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1.
《Arabian Journal of Chemistry》2021,14(11):103421
Processing of Carapa guianensis seeds to obtain oil on an industrial scale generates a significant amount of by-product, approximately 66% w/w, which is called cake and is a potential source of biomolecules, including simple phenolic structures. For this reason, studies were carried out on the chemical profiles of hydrolyzed extract from this agro-industrial by-product through High Performance Thin-Layer Chromatography (HPTLC) and Gas Chromatography coupled to Mass Spectrometry (GC–MS). These techniques were used to detect metabolic classes and/or groups, and to identify, for the first time, thirteen simple phenolic acids in this by-product. The sample antioxidant capacity was determined by methods of 2,2-diphenyl-1-picrylhydrazyl (DPPH)and 2,2′-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) diammonium salt (ABTS+) radicals direct sequestration. The hydrolyzed fraction showed a total of 63.47% in the relative abundance of the total of compounds, standing out: p-hydroxybenzoic acid (39.19%) and protocatechuic acid (3,4-dihydroxybenzoic acid) (5.62%), both from hydroxybenzoic acids and 3-(3,4-dihydroxyphenyl)lactic acid, (7.76%) hydroxycinnamic acids derivatives. In these results, the fraction rich in simple phenolic acids was obtained, attributing the prominent behavior of this matrix antioxidant activity, expressed by (IC50: of 16.42 µg/mL and 6.52 µg/mL for DPPH and ABTS+ radicals, respectively). The research demonstrated an alternative to applicability that involves sustainability from agro-industrial. These techniques were used to detect metabolic classes and/or groups, and to identify, for the first time, thirteen simple phenolic acids in this by-product, generating a process capable of converting biomass into a bioproduct, consisting of bioactive compounds, in addition to adding value to the industrial chain. 相似文献
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Efficient measurement of the performance index (the distance of a loading parameter from the voltage collapse point) is one of the key problems in power system operations and planning and such an index indicates the severity of a power system with regard to voltage collapse. There exist many interesting methods and ideas to compute this index. However, some successful methods are not yet mathematically justified while other mathematically sound methods are often proposed directly based on the bifurcation theory and they require the initial stationary state to be too close to the unknown turning point to make the underlying methods practical.This paper first gives a survey of several popular methods for estimating the fold bifurcation point including the continuation methods, bifurcation methods and the test function methods (Seydel's direct solution methods, the tangent vector methods and the reduced Jacobian method) and discuss their relative advantages and problems. Test functions are usually based on scaling of the determinant of the Jacobian matrix and it is generally not clear how to determine the behaviour of such functions. As the underlying nonlinear equations are of a particular type, this allows us to do a new analysis of the determinants of the Jacobian and its submatrices in this paper. Following the analysis, we demonstrate how to construct a class of test functions with a predictable analytical behaviour so that a suitable index can be produced. Finally, examples of two test functions from this class are proposed. For several standard IEEE test systems, promising numerical results have been achieved. 相似文献
4.
在计算机视觉理论基础上发展起来的视觉检测(vision inspection)技术具有非接触、速度快、精度适中、可实现在线等优点,已广泛地应用于工业产品的在线检测。在计算机视觉检测技术中CCD摄像机是一个最关键的器件,其参数是否准确决定了检测的精度。所以,摄像机标定是视觉检测技术中最基本的也是最重要的一步。在比较其他标定方法的基础上,为了解决传统标定方法对螺纹图像测量系统所带来的一系列问题,采用了一种新的图像测量系统的标定方法——网格式平行线标定方法,该方法运用了CCD亚像素细分技术及调焦技术,可直接得到纵横2个方向的像素,经过理论分析及实验结果均表明,采用该方法具有标定简单、精度高、重复性好等优点,是一种较好的螺纹图像测量系统标定方法。 相似文献
5.
Yoshikazu Takada 《Annals of the Institute of Statistical Mathematics》1998,50(2):325-335
This paper gives a condition which implies the nonexistence of parametric statistical procedures with bounded risk or error performance characteristics. Many examples for which such a condition is satisfied are considered. 相似文献
6.
Vasily L. Morgunov 《Pramana》2007,69(6):1097-1100
A new calorimeter energy calibration method was developed for the proposed ILC detectors. The method uses the center-of-mass
energy of the accelerator as the reference. It has been shown that using the energy conservation law it is possible to make
ECAL and HCAL cross calibration to reach a good energy resolution for the simple calorimeter energy sum.
相似文献
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江汉平原上空QTEC变化特征的统计分析 总被引:1,自引:0,他引:1
提出了一种观测台网用多接收机性能一致性的标定方法,并利用江汉平原GPS接收台网的观测数据,分析了该地区上空QTEC的日变化、季节变化、年变化和逐年变化的统计特征.标定结果表明,不同接收机之间的仪器偏差是从双频GPS卫星信标推算QTEC的主要误差来源之一,必须校正.统计分析证实,江汉平原上空QTEC的日变化特征同时受电离层和等离子层控制,其年变化以半年周期为主,峰值和谷值分别出现在两分点和两至点附近,QTEC值的逐年变化从太阳活动峰年到低年逐年下降,与以太阳黑子数为代表的太阳活动密切相关. 相似文献
9.
This paper examines the performance of Commodity Trading Advisors (CTAs) using fixed and variable benchmarking models. In
order to avoid the troublesome passive and active commodity and managed futures benchmarks (indices) when examining the performance
of CTAs, we innovate by using data envelopment analysis (DEA). Because this alternative class has non-linear returns due to
long/short positions, and derivatives (i.e., dynamic trading strategies), DEA can alleviate the problems usually associated
with these indices. The effectiveness of using benchmarking models in a DEA setting will provide investors with an alternative
technique in assessing the performance and identifying efficient CTAs. 相似文献
10.
由于储存环中各种元件误差的存在, 机器的实际运行模式与设计模式有一定的偏差. 目前广泛开展的响应矩阵方法研究, 可以分析出磁铁元件以及束流位置测量元件的误差, 使束流基本参数得到校正. 介绍了用响应矩阵分析方法, 在BEPC储存环上进行的局部轨道校正的实验研究, 以及BEPC储存环束流参数校正的模拟研究. 相似文献