金属β-二酮化合物用于MOCVD法生长铁电氧化物薄膜

对用于MOCVD法生长铁电氧化物薄膜的金属β－二酮化合物的制备、结构及性质进行了评述，对它们在生长铁电薄膜中的应用现状进行了介绍，并对它们的应用前景作了展望。     

Ultrasound imaging and evaluation of lesion induced by High Intensity Focused Ultrasound

The present study was to investigate the differential imaging method for detecting HIFU (High Intensity Focused Ultrasound)-induced lesions and the estimation of variation of attenuation for lesion evaluation with log spectral difference algorithm. Experiment results of bovine muscle and liver in vitro were acquired. Several algorithms for lesion detection - Absolute Difference (AD), Sum Absolute Differences (SAD) and Sum Squared Differences (SSD) - were analyzed with several window sizes and threshold values. Then three attenuation parameters were compared to evaluate the degree of tissue damage. It was found that variation of the mean attenuation △α was an effective parameter to evaluate lesions.     

Influence of Mobile Phase Composition on the Enantioseparation of Meythoxyl Flavanones with Self—prepared CDMPC Column and Chiral Recogniton Mechanism

The influence of different alcohol modifiers in mobile phase on the chiral separation of 4‘‘‘‘‘‘‘‘-methoxyl flavanone,5-methoxyl flavanone and 6-methoxyl flavanone on cellulose tris(3,5-dimethylphenylcarbamate)(CDMPC)column was studied and the chiral recognition mechanism was discussed.Using hexane-tert-butanol(1.31molL^-1) as the mobile phase,those three methoxyl flavanones were excellently separated on CDMPC chiral column.     

Effects of External Electric Field on Ferroelectric Superlattice with Two Alternating Layers

The effects of the external electric field on the ferroelectric superlattice with two alternating layers have been studied using the transverse Ising model based on the effective-field theory with the differential technique. The hysteresis loops and susceptibility of the system have been given. The stronger the external electric field, the smaller the susceptibility, reflecting that the polarization is weaker.     

流动注射化学发光法测定甲磺酸双氢麦角毒碱

磺酸双氢麦角毒碱(Co-dergocrine mesvlate,Hydergine)又名喜得镇、舒脑宁,我国将其列为国家基本药物.目前,测定甲磺酸双氢麦角毒碱的分析方法,主要有荧光分光光度法、可见紫外分光光度法、免疫分析法,但未见文献报道过化学发光法测定甲磺酸双氢麦角毒碱的研究.作者发现,在碱性条件下,过氧化氢直接氧化甲磺酸双氢麦角毒碱不会产生化学发光,但当高碘酸钾和甲磺酸双氢麦角毒碱混合反应后,再加过氧化氢氧化会产生较强的化学发光,且发光强度与甲磺酸双氢麦角毒碱的浓度在一定范围内有良好的线性关系,据此建立了流动注射化学发光测定甲磺酸双氢麦角毒碱的新体系.     

负动量压缩因子的环形对撞机磁聚焦结构的研究

探讨了设计负动量压缩因子(α_p<0)的正负电子对撞机储存环磁聚焦结构的可行性及方法.作为应用实例,说明了设计α_p<0的τ–粲工厂磁聚焦结构的可能性.     

金钢石的制备研究

本文研究了两种不同质异构体石墨—金刚石的转化条件，以及在实验室现有条件下，利用石墨材料制备金刚石颗粒的具体方法和试验结果。     

NaNO3掺杂Y2O3材料的制备及电流变性质

利用NaCO3和Y（NO3）3做主要原料，合成了一系列用稀土氧化物（Y2O3）作为基础材料的新型电流变材料——NaNO3掺杂Y2O3材料。对于这些材料的介电性质、微观结构和电流变性能的研究结果表明，NaNO3的掺杂可以明显地提高Y2O3材料的电流变活性。材料在二甲基硅油中的悬浮液的剪切应力随NaNO3在Y2O3中的掺杂程度有明显变化，当Na／Y（物质的量的比）为0．6时材料的电流变性能最好，     

毛细管电色谱中进样时间对柱效的影响

毛细管电色谱是近年发展起来的一种新型微分离技术，它结合了高效液相色谱和毛细管电泳的物点，具有高效、快速，高选择性，其有关理论研究和应用越来越深入，本文从色谱动力学角度讨论了毛细管电色谱中进样时间对柱的影响。     

光泽精化学发光体系的研究与应用

对光泽精化学发光体系的动力学性质、荧光光谱、化学发光光谱及化学发光机理进行研究和探讨。详细研究了光泽精 - H2 O2 - Co( )流动注射化学发光体系的最佳分析条件。结果表明 ,当光泽精 (L c)为 2 .5×10 - 5mol/L、H2 O2 为 0 .5 mol/L、Na OH为 0 .4 mol/L、CTMAB为 2 .0× 10 - 5mol/L时 ,测定 Co( )的校准曲线线性范围为 0 .0 5— 2 0 0μg/m L ,检出限为 0 .0 1μg/m L。对 10μg/m L Co( )连续测定 7次 ,相对标准偏差为 1.7%。