A simple,rapid and sensitive method based on modified multiwalled carbon nanotube for preconcentration and determination of lead ions in aqueous media in natural pHs

In this study, multiwalled carbon nanotube (MWCNT) was modified by the pyridine group using a silane agent and characterized by infrared spectroscopy (IR), thermal analysis (TG/DTA), and elemental analysis (CHN) and scanning electron microscopy (SEM). The application of this sorbent was investigated in determination of lead ions in aqueous samples, using flame atomic absorption spectrometry (FAAS). Through this study, different parameters such as pH and sample flow rate on adsorption process and eluent concentration, volume and flow rate were optimized. The limit of detection (LOD), the relative standard deviation and the recovery of the method were 2 ng mL^?1, 1.3% and 99.7%, respectively. Two standard reference materials (NIST 1571 and NIST 1572) were used to verify accuracy of this method. Finally, the sorbent was successfully applied for extraction and determination of low levels of Pb(II) ions in aqueous samples.     

微振动光电检测与数据采集系统的设计

提出了一种新的光学非接触式测量方法测量了物体的微振动振幅。用激光作为光源,以四象限硅光电池[1]作为光电探测器,借助三角测量原理,投射在振动源表面的激光反射光束在光电探测器上产生平面位移,将位移信号放大,通过A/D模块采集电压数值,并通过串口通信机制在PC终端实时显示。实验结果表明,该方法原理正确,灵敏度高,便于实现连续、快速、自动化检测,在工业在线检测方面具有良好的应用前景。     

A Modified Quasi-Newton Method for Structured Optimization with Partial Information on the Hessian

This paper develops a modified quasi-Newton method for structured unconstrained optimization with partial information on the Hessian, based on a better approximation to the Hessian in current search direction. The new approximation is decided by both function values and gradients at the last two iterations unlike the original one which only uses the gradients at the last two iterations. The modified method owns local and superlinear convergence. Numerical experiments show that the proposed method is encouraging comparing with the methods proposed in [4] for structured unconstrained optimization Presented at the 6th International Conference on Optimization: Techniques and Applications, Ballarat, Australia, December 9–11, 2004     

修正的Shepard型算子的Lp-逼近

摘要:本文在L_[0.1]~p空间给出了 Durrmeyer型修正的shepard算子D_n(f,x),对 f∈L_[0.1]~p,(p≥1),得到了下列的Jackson型估计:││D)n(f)-f││_p≤ C_(pλω)(f,n~(-1))p,λ≥2, Cω(f,n~(-1)logn)p,λ=2, C_(pλω)(f,n~(-1))p,1<λ<2,     

Modeling of radiative heat transfer in an axisymmetric cylindrical enclosure with participating medium

Radiative heat transfer in an axisymmetric enclosure with absorbing, emitting, and scattering medium is studied here by using the different methods such as MDOM, FVM, and MFVM with emphasis on the treatment of angular derivative term, which appears in curvilinear coordinates due to angular redistribution. After final discretization equation for MFVM is introduced by using the step scheme and directional weights, the present approach is validated by applying it to three different benchmarking problems with absorbing, emitting, and scattering medium. All of the results presented here support its accuracy as well as moderate efficiency. Finally, the present approaches are applied to a truncated cone-shaped enclosure as a body-fitted geometry case.     

The equivalence between the convergence of Ishikawa and Mann iterations with errors for strongly successively pseudocontractive mappings without Lipschitzian assumption

In this paper we prove some new equivalences between convergence of the Ishikawa and Mann iteration sequences with errors in two schemes by Xu [Y.G. Xu, Ishikawa and Mann iteration process with errors for nonlinear strongly accretive operator equations, J. Math. Anal. Appl. 224 (1998) 91-101] and Liu [L.S. Liu, Ishikawa and Mann iterative process with errors for nonlinear strongly accretive mappings in Banach spaces, J. Math. Anal. Appl. 194 (1995) 114-125], respectively, for strongly successively pseudocontractive mappings. Our main results improve and extend the corresponding results of the all references listed in this article.     

微纳米加工技术在纳米物理与器件研究中的应用

物质在纳米尺度下可能呈现出与体材料不同的物理特件，这正是纳米科技发展的基础之一。要想探索在纳米尺度下材料物埋性质的变化规律及可能的应用领域，离不开相应的技术手段，微纳米加工技术作为当今高技术发展的重要技术领域之一，是实现功能人工纳米结构与器件微纳米化的基础。本文根据几个不同的应用领域，介绍了微纳米加工技术在纳米物理与器件研究领域的应用。     

微纳米加工技术及其应用综述

材料与结构在微纳米尺度展现了许多不同于宏观尺度的新特征，纳米技术已经成为当前科学研究与工业开发的热门领域之一。微小型化依赖于微纳米尺度的功能结构与器件，实现功能结构微纳米化的基础是先进的微纳米加上技术，文章对微纳米加上技术做了一个综合的介绍，简要说明了微纳米加工技术与传统加工技术的区别，在微纳米加工技术的应用方面提出了一些合理选择加工技术的原则，并对当前微纳米加工技术面临的挑战和今后发展的趋势作了预测。