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1.
《Analytical letters》2012,45(15):1127-1132
Abstract

Disc electrophoresic can be used to determine if uncookee beef and beef products have Seen adulterated with meat from horses, hogs, deer, and buffalo.  相似文献   
2.
Cu(II) complexes have been synthesized from the Schiff base ligands derived from furfurlyidene-4-aminoantipyrine and aniline (L1)/p-nitroaniline (L2)/p-hydroxyaniline (L3). They were characterized using analytical and spectral techniques. All the Cu(II) complexes exhibit square planar geometry. The X-band ESR spectra of the copper complexes in DMSO solution at 300 and 77 K were recorded and their salient features are reported. The in vitro biological screening effects of the investigated compounds were tested against the bacterial species, Staphylococcus aureus, Escherichia coli, Klebsiella pneumoniae, Proteus vulgaris and Pseudomonas aeruginosa and fungal species, Aspergillus niger, Rhizopus stolonifer, Aspergillus flavus, Rhizoctonia bataicola and Candida albicans by serial dilution method. A comparative study of inhibition values of the Schiff base ligands and their complexes indicate that the complexes exhibit higher antimicrobial activity than the Schiff base ligands. Superoxide dismutase and reducing power activities of the copper complexes have also been studied. Depending on the molecular structure, the [CuL2(OAc)2] complex possess promising SOD mimetic activities.  相似文献   
3.
向日葵花盘经湿法消解,采用ICP-AES对其中钾、钙、钠、钡、铝、铬、铜、镁、铁、锰、镍、锶、锌13种元素进行测定.对光谱仪的工作条件及分析谱线等测定条件进行了选择,并进行了方法的回收率及精密度试验,其回收率在95%-122%之间.  相似文献   
4.
圆盘定理的改进与弱连对角占优矩阵   总被引:6,自引:1,他引:5  
本文对圆盘定理进行了改进,给出了特征值分布新的估计,由此引出了弱连对角占优矩阵,讨论了其基本性质,重点分析了该类矩阵的逆与分裂特征,证明了在该类矩阵条件下H-相容分裂是收敛分裂,并给出迭代矩阵谱半径的上界及SOR算法中参数ω的选取范围。  相似文献   
5.
一种高精度的增量式光学编码器   总被引:1,自引:0,他引:1  
梁雁冰  王胡顺 《光子学报》1998,27(11):1033-1037
本文介绍了一种14位增量式光学编码器,包括光学部分和电气部分的组成及工作原理。作为应用实例,还介绍了用单片机(MCU)对输出的编码进行计数并加以显示。  相似文献   
6.
To study the rock deformation with threedimensional model under rolling forces of disc cutter,by carrying out the circular-grooving test with disc cutter rollingaround on the rock,the rock mechanical behavior underrolling disc cutter is studied,the mechanical model of disccutter rolling around the groove is established,and the theory of single-point and double-angle variables is proposed.Based on this theory,the physics equations and geometricequations of rock mechanical behavior under disc cutters oftunnel boring machine(TBM) are studied,and then the balance equations of interactive forces between disc cutter androck are established.Accordingly,formulas about normalforce,rolling force and side force of a disc cutter are derived,and their validity is studied by tests.Therefore,a newmethod and theory is proposed to study rock-breaking mechanism of disc cutters.  相似文献   
7.
本文使用国产能量色散X射线荧光光谱仪对分析球团矿进行了方法试验研究,建立了适当的卫作条件,经试验,该方法速度快,精密度满足使用要求.  相似文献   
8.
A fully automated synthesizer was constructed and designed to perform high speed miniaturized syntheses of compound libraries using the SPOT technique. Utilizing magnetically controlled drop-on-demand ink jet nozzles, an r/phi array format of 2500 spots can be simultaneously dispensed from up to 24 separate reagent valves onto a rotating disc as the solid phase in less than three minutes. In addition, a complete wash station is on board allowing for fully programmable combinatorial syntheses without manual attention. A new carbon black/polypropylene composite solid phase disc was developed and tested for its functionalisation/loading, spot detection, durability and MALDI-TOF target capabilities. The carbon black/polypropylene composite was then successfully employed jointly as the solid phase in the syntheses of short peptide and PNA oligomers and as the target probe holder for MALDI-TOF measurement without transfer of the material. Several protocols for PNA syntheses were also investigated and an optimised PNA methodology for the carbon black/polypropylene composite is reported.  相似文献   
9.
1.IntroductionInthepresentpaper,wewillcontinuethestudyofHilbertmodules[1-5].LetHbeaHilbertspaceandAafunctionalgebra.WesaythatHisaHilbertmoduleoverAifthereisamultiplication(a,f)-affromAxHtoH,makingHintoanXmoduleandif,inaddition,theactionisjointlycontinuousinthesup-normonAandtheHilbertspacenormonH.ThecategoryHofallHilbertNmodulesisanaturalsettingfornumerousquestionsinoperatortheory.In[9],DouglasandPaulseninitiatedasystematicstudyofHilbertmodules'theywereabletotranslatemanyconceptsandpro…  相似文献   
10.
We construct a bijection from R2 to R2, which maps rectangles centered at the origin O onto ellipses centered at O, and preserves area. This bijection allows us to construct uniform and refinable grids on elliptic domains. Then, we combine a particular case of this bijection (i.e. that bijection that maps squares into circles) with another area preserving projection from R2 to a surface of revolution around Oz. This yields uniform and refinable grids on this surface of revolution. The lines of these grids are situated in horizontal planes, if they are images of squares centered at O. We consider the particular case of the hemisphere and show how the northern hemisphere of the Earth is projected onto a square. Thus, our equiareal maps can be useful for constructing geographical maps of one hemisphere of the Earth onto rectangles.  相似文献   
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