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Varlet et al. recently proposed a headspace-gas chromatography–mass spectrometry (HS-GC–MS) method applicable for the routine determination of CO2 in gaseous biologic matrices. This developed bioanalytical method was fully validated according to the SFSTP 1997 guidelines using the accuracy profile as a graphical decision-making tool.In this letter, we discuss the validity of HS-GC–MS method based on the newest SFSTP guideline. In particular, we demonstrate by the estimation of the β-expectation tolerance interval that the error total exceeds the acceptance limits (30%) for the second concentration level (0.5 μmol mL−1 vial HS). 相似文献
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本文通过对第四届全国超声治疗学术会议(1997年10月17-21日于南京)论文的综合介绍,显示我国超声波疗法在实验研究与临床应用方面所取得的成就。 相似文献
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计算了重离子引起的碎裂过程产生的类弹碎片动量分布约化宽度,拟合了实验数据.讨论了弹核碎裂过程从低能区到相对论能区随入射能量的系统演变. 相似文献
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