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排序方式: 共有2149条查询结果,搜索用时 15 毫秒
1.
Leila Torkian Mostafa M. Amini Tayebeh Gorji Omid Sadeghi 《Arabian Journal of Chemistry》2019,12(7):1315-1321
In this study, multiwalled carbon nanotube (MWCNT) was modified by the pyridine group using a silane agent and characterized by infrared spectroscopy (IR), thermal analysis (TG/DTA), and elemental analysis (CHN) and scanning electron microscopy (SEM). The application of this sorbent was investigated in determination of lead ions in aqueous samples, using flame atomic absorption spectrometry (FAAS). Through this study, different parameters such as pH and sample flow rate on adsorption process and eluent concentration, volume and flow rate were optimized. The limit of detection (LOD), the relative standard deviation and the recovery of the method were 2 ng mL?1, 1.3% and 99.7%, respectively. Two standard reference materials (NIST 1571 and NIST 1572) were used to verify accuracy of this method. Finally, the sorbent was successfully applied for extraction and determination of low levels of Pb(II) ions in aqueous samples. 相似文献
2.
A Modified Quasi-Newton Method for Structured Optimization with Partial Information on the Hessian 总被引:2,自引:0,他引:2
This paper develops a modified quasi-Newton method for structured unconstrained optimization with partial information on the
Hessian, based on a better approximation to the Hessian in current search direction. The new approximation is decided by both
function values and gradients at the last two iterations unlike the original one which only uses the gradients at the last
two iterations. The modified method owns local and superlinear convergence. Numerical experiments show that the proposed method
is encouraging comparing with the methods proposed in [4] for structured unconstrained optimization
Presented at the 6th International Conference on Optimization: Techniques and Applications, Ballarat, Australia, December
9–11, 2004 相似文献
3.
考虑一个奇异摄动罗宾问题在Bakhvalov-Shishkin网格上的迎风差分策略,得到在改进的Shishkin网格上迎风策略是关于ε一致的一阶L∞模收敛的.数值实验证实了此理论结果,显示估计是稳健的. 相似文献
4.
摘要:本文在L_[0.1]~p空间给出了 Durrmeyer型修正的shepard算子D_n(f,x),对 f∈L_[0.1]~p,(p≥1),得到了下列的Jackson型估计:││D)n(f)-f││_p≤ C_(pλω)(f,n~(-1))p,λ≥2, Cω(f,n~(-1)logn)p,λ=2, C_(pλω)(f,n~(-1))p,1<λ<2, 相似文献
5.
Man Young Kim Seung Wook Baek 《Journal of Quantitative Spectroscopy & Radiative Transfer》2005,90(3-4):377-388
Radiative heat transfer in an axisymmetric enclosure with absorbing, emitting, and scattering medium is studied here by using the different methods such as MDOM, FVM, and MFVM with emphasis on the treatment of angular derivative term, which appears in curvilinear coordinates due to angular redistribution. After final discretization equation for MFVM is introduced by using the step scheme and directional weights, the present approach is validated by applying it to three different benchmarking problems with absorbing, emitting, and scattering medium. All of the results presented here support its accuracy as well as moderate efficiency. Finally, the present approaches are applied to a truncated cone-shaped enclosure as a body-fitted geometry case. 相似文献
6.
G. Perelman 《Journal of Differential Equations》2007,235(1):56-73
We exhibit a time reversible geometric flow of planar curves which can develop singularities in finite time within the uniform topology. The example is based on the construction of selfsimilar solutions of modified Korteweg-de Vries equation of a given (small) mean. 相似文献
7.
A time‐marching formulation is derived from the space–time integrated least squares (STILS) method for solving a pure hyperbolic convection equation and is numerically compared to various known methods. Copyright © 2004 John Wiley & Sons, Ltd. 相似文献
8.
用阳离子表面活性剂十四烷基三甲基溴化铵(C17H38NBr)对膨润土进行插层改性制备.配制浓度为2.35%十四烷基三甲基溴化铵溶液备用.在碘量瓶中称取3.04g膨润土,加入30mL超纯水、10mL十四烷基三甲基溴化铵溶液,制成土浆,放入微波炉中反应1min.产物经抽滤、洗涤、烘干、研磨,做FT-IR和DSC-TG分析.DSC曲线在500℃时有一明显的放热峰;TG曲线显示改性土的失重率有明显的增大.有机改性膨润土中确实含有大量有机物,改性成功. 相似文献
9.
Miao Changxing 《数学学报(英文版)》1997,13(2):247-268
We consider the scattering problem for the Hartree equation with potential |x|−1 in a space of dimensionn≥2. We prove the existence ofH
m
-modified wave operator for Hartree equation on a dense set of a neighborhood of zero inH
m
(ℝ
n
), meanwhile, we obtain also the global existence for the Cauchy problem of Hartree equation in a space of dimensionn≥2.
This project is supported by the National Natural Science Foundation of China, 19601005 相似文献
10.
Investigation of the electrocatalytic behavior of single-wall carbon nanotube films on an Au electrode 总被引:1,自引:0,他引:1
The voltammetric behavior of uric acid (UA) was studied with an Au electrode modified with single-wall carbon nanotubes (SWNTs). In 0.1 M HAc-NaAc buffer solution (pH 5.0), the SWNT-modified electrode shows high electrocatalytic activity toward UA oxidation. The electro-oxidation of UA is an irreversible diffusion-controlled process with a diffusion coefficient (D) of 8.85×10−6 cm2 s−1. The peak current increases linearly with the concentration of UA in the range of 4.0×10−6-7.0×10−4 M. The detection limit is 1.0×10−6 M. The SWNT was characterized with scanning electron microscopy (SEM). Furthermore, the SWNT-modified electrode has favorable electrocatalytic activity toward dopamine and norepinephrine. This SWNT-modified electrode can also separate the electrochemical responses of uric acid, norepinephrine and ascorbic acid. 相似文献