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《Arabian Journal of Chemistry》2022,15(7):103933
In this study, a fingerprint-activity relationship modeling between chemical fingerprints and antirheumatic activity was established, and multivariate statistical analysis was used to evaluate the quality of Taxilli Herba (TH) from different hosts. Characteristic fingerprints of 20 batches of TH samples were generated by high-performance liquid chromatography coupled with triple quadrupole-time of flight tandem mass spectrometry (HPLC-Triple TOF-MS/MS), and the similarity analysis was calculated based on thirteen common characteristic peaks by hierarchical clustering analysis (HCA). Subsequently, nine efficacy markers were discovered by combining fingerprints and antirheumatic activity through grey correlation analysis (GCA) and bivariate correlation analysis (BCA). Meanwhile, the content of 5 constituents in 9 markers was determined by high-performance liquid chromatography coupled with triple quadrupole-linear ion trap tandem mass spectrometry (HPLC-QTRAP-MS/MS). The comprehensive quality of TH was assessed using multivariate statistical analysis, including principal components analysis (PCA) and technique for order preference by similarity to ideal solution (TOPSIS). The results showed that a high dose of TH extract could markedly ameliorate arthritis damage compared to other doses, with flavonoids playing an important role in the antirheumatic activity. The comprehensive quality of samples from Morus alba L. (SS) was superior to those from Liquidambar formosana Hance (FXS). The present study will demonstrate the markers associated with efficacy, and provide an applicable strategy for more comprehensive quality control and evaluation of TH. 相似文献
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Micro X-ray fluorescence spectrometry (μXRF) is a standard technique used for the elemental analysis of glass fragments in forensic casework. The glass specimens encountered in casework are usually small (<1 mm), thin fragments that are partially transparent to the exciting X-ray beam. In addition to providing fluorescence from the small glass fragments, the primary beam X-rays can scatter within the chamber and provide noise in the measurements. To reduce scatter from the sample stage, the fragments are typically mounted on a thin plastic film and raised on an XRF sample cup (≤3 cm in height). However, at these heights, there may still be significant scatter from the sample stage, which adversely affects the signal-to-noise ratio (SNR) and the limit of detection (LOD). A plastic mount was designed and 3D-printed in-house to allow fragments to be raised as high as possible from the sample stage, thereby minimizing stage scatter. Most elements detected in glass showed an improvement in the SNR when using the 3D-printed mount for analyses. The greatest improvement (>30%) was observed for lower atomic number elements (Na and Mg) and higher atomic number elements (Sr and Zr). Another simple method to improve SNR is the use of primary beam filters; when using primary beam filters during analyses, elements with characteristic lines in the high-energy range (Rb, Sr, and Zr) showed the greatest improvement (>70%) in SNR. The impact of both strategies for the improvement of SNR is presented here. 相似文献
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Stochastic resonance in a time-delayed asymmetric bistable system with mixed periodic signal
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This paper studies the phenomenon of stochastic resonance
in an asymmetric bistable system with time-delayed feedback and
mixed periodic signal by using the theory of signal-to-noise ratio
in the adiabatic limit. A general approximate Fokker--Planck
equation and the expression of the signal-to-noise ratio are derived
through the small time delay approximation at both fundamental
harmonics and mixed harmonics. The effects of the additive noise
intensity $Q$, multiplicative noise intensity $D$, static asymmetry
$r$ and delay time $\tau$ on the signal-to-noise ratio are
discussed. It is found that the higher mixed harmonics and the
static asymmetry $r$ can restrain stochastic resonance, and the
delay time $\tau $ can enhance stochastic resonance. Moreover, the
longer the delay time $\tau $ is, the larger the additive noise
intensity $Q$ and the multiplicative noise intensity $D$ are, when
the stochastic resonance appears. 相似文献
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通过分析耦合参数作用、系统所呈现大尺度周期相态的复杂性以及与系统在无噪声条件下状态的比较,得出耦合振子系统的动力学行为比同类单振子系统的复杂,周期相态更稳定、抗噪能力更强.用构造的一类含特定恢复力项双中强度耦合Duffing振子系统检测色噪声背景中的谐波、方波信号,信噪比分别达到-111.0和-108.45dB.
关键词:
特定双耦合 Duffing振子系统
色噪声
周期信号
信噪比 相似文献
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Stochastic resonance in an asymmetric bistable system driven by coloured correlated multiplicative and additive noise
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This paper investigates the stochastic resonance (SR) phenomenon in an asymmetric system with coupling between multiplicative and additive noise when the coupling between two noise terms is coloured. The approximate expression of signal-to-noise ratio has been obtained by applying the two-state theory and SR exhibits in the bistable system. Moreover, the potential asymmetry r and cross-correlation strength λ can weaken the SR phenomenon, while the cross-correlation time r can strengthen the SR phenomenon. 相似文献