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1.
This paper deals with the small-angle neutron scattering (SANS) investigation on solution-quenched PH13-8 Mo stainless steel.
From the nature of the variation of the functionality of the profiles for varying specimen thickness and also from the transmission
electron microscopy (TEM), it has been established that the small-angle scattering signal predominantly originates from the
block-like metallic carbide precipitates in the specimen. The contribution due to double Bragg reflection is not significant
in the present case. The single scattering profile has been extracted from the experimental profiles corresponding to different
values of specimen thickness. In order to avoid complexity and non-uniqueness of the multi-parameter minimization for randomly
oriented polydisperse block-like precipitate model, the data have been analyzed assuming randomly oriented polydisperse cylindrical
particle model with a locked aspect ratio. 相似文献
2.
The oxide films formed on AISI 304L stainless steel at 300 °C in the oxidation time range between 2 and 4 h have been studied by photoelectrochemistry. Photocurrents were investigated as a function of the wavelength of the incident light and the electrode potential. The investigation allowed the determination of the semiconductive properties of the oxides. The oxide films showed n-type behaviour. A duplex structure of the oxide films has been suggested on the basis of the photocurrent spectra, with an internal oxide layer having an optical gap (Eg2 = 2.16-2.3 eV) depending on the applied potential and oxidation time, higher to that of the external oxide layer (Eg1 ≈ 1.9 eV). Significant variations in the amplitude of the photocurrent were detected as a function of the applied potential and the oxidation time. 相似文献
3.
采用光学显微镜和扫描电子显微镜等手段,对某轻型汽车40Cr后桥半轴断裂件的组织及断口特征进行了分析结果表明:半轴在调质处理时的淬火温度不够高,使其表层和心部组织中存在较多的铁素体相,造成了工件最终的硬度和疲劳强度不足,导致半轴在使用中发生扭转疲劳断裂. 相似文献
4.
Low-loss and rugged distal tips for CO2 laser have been proposed and fabricated based on a commercially available stainless steel (St) pipe. A method of smoothening the inner surface of the St pipe with a rough inner surface is put forward. Fabrication parameters, transmission properties, and mechanical strength of the cyclic olefin polymer-coated silver hollow St distal tip are experimentally discussed. 相似文献
5.
采用有限元方法对大型钢结构人行景观天桥进行了静力学、温度应力、动力学模态和初步的抗震能力分析,并就桥自重作用下的最大竖向位移和实际观测结果进行了比较,两者是一致的.计算结果表明:人行景观天桥在常规、温度极值改变和多遇地震荷载作用等多种工况下,现有的设计方案具有足够的强度、刚度和抗震能力. 相似文献
6.
Mössbauer spectroscopy was used to investigate the influence of dissolved hydrogen on the interatomic bonds in austenitic steels. It was carried out to prove the decohesion mechanism of hydrogen embrittlement (HE). It is shown that hydrogen increases Debye temperature, i.e., the interatomic bonds in hydrogenated austenitic steel becomes stronger. 相似文献
7.
The efficiency of 3,5-bis(n-pyridyl)-1,3,4-oxadiazole (n-POX, n = 1, 2, 3), as corrosion inhibitors for mild steel in 1 M perchloric acid (HClO4) have been determined by weight loss measurements and electrochemical studies. The results show that these inhibitors revealed a good corrosion inhibition even at very low concentrations. Comparison of results among those obtained by the studied oxadiazoles shows that 3-POX was the best inhibitor. Polarisation curves indicate that n-pyridyl substituted-1,3,4-oxadiazoles are mixed type inhibitors in 1 M HClO4. The adsorption of these inhibitors follows a Langmuir isotherm model. The electronic properties of n-POX, obtained using the AM1 semi-empirical quantum chemical approach, were correlated with their experimental efficiencies using the linear resistance model (LR). 相似文献
8.
35Cr25Ni12奥氏体耐热钢中碳化物的电子显微分析 总被引:1,自引:0,他引:1
应用扫描电镜(SEM)和透射电镜(TEM)研究了长期使用前后的35Cr25Ni12奥氏体耐热钢中的碳化物演变行为;该钢固溶时效后的组织由初晶奥氏体及M23C6共晶碳化物组成,奥氏体基体中析出了二次M23C6,二次碳化物总是与基体保持立方-立方取向关系;长期使用(3、5年)后,奥氏体中析出的二次碳化物量明显增加,部分M23C6已转变为M6C,M6C与奥氏体基体以及二次碳化物M23C6保持[001]M6C//[221]A//[221]M23C6孪晶取向关系。 相似文献
9.
新型的不锈钢镀Pt(Ir)电极 总被引:1,自引:0,他引:1
应用欠电位沉积与锚定效应,研制了一种新型的不锈钢镀Pt(Ir)电极,此电极具有优越的电化学特性,可望用于微传感器。 相似文献
10.
Rebuilding of metal components with laser cladding forming 总被引:4,自引:0,他引:4
Laser cladding forming (LCF) is a novel powerful tool for the repairing of metal components. Rebuilding of V-grooves on medium carbon steel substrates has been carried out with laser cladding forming technique using stainless steel powder as the cladding material. Microstructure of the deposited layers has been characterized using optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive X-ray microanalysis (EDAX), electron probe microanalysis (EPMA) and X-ray diffraction (XRD). Mechanical properties of the rebuilt V-groove samples have been evaluated by tensile and impacting tests and microhardness measurement. Experimental results show that good fusion bonding between the rebuilt layers and the substrate has been formed, and the microstructure of the cladding layers is mainly composed of fine, dense and defect-free epitaxial columnar dendrites. Due to the effect of grain size refinement, the tensile strength, impacting toughness, elongation and microhardness of the rebuilt samples have been greatly enhanced compared to those of the substrate. Microhardness is also very uniform throughout the rebuilt regions. With the growth of the deposited layers, the microhardness increases gradually. The good ductility of the deposited regions is verified by the SEM fracture analysis. 相似文献