary  Thermopiezoelastic materials have recently attracted considerable attention because of their potential use in intelligent or smart structural systems. The governing equations of a thermopiezoelastic medium are more complex due to the intrinsic coupling effects that take place among mechanical, electrical and thermal fields. In this analysis, we deal with the problem of a crack in a semi-infinite, transversely isotropic, thermopiezoelastic material by means of potential functions and Fourier transforms under steady heat-flux loading conditions. The problem is reduced to a singular integral equation that is solved. The thermal stress intensity factor for a crack situated in a cadmium selenide material is calculated. Received 20 March 2001; accepted for publication 18 October 2001     

双极型静电感应晶体管开关时间的测量与分析

从理论和实验两方面对静电感应晶体管（ＢＳＩＴ）的开关时间进行了分析和测量，提出了简单的分析方法，将影响ＢＳＩＴ开关时间的各个因素归结为结构因子和材料因子，从而简化了分析影响ＢＳＩＴ开关时间的因素，对于ＢＳＩＴ的实际工艺，结构设计有指导意义。     

Development of a Millimeter Wave Compact Equipment for NDT of Materials

We developed a compact equipment working at 94 GHz to replace the commonly used network analyzer for nondestructive testing of materials. The compact equipment was designed to measure the variations in the amplitude and phase of the reflected signal from the material relative to a reference signal. A good accuracy of the amplitude and phase measurement of the equipment was obtained in the confirmative experiments. The distribution of a drop of water in a wood plate is clearly visible in the millimeter wave images obtained by the amplitude and phase measurement.     

Dependence of surface morphology of CVD diamond films on deposition conditions

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Remarks on the sample preparation of oxidic materials for X-ray analysis

Summary The universal method which is established in practice and has the best reproducibility is indicated in a critical comparison of different techniques for producing melting fusion tablets for the X-ray analysis. By studying fusion tablets with methods of local analysis, users of the tablet technique shall be made critical. The different objectives of analytical problems with the analysis of oxides are discussed.

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Bemerkungen zur Probenvorbereitung oxidischer Materialien für die Röntgenfluorescenzanalyse

Zusammenfassung Ausgehend von einem kritischen Vergleich verschiedener Techniken zur Herstellung von Schmelzaufschluß-Tabletten für die RFA wird auf die in der Praxis bewährte Universalmethode mit der besten Reproduzierbarkeit hingewiesen. Durch die Untersuchung von Schmelztabletten mit Hilfe lokalanalytischer Methoden sollen Anwender der Tablettentechnik zur Kritik angeregt werden. Die unterschiedlichen Zielsetzungen analytischer Aufgaben bei der Untersuchung von Oxiden werden diskutiert.

     

Initiation of polymer degradation via transfer of infectious species

A novel dual stage chemiluminescence detection system incorporating individually controlled hot stages has been developed and applied to probe for material interaction effects during polymer degradation. Utilization of this system has resulted in experimental confirmation for the first time that in an oxidizing environment a degrading polymer A (in this case polypropylene, PP) is capable of infecting a different polymer B (in this case polybutadiene, HTPB) over a relatively large distance. In the presence of the infectious degrading polymer A, the thermal degradation of polymer B is observed over a significantly shorter time period. Consistent with infectious volatiles from material A initiating the degradation process in material B it was demonstrated that traces (micrograms) of a thermally sensitive peroxide in the vicinity of PP could induce degradation remotely. This observation documents cross-infectious phenomena between different polymers and has major consequences for polymer interactions, understanding fundamental degradation processes and long-term aging effects under combined material exposures.     

The determination of adsorbable organically bound halogens (AOX) in soil: interlaboratory comparisons and reference materials

The interlaboratory variability in the quantification of adsorbable organically bound halogens (AOX) in industrially contaminated soil is presented. Three consecutive rounds of a proficiency testing scheme, in which between 88 and 119 routine laboratories participated, yielded relative reproducibility standard deviations between 7 and 20% at AOX contents between 10.9 and 268 mg kg⁻¹. Nineteen laboratories with established proficiency were invited to participate in the certification of the AOX content in three soil reference materials meant for the internal quality control in analytical laboratories. The certified values are (1349 ± 59) mg kg⁻¹, (80 ± 7) mg kg⁻¹ and (102 ± 8) mg kg⁻¹, respectively.