注浆覆岩离层力学机理及其离层发育分类研究

依据覆岩离层生成的力学机理,结合煤层开采程度的不同,将可注浆层位的离层划分为三类.以岩石的应变为指标,确立了覆岩离层可注浆层位岩梁的断裂步距表达式,理论上证明了划分注浆层位的合理性.根据岩石的全应力应变试验,结合现场实际观测数据,对以应变为指标的岩梁断裂步距表达式做了初步验证.结果表明:可注浆层位的分类和断裂步距表达式的确定对注浆减沉工程具有指导意义.     

添加剂PVP和MTS对合成Beta分子筛结构与性能的影响

分别以铝酸钠和硅溶胶为铝源和硅源,四乙基氢氧化铵为模板剂,在水热条件下,考察了添加剂(聚乙烯吡咯烷酮(PVP)和甲基三乙氧基硅烷(MTS))对合成Beta分子筛结构与性能的影响,并通过XRD、TEM、BET、ICP、~(29)Si-NMR和NH_3-TPD等方法对合成样品进行了结构表征和作用机理讨论,同时以催化裂化异丙苯为模型反应评价其催化性能。结果表明,与传统Beta分子筛相比,加入PVP后所得样品具有更高结晶度和较高的硅铝物质的量比(25.68)以及较大的比表面积(772 m~2/g);而加入MTS后尽管具有较大比表面积(657 m~2/g)和较高硅铝物质的量比(25.76),但是结晶度却相对降低,且粒径减小(160-320 nm)。两种添加剂作用下所得样品均具有更多酸量,在催化裂化异丙苯的反应中表现出较高的催化活性。     

马田系统在数据分类中的应用

马田系统是一种新的模式识别技术,是将田口式信噪比的试验设计方法的一整套思想应用到模式识别的特征变量选择问题上,并通过构建正常样品的基准空间,应用马氏距离值进行样品类别的识别.探讨了马田系统的基本原理,并应用MTGS模型方法对费希尔关于鸢尾花类型的判别问题进行研究,显示了马田系统方法的良好判别分类效果.     

简单自反MTS(υ,λ)的存在谱

一个Mendelsohn三元系MTS(υ,λ)=(X,B)被称作是自反的,如果它与它的逆(X,B-1)是同构的,其中B-1=｛〈z,y,x〉;〈x,y,z〉∈B.在[2]中已给出了简单自反MTS((υ,1)的存在谱,即υ≡0,1(mod3),υ3且υ≠6.本文讨论一般λ的情况,并得到简单自反MTS(υ,λ)的存在谱是λυ(υ-1)≡0(mod3);λυ-2,υ3且(υ,λ)≠(6,1);(6,3).     

A novel methodology for online detection of bearing health status for naturally progressing defect

A methodology is proposed for the online detection of health status of rolling element bearing into various damage stages for naturally progressing defect. Various damage identification parameters are derived from processing vibration data in time domain, frequency domain and time–frequency domain. The parameters are fused into a single parameter, Mahalanobis distance, by application of Gram–Schmidt Orthogonalization process. Chebyshev?s inequality is applied to the Mahalanobis distance for online monitoring and damage stage detection. A simulation study is first carried out to show working of the proposed methodology in presence of varying trends of damage identification parameters. The proposed methodology is then validated on experimental data. The first validation is on the vibration data acquired from a bearing having seeded defect. Later, two accelerated life tests are conducted on a specially designed test rig at different load and speed combinations on the bearings for ensuring naturally induced and progressed defects. The methodology is successfully verified on the vibration data acquired from the naturally induced and progressed defect experiments.     

Synergistic effects and related bioactive mechanisms of Potentilla fruticosa Linn. leaves combined with green tea polyphenols studied with microbial test system (MTS)

Previous research found Potentilla fruticosa leaf extracts (PFE) combined with green tea polyphenols (GTP) showed obvious synergistic effects based on chemical mechanisms. This study further confirmed the synergy of PFE + GTP viewed from bioactivities using the microbial test system (MTS). The MTS antioxidant activity results showed the combination of PFE + GTP exhibited synergistic effect and the ratio 3:1 showed the strongest synergy, which were in accordance with the results in H₂O₂ production rate. The combination of PFE + GTP promoted CAT and SOD enzyme activity and their gene expression especially at the ratio 3:1. Therefore, the synergism of PFE + GTP may be due to the promotion of CAT and SOD genes expression which enhanced the CAT and SOD enzyme activities. These results confirmed the synergy of PFE + GTP and could provide theoretical basis to produce a compounded tea made of a mixture of leaves from Potentilla species.     

间接糖基化马蹄金素衍生物的合成及抗乙肝病毒活性研究

以二缩三乙二醇或三缩四乙二醇为连接臂, 通过间接引入具有肝靶向性的D-半乳糖配基的方法, 设计合成了6个半乳糖糖基化修饰的肝靶向马蹄金素(MTS)衍生物; 通过¹H NMR, ¹³C NMR, ¹H-¹H COSY, HMQC和ESI-MS对其结构进行了表征; 并以HepG2 2.2.15为细胞模型初步评价了目标化合物的抗乙肝病毒(HBV)活性. 结果表明, 所有目标化合物对HBV DNA的复制均有抑制作用, 且具有一定的量效关系. 化合物15b的体外抗HBV活性最好, 后期研究将选用其进行小鼠体内组织分布实验, 并与原型化合物以及Y101体内组织分布情况进行比较研究, 以验证半乳糖基的引入能否提高MTS衍生物的肝靶向性.     

A review on enzyme and ultrasound: A controversial but fruitful relationship

A critical review on the effect of ultrasound (US) on enzymes and their biocatalytic action is presented here. Discussion on the information users of US acquire before utilizing the different devices, and the importance they give to US frequency is constant along the review. The authors have gone into the different areas in which the US–enzyme binomial has been applied. The lack of enough information on the US–enzyme-working conditions under which each piece of research has been developed, and the necessity to provide complete information on the data and metadata to give enough light on each piece of research (and thus on the potential comparison of results from different studies) are critically exposed. With this aim, the study has been divided into the positive effect of US on enzymes to favor the production of metabolites, polymers or proteins; and the degradation, inhibition or activation of the biocatalyst under US application. Also the effect of US on enzyme production and the main fields of application of the US–enzyme binomial are discussed.     

磁悬浮隔振器动态电磁力实验与建模

磁悬浮隔振器的核心部件是电磁作动器,得到其输出电磁力与线圈电流及气隙之间的模型对实现磁悬浮隔振器的主动隔振有着重要的意义.实际系统中,磁悬浮隔振器运动频率对电磁力模型参数有较大影响,为了得到比较精确的符合实际的电磁力模型,对原有模型进行了修正,给出了新的考虑频率因素的修正模型;并且设计了基于MTS809的动态电磁力实验建模方案,直接根据电磁力实时测量数据辨识得到动态电磁力修正模型,而不需要对磁路进行任何假设.实验结果表明,该方法建立的电磁力修正模型更符合实际情况.