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毛细管电泳安培检测扑热息痛及其水解物 总被引:1,自引:0,他引:1
研究了各种电化学预处理条件下碳纤维电极对扑热息痛及水解物的电化学行为。确定该体系最佳预处理条件为0.2V电位下阳极化1min,再于-2.0V下阴极化10s。预处理后的碳纤维伏安响应得到明显提高。运用最佳条件并在支持电解中加入添加剂后,扑热息痛及其水解物在毛细管电泳上获得很好的分离和检测。其中扑热息痛的检测下限为2.78pg;对氨基酚为1.84pg。 相似文献
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Let D
N
, G
M
be two open sets, E D and F G two compact sets which satisfy the condition (H) (that is a harmonic condition similar to Leja"s condition). We find an open set
N+M
such that each separately harmonic function f : X : = (D× F) (E × G) (i.e.: for all x in E, f(x,.) is harmonic on G; for all y in F, f(., y) is harmonic on D) extends to a harmonic function on . 相似文献
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本文利用联合谱半径刻画了级联算法在Besov和Thiebel-Lizorkin空间上的收敛性,给出了级联算法初值函数矩条件的新证明,并利用到细分分布的光滑性和非齐次细分方程解的存在性等方面.特别地,在某些条件下,我们证明了级联算法的有界性和收敛性相互等价. 相似文献
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《Comptes Rendus Physique》2015,16(9):836-850
In this paper, we first present a feasibility study to design 4G antennas (700–960 MHz and 1.7–2.7 GHz) for eyewear devices. Those eyewear devices should be connected to the last generation cellular networks, Wireless Local Area Networks or wireless hotspots. Three coupling element type antennas with their matching networks are evaluated in terms of reflection coefficient and total radiation efficiency when the eyewear is placed on the user's head. We also present Specific Absorption Rate (SAR) simulations when the eyewear is positioned over a homogeneous SAM phantom and over a heterogeneous VH (Visible Human) phantom: the SAR levels are compared to international limit values. In a second step, we present experimental results obtained with 3D printed eyewear and coupling elements etched on a classical PCB substrate where the matching circuits are optimized close to the feeding point of the coupling element. Simulated and measured values are in very good agreement: 7 to 16% and 9 to 35% total efficiency are respectively obtained for the low- and high-frequency bands. However, simulated SAR values are somewhat higher than authorized levels with preoccupant high electromagnetic field distribution close to the eye of the user. 相似文献
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本文介绍一种非跟踪式的由微处理器控制的轴角转换器的原理,对比分析了它与跟踪式轴角转换器的性能及特点。并附例供验证及参考。 相似文献
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赵晴初 《核聚变与等离子体物理》1991,11(3):177-180
在Tokamak等离子体实验结果分析中实际的平衡磁面是极需要的。本文试探从电磁测量信号推得平衡磁面。 一、自由边界平衡程序 借助于自由边界平衡程序计算中等托卡马克装置HT-6M的平衡量。从MHD平衡方程出发, 相似文献
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New interpolation error estimates and a posteriori error analysis for linear parabolic interface problems 下载免费PDF全文
Jhuma Sen Gupta Rajen Kumar Sinha G. Murali Mohan Reddy Jinank Jain 《Numerical Methods for Partial Differential Equations》2017,33(2):570-598
We derive residual‐based a posteriori error estimates of finite element method for linear parabolic interface problems in a two‐dimensional convex polygonal domain. Both spatially discrete and fully discrete approximations are analyzed. While the space discretization uses finite element spaces that are allowed to change in time, the time discretization is based on the backward Euler approximation. The main ingredients used in deriving a posteriori estimates are new Clément type interpolation estimates and an appropriate adaptation of the elliptic reconstruction technique introduced by (Makridakis and Nochetto, SIAM J Numer Anal 4 (2003), 1585–1594). We use only an energy argument to establish a posteriori error estimates with optimal order convergence in the ‐norm and almost optimal order in the ‐norm. The interfaces are assumed to be of arbitrary shape but are smooth for our purpose. Numerical results are presented to validate our derived estimators. © 2016 Wiley Periodicals, Inc. Numer Methods Partial Differential Eq 33: 570–598, 2017 相似文献