古诗与气象气候

中国诗歌源远流长，博大精深，内容涉及气象、气候知识的为数不少．其中借气象、气候景观表达真情实感最为亮丽，或热情奔放、直抒胸臆，或诙谐、暗喻，有浓郁的生活色彩．     

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阿斯巴甜合成工艺研究

探讨了以天冬氨酸和苯丙氨酸为原料制备甜味剂阿斯巴甜的合成工艺。首先对合成的各步反应进行了研究,然后考察了前三步反应每步之间连接的可能性,最后实现了中和之前各步反应的一锅化。一锅化的总收率达到63.6%左右,并且α－异构体与β－异构体的比率达到95.4：4.6。     

由5-唑烷酮合成α-天冬氨酰肽类的简便方法(英文)

用一锅法制得了２－三溴甲基－３－甲酰基－５－氧－４－口恶唑烷乙酸，它与氨基酸酯反应形成题称化合物Ｎ－甲酰基－α－天冬氨酰肽类。     

RP-HPLC法同时测定湿生扁蕾中4种有效成分的含量

建立同时测定藏药湿生扁蕾中獐牙菜苦苷、獐牙菜苷、异荭草苷、1,7-二羟基-3,8-二甲氧基口山酮含量测定方法.RP-HPLC法,使用VP-ODS C18柱(5μm,150 mm×4.6 mm),流动相为乙腈-0.4%磷酸水溶液,梯度洗脱[0～40.00min乙腈的体积分数(以下同)由10%线性递增至30%;40.01～55.00 min由30%线性递增至100%],流速为1.0 mL/min,柱温30℃,检测波长260 nm.结果:獐牙菜苦苷、獐牙菜苷、异荭草苷、1,7-二羟基-3,8-二甲氧基口山酮的线性范围为2.80～14.0 μg(r=0.9992),4.12～20.6μg(r=0.9997),0.34～1.68μg(r=0.9997),2.64～13.2 μg(r=0.9994);回收率分别为99.89%,99.52%,101.88%,99.42%.该方法可用于控制湿生扁蕾的质量.     

新疆保险公司营业大楼大体积筏板基础冬期施工

1996年，商品混凝土在乌鲁木齐还未得到广泛推广应用的情况下，不留施工缝，一次浇筑长65m，宽25m，厚1．6m，防渗等级S8这样大体积筏板基础混凝土，确有一定难度．为此，本文采取了有条件时优先选用商品混凝土，无条件或商品混凝土供应中断时现场搅拌进行浇筑的方法解决了这一难题．     

A New Furost—20（22）—ene Oligoglycoside from Asparagus cochinchinensis

A new furost-20(22)-ene oligoglycoside named as aspacochioside C was isolated from the roots of Asparagus cochinchinensis (Lour.) Merr. Its structure was elucidated to be 26-O-β-D-glucopyranosyl-(25S)-5β- furost-20(22)-en-3β,26-diol-3-O-α-L-rhamnopyranosyl-( 1 →4)-β-D-glucopyranoside on the basis of spectroscopic techniques including 1D and 2D NMR experiments.     

ON CERTAIN CONFIGURATIONS(T)OF FINIKOFF AND THE TRANSFORMATIONS OF CALAPSO

ⅠNTRODUC(?)NIn a recent paper the author has published the result, ofsome,investigations on the periodic sequences of Laplace of periodfour with a stratifiable couple of diagonal congruences.Thedeterinination of these soquences of Laplace requires the integrationof the classical partial differential equation     

Synthesis and Characterization of Poly （hydroxylethyl, octanediamine）-DL-aspartamide： a New Tissue Engineering Scaffolds

Collagen is the most widely used tissue-derived natural polymer for its goodbiocompatibility and cell adhesion but offers a limited range of mechanical properties1.The construction and properties of synthesized polypeptides are similar to collagen havethe…