新型高速气流测温传感器——半导体总温探针

采用IOTS 型半导体感温元件与气流滞止罩组合成测量高速气流总温的总温探针(TTPS).配以稳定度为5×10~(-5)的恒流源,在t=30～90℃的温度范围内,其最小二乘法非线性误差小于0.2℃,即最小二乘法线性度为0.2%;重复性为0.1%;灵敏度约为2mV/℃;在马赫数M=0.3～0.75范围内,动温校正系数β≥0.992,恢复系数γ=0.91～0.98.试验结果证明,国产半导体感温元件制作的TTPS 是可以代替热偶总温探针(TTPT)的.与TTPT 相此,不需冷端温度补偿,使用方便,并可避免由于补偿不完善而存在的误差;它比TTPT 的灵敏度高50倍,如与微机配合组成数据自动采集系统,可以降低对放大器性能的要求.     

Development and Research on the Internet Resources Aggregation Platform

We proposed an Intemet resource aggregation platform based on semantic web. The platform includes an Web Ontology Language（OWL） ontology design toolkit（VO-Editor） and a selective inference algorithm engine so that it can visually editing ontology and using novel selective reasoning for information aggregation. We introduce the VO-Editor and the principle of selective inference algorithm. At last a case of budget travel system is used to interpret the approach of Internet resources aggregation by this platform.     

A robust near infrared luminescent ytterbium metal-organic framework for sensing of small molecules

The first near-infrared luminescent ytterbium metal-organic framework has been realized for the highly selective and sensitive sensing of small molecules.     

Macroscopic Polarization Change of Mononuclear Valence Tautomeric Cobalt Complexes Through the Use of Enantiopure Ligand

The crystallization of a complex having electron transfer properties in a polar space group can induce the polarization switching of a crystal in a specific direction, which is attractive for the development of sensors, memory devices, and capacitors. Unfortunately, the probability of crystallization in a polar space group is usually low. Noticing that enantiopure compounds crystallize in Sohncke space groups, this paper reports a strategy for the molecular design of non-ferroelectric polarization switching crystals based on the use of intramolecular electron transfer and chirality. In addition, this paper describes the synthesis of a mononuclear valence tautomeric (VT) cobalt complex bearing an enantiopure ligand. The introduction of enantiomer enables the crystallization of the complex in the polar space group (P2₁). The polarization of the crystals along the b-axis direction is not canceled out and the VT transition is accompanied by a change in the macroscopic polarization of the polar crystal. Polarization switching via electron transfer is realized at around room temperature.     

常用抗菌药物对常见致病菌L型诱导的实验研究

目的:探讨临床常用抗菌药物对常见致病菌L型的实验室诱导作用,为临床诊治提供科学依据。方法:利用纸片弥散法和试管稀释法,分别对金黄色葡萄球菌、铜绿假单胞菌、大肠埃希菌、痢疾志贺菌进行L型菌的抗菌药物实验室诱导。结果:头孢唑林、头孢哌酮、氨苄西林、哌拉西林、左氧氟沙星均可不同程度诱导铜绿假单胞菌、大肠埃希菌、痢疾志贺菌形成相应的L型细菌,相同条件下金黄色葡萄球菌L型未诱导出。结论:部分抗菌药物在一定条件下能使某些细菌失去细胞壁转为L型菌,继而发生生物学性状的改变,临床诊断治疗时应给予重视。     

土与强风化岩双元边坡圆弧-平面破坏模式与支护设计方法

为了探究土与强风化岩边坡中强风化岩不破坏的临界坡率及稳定性判断方法,基于济南地层,得出适用于数值模拟的土层参数,并利用强度折减法求出边坡的临界坡率,为施工提供参考。针对强风化岩不破坏的边坡,运用改进的瑞典条分法求出边坡安全系数解析解,并利用滑移线场法求出滑移线,为安全系数解析解的应用提供依据。结果表明,岩层厚度超过边坡高度1/2或坡率大于1:0.5时,强风化岩一定破坏;解析解得出的安全系数偏小,有利于工程安全;针对土与强风化岩边坡,文中结果可确定边坡破坏区域,设计支护方案。     

Cubic and doubly-fused cubic samarium clusters from Sm(II)-mediated reduction of organic azides and azobenzenes

A polynuclear samarium imido complex [(L)Sm(4)(μ(3)-NSiMe(3))(4)] (2) featuring a cubane-like cluster has been synthesized from the reaction of an organic azide and a samarium(II) complex [(L)SmI(2)Li(2)(THF)(Et(2)O)(2)] (1). In addition, this divalent samarium starting material (1) reacts with azobenzene to give the first example of a well-defined doubly-fused cubic imido-cluster [(L)Sm(6)(μ(3)-NPh)(4)(μ(4)-NPh)(2)I(2)(THF)(2)] (4) in addition to a major cubic complex [(L)Sm(4)(μ(3)-NPh)(4)] (3).     

Towards a smallest scale of context in ontology integration

In order to solve the ambiguity problems in the semantic context （structure, granularity or scale） emerging in the process of ontology integration application, this paper analyzes the essential characters of context structure, proposes a novel semantic context generating algorithm, which is implemented over VO-Editor（visual ontology editor）, from the satisfiability-based point of view, and proves that the context entity generated by this algorithm is smallest in scale and unique. It offers a feasible means for developers to handle context problems for ontology integration application.     

Manipulating Slow Magnetic Relaxation by Light in a Charge Transfer {Fe2Co} Complex

Some cyanide-bridged complexes are known for exhibiting slow magnetic relaxation behavior in a light-induced metastable state. Herein, an unexpected reverse effect is observed for the first time in the S= {Fe^II_LS-Co^III_LS-Fe^III_LS} (HS=high spin, LS=low spin) ground state of a novel V-shaped trinuclear cyanide-bridged {Fe₂Co} complex. In this complex, light-switchable iron-cobalt charge transfer with repeatable off/on switching of slow magnetic relaxation is discovered upon alternating laser irradiation at 785 and 560 nm. An important characteristic of the present compound is that the S= ground state exhibits slow magnetic relaxation before irradiation, whereas this is accelerated after irradiation. This is different from the typical behavior, where the light-induced metastable state exhibits slow magnetic relaxation.     

小型西瓜新品系苗期对亚适温弱光的适应性差异研究

通过研究亚适温弱光下4个小型西瓜新品系的叶绿素含量、光合速率和叶绿素荧光参数等的变化,比较和评价小型西瓜新品系对亚适温弱光逆境的适应性差异。结果表明:亚适温弱光胁迫使小型西瓜幼苗叶片的叶绿素含量、净光合速率、蒸腾速率、胞间CO2浓度和气孔导度、光合量子效率、光化学猝灭、非光化学猝灭下降。不同品系相比,处理前后均以‘W005×M04’和‘S-12×X-4’幼苗叶片的净光合速率最高,‘W005×M04’幼苗叶片的蒸腾速率、气孔导度值最小,以‘S-2-6×T10’和‘新5×X-4’2个品系的净光合速率最低,蒸腾速率、气孔导度值最大;处理前4个新品系幼苗叶片胞间CO2浓度、光合量子效率、最大光化学效率、非光化学猝灭无差异,处理后以‘W005×M04’和‘S-12×X-4’幼苗叶片的光合量子效率、最大光化学效率、非光化学猝灭值最大,降幅最小;‘W005×M04’的胞间CO2浓度最大,‘S-2-6×T10’和‘新5×X-4’最小。因此亚适温弱光逆境的适应性差异由强到弱依次为:‘W005×M04’>‘S-12×X-4’>‘S-2-6×T10’和‘新5×X-4’。