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1.
R.?Mitchell C.?M.?CarrEmail author M.?Parfitt J.?C.?Vickerman C.?Jones 《Cellulose (London, England)》2005,12(6):629-639
The surface chemical composition of raw unscoured cotton was successfully investigated by the surface analytical techniques
X-ray Photoelectron Spectroscopy (XPS) and Time of Flight Secondary Ion Mass Spectrometry (ToF-SIMS). The presence of non-cellulosic
material at the fibre surface was established and determined to be a complex mixture of fatty acids, alcohols, alkanes, esters
and glycerides. The effect of scouring and bleaching was to reduce the surface concentration of these materials but even after
aqueous processing some non-cellulosic material residue was still detected at the fibre surface. 相似文献
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为了评估某型机载瞄准系统的精度,根据飞行试验参数测试需要,提出了通过图像测量与DGPS融合处理方法进行瞄准精度评估的试验方案。该方案利用飞行试验获取的图像数据与其他测量数据相结合,建立精度评估的方法,该评估方法在该机载武器瞄准系统精度评估得到应用,并且可在同类试验课题中推广应用。 相似文献
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Blokland MH Zoontjes PW Sterk SS Stephany RW Zweigenbaum J van Ginkel LA 《Analytica chimica acta》2008,618(1):86-93
The use of accurate mass measurement as a confirmation tool is examined on a TOF-MS and compared with confirmation using a triple quadrupole mass spectrometer (QqQ-MS). Confirmation of the identity of a substance using mass-spectrometric detection has been described. However, the use of accurate mass measurement for confirmatory analysis has not been taken into account. In this study, criteria for confirmation with accurate mass are proposed and feasibility is demonstrated. Mass accuracy better than 3 ppm of the quasi-molecular ion and a fragment and their relative ratios determined with LC/TOF-MS are compared to the criteria of two transition ions and their ratio of LC/QqQ-MS. The results show that these criteria can be met for Trenbolone in samples of bovine urine and that single MS accurate mass measurement is comparable to nominal mass MS/MS for confirmation. The increase in popularity and availability of LC/TOF-MS instruments and the ease, of which exact masses can be measured, make it important to formulate criteria for this type of instrumentation. It is shown in this study that accurate mass measurement can be used for confirmatory analysis. However, more experiments need to be conducted to demonstrate the applicability of accurate mass measurement in general for residue analysis. 相似文献
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Dynamic flight stability of a model dronefly in vertical flight 总被引:1,自引:0,他引:1
The dynamic flight stability of a model dronefly in hovering and upward flight is studied.The method of computational fluid dynamics is used to compute the stability derivatives and the techniques of eigenvalue and eigenvector used to solve the equations of motion.The major finding is as following.Hovering flight of the model dronefly is unstable because of the existence of an unstable longitudinal and an unstable lateral natural mode of motion.Upward flight of the insect is also unstable,and the instability increases as the upward flight speed increases.Inertial force generated by the upward flight velocity coupled with the disturbance in pitching angular velocity is responsible for the enhancement of the instability. 相似文献
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Rapid multivariate analysis of 3D ToF‐SIMS data: graphical processor units (GPUs) and low‐discrepancy subsampling for large‐scale principal component analysis 下载免费PDF全文
Peter J Cumpson Ian W Fletcher Naoko Sano Anders J Barlow 《Surface and interface analysis : SIA》2016,48(12):1328-1336
Principal component analysis (PCA) and other multivariate analysis methods have been used increasingly to analyse and understand depth‐profiles in XPS, AES and SIMS. For large images or three‐dimensional (3D) imaging depth‐profiles, PCA has been difficult to apply until now simply because of the size of the matrices of data involved. In a recent paper, we described two algorithms, random vector 1 (RV1) and random vector 2 (RV2), that improve the speed of PCA and allow datasets of unlimited size, respectively. In this paper, we now apply the RV2 algorithm to perform PCA on full 3D time‐of‐flight SIMS data for the first time without subsampling. The dataset we process in this way is a 128 × 128 pixel depth‐profile of 120 layers, each voxel having a 70 439 value mass spectrum associated with it. This forms over a terabyte of data when uncompressed and took 27 h to process using the RV2 algorithm using a conventional windows desktop personal computer (PC). While full PCA (e.g. using RV2) is to be preferred for final reports or publications, a much more rapid method is needed during analysis sessions to inform decisions on the next analytical step. We have therefore implemented the RV1 algorithm on a PC having a graphical processor unit (GPU) card containing 2880 individual processor cores. This increases the speed of calculation by a factor of around 4.1 compared with what is possible using a fast commercially available desktop PC having central processing units alone, and full PCA is performed in less than 7 s. The size of the dataset that can be processed in this way is limited by the size of the memory on the GPU card. This is typically sufficient for two‐dimensional images but not 3D depth‐profiles without sampling. We have therefore examined efficient sampling schemes that allow a good approximate solution to the PCA problem for large 3D datasets. We find that low‐discrepancy series such as Sobol series sampling gives more rapid convergence than random sampling, and we recommend such methods for routine use. Using the GPU and low‐discrepancy series together, we anticipate that any time‐of‐flight SIMS dataset, of whatever size, can be efficiently and accurately processed into PCA components in a maximum of around 10 s using a commercial PC with a widely available GPU card, although the longer RV2 approach is still to be preferred for the presentation of final results, such as in published papers. Copyright © 2016 The Authors Surface and Interface Analysis Published by John Wiley & Sons Ltd 相似文献
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Walter Hohmann was a civil engineer who studied orbital maneuvers in his spare time. In 1925, he published an important book (Ref. 1) containing his main result, namely, that the most economical transfer from a circular orbit to another circular orbit is achieved via an elliptical trajectory bitangent to the terminal orbits. With the advent of the space program some three decades later, the Hohmann transfer maneuver became the most fundamental maneuver in space.In this work, we present a complete study of the Hohmann transfer maneuver. After revisiting its known properties, we present a number of supplementary properties which are essential to the qualitative understanding of the maneuver. Also, we present a simple analytical proof of the optimality of the Hohmann transfer and complement it with a numerical study via the sequential gradient-restoration algorithm. Finally, as an application, we present a numerical study of the transfer of a spacecraft from the Earth orbit around the Sun to another planetary orbit around the Sun for both the case of an ascending transfer (orbits of Mars, Jupiter, Saturn, Uranus, Neptune, and Pluto) and the case of a descending transfer (orbits of Mercury and Venus). 相似文献