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排序方式: 共有126条查询结果,搜索用时 515 毫秒
1.
A spot test was implemented in a flow-injection system for the spectrophotometric determination of zinc in digests of plant materials. It is based on the influence of Zn2+ on the oxidation rate of 1-naphthylethylenediamine (NED) by hexacyanoferrate(III) under acidic conditions. In order to control the precipitate formation and to maintain the resulting suspension, a micellar medium was established by adding Triton X-100. The proposed system handles about 65 samples per hour, meaning 72 μg NED and 9.0 mg K3[Fe(CN)6] per determination. Baseline drift is usually <0.01 absorbance per hour and the analytical signals for 0.5-2.5 mg l−1 Zn range within ca. 0.07-0.45 absorbance. Linearity of the analytical curve is fair (r>0.999, n=6) and detection limit was estimated as 0.2 mg l−1 Zn. Results are precise (R.S.D.<1%, n=10) and in agreement with flame atomic absorption spectrometry and with certified values of standard reference materials. 相似文献
2.
Summary Electrography and paper chromatography were combined to analyse rapidly metallic alloys in an almost non destructive technique. Using anodic dissolution the sample is applied on the start point of the chromatographic paper. Known ketones-HCl-water mixtures are usually used as solvents to analyse electrospots of different alloys and metal coatings and a separate electrospottest is recommended for Cr. Results of qualitative analysis of some steels, Cu–Ni, and Pb alloys are presented. 相似文献
3.
为了获得较高的空间分辩率,设计了一种新型小束斑驻波电子直线加速器,该加速器取消了加速腔中的鼻锥结构,而在耦合腔中设置鼻锥结构。用狭缝法代替小孔法测得X射线源的焦斑尺寸为1.4mm。讨论了射线源焦点对成像质量的影响,分析了在高能条件下小孔法不适合用于焦点测量的物理原因,用4种测量方法测量了该高能X射线源的参数,测得该系统的成像极限分辩率为2.5 lp/mm,最后对实验结果进行了分析。 相似文献
4.
In a laser butt joint welding process,it is required that the laser beam focus should be controlled to follow the weld joint path accurately.Small focus wandering off the weld joint may result in insufficient penetration or unacceptable welds.Recognition of joint position offset,which describes the deviation between the laser beam focus and the weld joint,is important for adjusting the laser beam focus and obtaining high quality welds.A new method based on the magneto-optical(MO)imaging is applied to measure the micro weld joint whose gap is less than 0.2 mm.The weldments are excited by an external magnetic field,and an MO sensor based on principle of Faraday magneto effect is used to capture the weld joint images.A sequence of MO images which are tested under different magnetic field intensities and different weld joint widths are acquired.By analyzing the MO image characteristics and extracting the weld joint features,the influence of magnetic field intensity and weld joint width on the MO images and detection of weld joint position is observed and summarized. 相似文献
5.
Laser hybrid welding of an eccentric fillet joint causes a complex geometry for fatigue load by 4-point bending. The weld surface geometry and topography were measured and studied in order to understand the crack initiation mechanisms. The crack initiation location and the crack propagation path were studied and compared to Finite Element stress analysis, taking into account the surface macro- and micro-geometry. It can be explained why the root and the upper weld toe are uncritical for cracking. The cracks that initiate from the weld bead show higher fatigue strength than the samples failing at the lower weld toe, as can be explained by a critical radius for the toe below which surface ripples instead determine the main stress raiser location for cracking. The location of maximum surface stress is related to a combination of throat depth, toe radius and sharp surface ripples along which the cracks preferably propagate. 相似文献
6.
Summary The influence of the distance between the solvent entry and the starting zone positions, Z0, on the average plate height was studied. This factor was found to be of major importance and could be optimized. The Guiochon and Siouffi model greatly underestimates the plate height for low values of Z0. 相似文献
7.
C.W. Tan Y.C. Chan Bernard N.W. Leung John Tsun Alex C.K. So 《Optics and Lasers in Engineering》2005,43(2):374
For the packaging of a pump laser in butterfly package, the most crucial assembly step is the fiber-to-laser diode coupling and attachment. The use of laser welding as the joining method offers several advantages if compared with the adhesive joints: strong joining strength, short process time and less contamination. This paper reports on laser welding process characteristics; weld strength and its fracture mode. The penetration depth and melt area of laser spot welds were found to be complicated functions of laser pulse energy, intensity, and beam diameter. Effects of pulse width, input power and size of the focal spot on the rate of energy input to the workpieces and consequently, the weld strength were reported. The weld strength was found to be dependent on the overlapping area between the two joining materials. Surface roughness, Ra, has influence on the fraction of energy absorbed, A, and therefore, affecting the penetration depth. Thermal analysis was carried out on the laser-welded joints and its heat-affected zone (HAZ) induced by various power densities was examined. These data are important in order to optimize and utilize the laser welding process as an effective manufacturing tool for fabrication of reliable pump laser. 相似文献
8.
给定寿命下的焊趾疲劳裂纹深度尺寸分析 总被引:1,自引:0,他引:1
本文提供并用统计方法研究了焊趾疲劳裂纹扩展的N~α曲线族,给出了联系给定裂纹尺寸下的疲劳分布,给定疲劳寿命下的裂纹尺寸分布以及随机初始条件的概率相容条件。研究表明,给定寿命下的焊趾疲劳裂纹深度尺寸α服从分布Ф[(μ(a)-logN)/σ(a)]。 相似文献
9.
The emergence of B2B spot markets has greatly facilitated spot trading and impacted supply chain structures as well as the way commercial transactions take place between firms in many industries. While providing new opportunities, the B2B spot market also exposes participants to a price risk. This new business landscape raises some important questions on how the supplier and manufacturer should change their sales channel and procurement strategies and tailor their decisions to this changing environment. In this paper, we study the channel-choice, pricing and ordering/production decisions of the risk-averse supplier and manufacturer in a two-tier supply chain with a B2B spot market. Our analysis shows that, to benefit from the B2B spot market and control the risk exposure, the upstream supplier should develop an integrated channel-choice and pricing strategy. When the supplier adopts a dual-channel strategy, the equilibrium contract price decreases in the supplier’s risk attitude, but increases in the demand uncertainty. However, it first decreases and then increases in the manufacturer’s risk attitude and spot price volatility. We conclude that rather than simply being a second channel, the B2B spot market provides a strategic tool to supply chain members to achieve an advantageous position in their contract trading. 相似文献
10.