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Dong Zheng Fu-Quan Wang Yuan-Guang Li Liang-Hong Guo Jing Cheng 《Analytica chimica acta》2004,508(2):225-231
Optimized combination of chemical agents was selected for sensitive electrochemical detection of dissolved ruthenium tris-(2,2′-bipyridine) (Ru-bipy). The detection was based on the chemical amplification mechanism, in which the anodic current of a redox-active analyte was amplified by a sacrificial electron donor in solution. On indium-doped tin oxide (ITO) electrodes, electrochemical reaction of the analyte was reversible, but that of the electron donor was greatly suppressed. Several transition metal complexes, such as ferrocene and tris-(2,2′-bipyridine) complexes of osmium, iron and ruthenium, were evaluated as model analyte. A correlation between the amplified current and the standard potential of the complex was observed, and Ru-bipy generated the largest current. A variety of organic bases, acids and zwitterions were assessed as potential electron donor. Sodium oxalate was found to produce the largest amplification factor. With Ru-bipy as the model analyte and oxalate as the electron donor, the analyte concentration curve was linear up to 50 μM, with a lower detection limit of approximately 50 nM. Preliminary work was presented in which a Ru-bipy derivative was attached to bovine serum albumin and detected electrochemically. Although the combination of Ru-bipy, oxalate and ITO electrode has been used before for electrochemiluminescent detection of Ru-bipy and oxalate, as well as electrochemical detection of oxalate, its utility in amplified voltammetric detection of Ru-bipy as a potential electrochemical label has not been reported previously. 相似文献
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凸序列不等式的控制证明 总被引:2,自引:0,他引:2
利用控制不等式理论简洁地证明了一类凸序列不等式 (包括著名的 Nanson不等式的几个推广 ) ,并给出若干应用 . 相似文献
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James Murdock 《Journal of Differential Equations》2004,205(2):424-465
Hypernormal forms (unique normal forms, simplest normal forms) are investigated both from the standpoint of foundational theory and algorithms suitable for use with computer algebra. The Baider theory of the Campbell-Hausdorff group is refined, by a study of its subgroups, to determine the smallest substages into which the hypernormalization process can be divided. This leads to a linear algebra algorithm to compute the generators needed for each substage with the least amount of work. A concrete interpretation of Jan Sanders’ spectral sequence for hypernormal forms is presented. Examples are given, and a proof is given for a little-known theorem of Belitskii expressing the hypernormal form space (in the inner product style) as the kernel of a higher-order differential operator. 相似文献
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INTERSECTION OF PRIME SUBMODULES AND DIMENSION OF MODULES 总被引:1,自引:0,他引:1
A.Azizi 《数学物理学报(B辑英文版)》2005,25(3):385-394
The aim of this paper is to study the conditions by which a P-prime submodule can be expressed as a finite intersection or union of P-prime submodules. Also corresponding to dimension and rank of modules, some equivalent conditions for a ring to be a Dedekind domain are given. 相似文献
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Song LI Guo Mao WANG Zhi Song LIU 《数学学报(英文版)》2005,21(6):1475-1486
The purpose of this paper is to investigate the mean size formula of wavelet packets in Lp for 0 〈 p ≤ ∞. We generalize a mean size formula of wavelet packets given in terms of the p-norm joint spectral radius and we also give some asymptotic formulas for the Lp-norm or quasi-norm on the subdivision trees. All results will be given in the general setting, 相似文献
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弱拓扑和强可容许拓扑之间的一个关系 总被引:2,自引:0,他引:2
本文对局部凸空间X及其对偶X′,建立了弱拓扑σ(X,X′)和强拓扑β(X,X′)之间的一个新关系,改进了有关(X,X′)--可容许拓扑全体上的不变性结果。 相似文献
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曾六川 《高等学校计算数学学报(英文版)》2003,12(1)
The purpose of this paper is to investigate the problem of approximating fixed points of non-Lipschitizian asymptotically pseudocontractive mappings in an arbitrary real Banach space by the modified Ishikawa iterative sequences with errors. 相似文献