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V. V. Semenov E. Yu. Ladilina T. A. Chesnokova N. K. Elistratova Yu. A. Kurskii N. P. Makarenko 《Russian Chemical Bulletin》1995,44(5):927-930
Reactions of Cl2MeSiSiMeCl2 with RMgCl make it possible to obtain and isolate pure disilanes containing a smaller number of functional groups, namely, RMeClSiSiMeCl2 (R = Ph), RMeClSiSiMeRCl (R = Pri, Ph), and R2MeSiSiMeRCl (R = Bui). The reaction of Cl2MeSiSiMeCl2 with BunMgCl is the least selective. The chlorides obtained were reduced with LiAlH4 into the corresponding hydrides.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 5, pp. 954–957, May, 1995. 相似文献
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