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排序方式: 共有79条查询结果,搜索用时 750 毫秒
1.
E. K. Merabet H. K. Yuen W. A. Grote K. L. Deppermann 《Journal of Thermal Analysis and Calorimetry》1994,42(5):895-906
A new sensitive isothermal titration microcalorimeter using polyvinylidene difluoride (PVDF) as detector has been developed. Heat pulses of less than 0.4 μJ can be detected and the baseline noise level (p-p) is 40 nW. The calorimeter is constructed with one reaction cell (0.7 ml) insulated by several radiation shields inside a vacuum chamber. The performance of the instrument was examined by measuring the heat of protonation of Tris with HCl. The enthalpy of reaction was found to be ?49±1 kJ·mol?1, in good agreement with the reported value of ?47.5 kJ·mol?1. 相似文献
2.
FTIR-RAIRS and ATR techniques are shown to provide a powerful means of investigating the molecular behaviour responsible for the pyroelectric properties of organic monolayer assemblies on silicon and aluminised glass. Spectral changes, associated with either proton transfer or head group rearrangement, are well correlated with the level of pyroelectric response for two different devices. The technique promises to be extremely important for the elucidation of the microscopic properties of molecular electronic devices. 相似文献
3.
Sabine Apelt Susanne Höhne Petra Uhlmann Ute Bergmann 《Surface and interface analysis : SIA》2020,52(12):1150-1155
Active deicing of technical surfaces, such as for wind turbines and heat exchangers, currently requires the usage of heat or chemicals. Passive coating strategies that postpone the freezing of covering water would be beneficial in order to save costs and energy. One hypothesis is that pyroelectric active materials can achieve this because of the surface charges generated on these materials when they are subject to a temperature change. High-quality poly(vinylidene fluoride-co-trifluoroethylene) (P(VDF-TrFE)) thin films with a high crystallinity, prefererd edge-on orientation, low surface roughness, and comprised of the β-analogous ferroelectric phase were deposited by spin-coating. Freezing experiments with a cooling rate of 1 K min−1 were made on P(VDF-TrFE) coatings in order to separate the effect of different parameters such as the poling direction, film thickness, used solvent, deposition process, underlying substrate, and annealing temperature on the achievable supercooling. The topography and the underlying substrate significantly changed the distribution of freezing temperatures of water droplets in contact with these thin films. In contrast, no significant effect of the thickness, morphology, or pyroelectric effect of the as-prepared domain-state on the freezing temperatures was found. 相似文献
4.
5.
在制造红外热释电探测器阵列过程中,需要利用超薄钽酸锂(LiTaO3)晶片作为红外热释电探测器件的敏感层。通常LiTaO3晶片的厚度远厚于红外热释电探测器件要求的厚度,所以需要采用键合减薄技术对LiTaO3晶片进行加工处理。键合减薄技术主要包括:苯并环丁烯(BCB)键合、铣磨、抛光、加热剥离、刻蚀BCB。加工后得到面积为10mm×10mm、厚度为25μm的超薄单晶LiTaO3薄膜,晶片厚度、表面粗糙度和面形精度比较理想。测得了LT晶片减薄后的热释电系数为1.6×10-4Cm-2K-1。得到的单晶LiTaO3薄膜满足红外热释电探测器敏感层的要求。 相似文献
6.
You Ming-Chang 《International Journal of Infrared and Millimeter Waves》1986,7(6):919-925
The configurations of the coupling network, which can effectively aecrease the effect of the noise sources within the amplifier on the equivalent input noise of the whole pyroelectric detector-amplifier system, are studied. The influences of feedback upon the noise properties of the basic amplifiers are analyzed. The procedures of designing low-noise pyroelectric detector-amplifier systems are followed. 相似文献
7.
Optically driven actuators have a feature of a non-contact method supplied by light energy. A new method is proposed with
three poly(vinylidene difluoride) (PVDF) cantilevers as the legs and a polymer film as the body. The PVDF cantilevers are
coated with silver on one surface. When one side of the cantilever is irradiated by a laser beam, an electric field is produced
along a cross-section of the cantilever by the pyroelectric effect and a mechanical displacement occurs by the piezoelectric
effect. Its response time and its generated force are measured experimentally. Two types of optically driven actuators using
PVDF film are proposed to move using different characteristics. 相似文献
8.
一种实用化实时测温系统的优化设计 总被引:11,自引:1,他引:10
基于基尔霍夫定律,利用半导体激光器及钽酸锂热释电探测器设计了一种实用化的实时测温系统。依照测温系统各主要技术指标(温度分辨力、温度的标准偏差及测温范围)与各主要技术参量(激光光源的能量、波长、放大器的带宽及光学系统的相对孔径等)之间的关系,对实时测温系统的各主要参量(激光光源的能量、光学系统的相对孔径及放大器的带宽)进行了优化设计。实验表明,在测温范围673~1473K内,温度测量的不确定度优于0.3%,分辨力优于0.4K,均符合设计要求。 相似文献
9.
层合球面各向同性热释电空心球的瞬态响应 总被引:1,自引:0,他引:1
运用叠加原理,将层合球面各向同性热释电空心球的球对称动力学问题的解分成准静态和动
态两部分,准静态部分首先运用状态空间法给出了显式表达式,然后运用分离变量法、初参
数法和特征函数展开技术,给出了动态部分的表示式,再结合内外表面上的电学边界条件和
界面上的电学连续条件,导出一个关于时间函数的第二类Volterra积分方程,运用插值法
可成功地给出此积分方程的高精度数值解,最终可求得原问题的位移、应力、电位移以及电
势的响应. 此方法适用任意层数且各层是任意厚度的层合热释电空心球作用随时间以任意形
式变化的球对称温度场. 文中还给出了数值结果. 相似文献
10.