Micro enzymatic assay coupled to capillary electrophoresis via liquid junction

Summary A system for capillary electrophoresis combined with enzymatic assay has been evaluated for the two enzymes glucose-6-phosphate dehydrogenase and 6-phosphogluconate dehydrogenase. Instrumentation included a post-column reactor coupled to the separation capillary by a liquid junction. A technique for generating a substrate solution flow into the reactor by utilizing two high voltage supplies is proposed. This method offers a high degree of freedom in optimizing the separation and enzymatic reaction conditions individually. Possibilities for improving the enzymatic assay sensitivity were also examined.     

幅相一致行波管高频电路CAD研究

 在行波管的设计和装配过程中，各部件的尺寸必须严格控制，高频电路参数的离散对行波管色散特性有极大的影响。使用螺旋导电面模型，模拟计算了高频结构各主要参数离散对色散特性和轴向互作用耦合阻抗的影响。分析计算了夹持杆宽度、翼片高度、螺旋线平均半径、螺距、夹持杆介电常数等离散时对色散特性和轴向互作用耦合阻抗的影响，为新型幅相一致行波管的设计和生产提供了很有价值的参考建议。     

The push-out region of an immersed manifold

We consider immersions: and construct a subspace of which corresponds to a set of embedded manifolds which are either parallel to f, tubes around f or, in general, partial tubes around f. This space is invariant under the action of the normal holonomy group, We investigate the case where is non-trivial and obtain some results on the number of connected components of . Received 24 March 2000.     

Polytetrafluoroethylene and metal structure convective-flow CO laser

A convective flow CO laser composed of polytetrafluoroethylene discharge tubes, nickel–chromium steel components, a cupric heat exchanger and other components is described. Operating in liquid nitrogen condition, output power of 60 W has been obtained from a non-selective cavity.     

双面加热环形通道内干涸点的确定

根据环形管通道内流体流动和换热的特点,以Kirillov和Smogalev提出的干涸点理论模型假设为基础,从最基本的质量守恒方程出发,并引入临界液膜厚度等相应的辅助模型,得到了双面加热环形通道内流动沸腾干涸点的理论模型。同时针对间隙为1.0mm和1.5mm的环形窄缝进行了低压低质量流速工况下干涸点的实验研究。比较发现理论模型预测值与实验结果基本相符。说明本文提出的理论模型适用于低压低流量条件下的窄环形通道。实验同时发现:环状流临界热流密度在系统压力为2.2MPa达到最大值,临界含汽量随质量流速的增大呈缓慢下降趋势。     

Fully developed mixed convection in horizontal and inclined tubes with uniform heat flux using nanofluid

Fully developed laminar mixed convection of a nanofluid consists of water and Al₂O₃ in horizontal and inclined tubes has been studied numerically. Three-dimensional elliptic governing equations have been solved to investigate the flow behaviors over a wide range of the Grashof and Reynolds numbers. Comparisons with previously published experimental and numerical works on mixed convection in a horizontal and inclined tube are performed and good agreements between the results are observed. Effects of nanoparticles concentration and tube inclinations on the hydrodynamics and thermal parameters are presented and discussed. It is shown that the nanoparticles concentration does not have significant effects on the hydrodynamics parameters. Heat transfer coefficient increases by 15% at 4 Vol.% Al₂O₃. Skin friction coefficient continually increases with the tube inclination, but the heat transfer coefficient reaches a maximum at the inclination angle of 45°.     

用毛细管测量纯水表面张力系数的误差讨论

通过用毛细管测量纯水表面张力系数实验，得到管内径d与接触角θ的相对误差之间的关系曲线，由此说明实验测得的表面张力系数α和理论公式相比呈现一定的偏差，并简单地讨论了实验的理想状态与实际情况的差别．     

螺旋线径向挤压变形对其慢波结构冷测特性的影响

 介绍了用MAFIA软件的准周期边界条件计算螺旋线行波管慢波结构的色散和耦合阻抗，以及用ANSYS软件对螺旋线径向挤压变形建模的方法，并对螺旋线受挤压径向变形对其冷测特性的影响进行了详细的分析。结果表明:螺旋线径向挤压变形会导致相速增大，而在通常的变形范围内耦合阻抗也会增加；当变形继续增大时耦合阻抗上升到最大值后开始下降。     

微全分析系统检测方法的研究进展

综述了不同类型的检测方法在微全分析系统的应用，并简述了各类型的检测方法的优缺点。引用文献92篇。     

Quality assurance for the analytical data of micro elements in food

The micro element content of food is an important quality index due to the action of these elements on human health. In this article, we discuss how to ensure the reliability of analytical data on micro elements in order to truly represent the condition of food. Sampling, treatment of the analytical sample, selection of the analytical method, standard solution, and certified reference material, blank test, calibration of the instrument and equipment, application of the quality control chart, assessment of the final analytical result, and quality assurance system are briefly described. Received: 5 July 2001 Accepted: 19 November 2001