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1.
2.
Microwave-induced organic reaction enhancement (‘MORE’) chemistry technique (open vessel; controlled microwave energy to stay below the boiling point of the reaction mixture) was used for the N-formylation of aliphatic and aromatic amines and amino heterocycles with aq formic acid (80%) on a multiple gram scale in a few minutes. 相似文献
3.
Masashi Ohkawa Yuki Shirai Takeshi Goto Seishi Sekine Takashi Sato 《Fiber and Integrated Optics》2002,21(2):105-113
In this paper, a silicon-based integrated optic pressure sensor using an intermodal interference between the fundamental TM-like and TE-like modes is described. The sensor consists of a micromachined rectangular diaphragm and a straight polystyrene optical waveguide passing over the diaphragm. Its sensitivity is theoretically known to be strongly dependent on the position of the waveguide over the diaphragm. To experimentally investigate such dependence, we fabricated a sensor with a 1.2 mm ×10 mm ×20 μm diaphragm, over which waveguides were placed at 50 μm intervals. The measured phase sensitivity was 98 mrad/kPa for the waveguide nearest to the diaphragm edge. The measurement was also carried out for the other waveguides. As theoretically expected, the largest sensitivity was obtained for the waveguide nearest to the edge. 相似文献
4.
A. B. Mitkevich 《Mechanics of Composite Materials》2005,41(6):497-504
Errors in the programs of winding pressure vessels can lead to an asymmetric reinforcement structure, which affects the equilibrium
shape of their domes and the tension in the left and right families of filaments. In this paper, equations determining the
equilibrium shape of the domes, the tension in filaments, and the shear stresses between layers are obtained. Examples with
winding trajectories in the form of geodesics and constant-deviation lines are considered. It is found that, for pressure
vessels, in the absence of external torque, the tension levels in filaments of the left and right families differ considerably.
It is also revealed that, for actual friction coefficients in winding, the shear stresses taken up by the binder are insignificant.
__________
Translated from Mekhanika Kompozitnykh Materialov, Vol. 41, No. 6, pp. 743–752, November–December, 2005. 相似文献
5.
A novel field emission pressure sensor has been achieved utilizing carbon nanotubes (CNTs) as the electron source. The sensor consists of the anode sensing film fabricated by wet etching process and multi-wall carbon nanotubes (MWNTs) cathode in the micro-vacuum chamber. MWNTs on the silicon substrate were grown by thermal CVD. The prototype pressure sensor has a measured sensitivity of about 0.17-0.77 nA/Pa (101-550 KPa). The work shows the potential use of CNTs-based field-emitter in microsensors, such as accelerometers and tactile sensors. 相似文献
6.
W.F. Wang 《Journal of Quantitative Spectroscopy & Radiative Transfer》2004,86(4):437-444
It is shown that by including the second term of Magnus expansion, improved convergence can be achieved for the non-perturbative pressure broadening formalism proposed by Neilson and Gordon (J. Chem. Phys. 58 (1973) 4131). The present method was applied to the line broadening calculations of CO in a bath of Ar. 相似文献
7.
开放式微波消解与干灰化法消解测量食品中铅的方法比较 总被引:1,自引:0,他引:1
对开放式微波消解法与干灰化法消解测量食品中铅的方法进行了比较,试验表明,前者操作简易,试验周期短,在测量精度和加标回收率方面两种方法无显著性差别。 相似文献
8.
Endoscopic Observation of Tissue by Narrowband Illumination 总被引:6,自引:0,他引:6
Kazuhiro Gono Kenji Yamazaki Nobuyuki Doguchi Tetsuo Nonami Takashi Obi Masahiro Yamaguchi Nagaaki Ohyama Hirohisa Machida Yasushi Sano Shigeaki Yoshida Yasuo Hamamoto Takao Endo 《Optical Review》2003,10(4):211-215
We propose a new illumination method for a medical endoscope: narrow band imaging (NBI), in which the spectral bandwidth of the filtered light is narrowed. To confirm how the spectral specifications of the filtered light influence a reproduced image, an experiment was conducted observing the endoscopic images of the back mucosa of a human tongue. In addition, the effect of NBI on endoscopic images was investigated through preliminary clinical tests in colonoscopy and upper gastrointestinal endoscopy. It has been shown that NBI can enhance the capillary pattern and the crypt pattern on the mucosa. These patterns are useful features for diagnosing an early cancer. 相似文献
9.
10.
Jean-Marcel Colmont François Rohart Jean-Pierre Bouanich 《Journal of Molecular Spectroscopy》2006,238(1):98-107
Extensive experiments on the K = 3 component of the J = 12-11 rotational transition of acetonitrile CH3C14N, located near 220.7 GHz, were performed at different temperatures in the range 235-350 K. They allow determining the N2-, H2-, and He-broadening coefficients, as well as their temperature dependences. More specific measurements on all the K-components of the involved transition perturbed by N2 at 303 K allow to point out a clear decreasing of the broadening coefficient with increasing K. Narrowing effects are clearly observed, and experimental lines were analysed both with Voigt and speed dependent Voigt profiles; but no exhaustive lineshape study was carried out. All the experimental parameters are compared with results derived from a semiclassical calculation of collisional interactions, including electrostatic, induction, and dispersion energy contributions. 相似文献