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排序方式: 共有611条查询结果,搜索用时 15 毫秒
1.
用相位调制方法测量光盘盘基应力双折射的精度分析 总被引:4,自引:2,他引:2
偏振相位调制方法是测量微小双折射的一种高精度检测方法。本文系统全面地分析了以PMCSA结构形式测量光盘盘基应力双折射的相位调制方法中,由各种误差源造成的对测试结果的影响。 相似文献
2.
表面粗糙度测量的磁光位相调制和锁相干涉 总被引:1,自引:0,他引:1
提出了一种表面粗糙度测量的新方法,该方法采用了微分偏振干涉的原理,利用由法拉第磁光调制器所组成的调制系统对偏振干涉光路的位相进行调制,利用锁相干涉原理对位相进行探测,该方法可实现无参考面快速非接触测量,在普通实验条件下,也可保持良好的稳定恶性循环 ,实验装置即可给出表面的轮廓又可给出其它统计数据,其横向分辨率为1.2μm纵向为2nm。 相似文献
3.
以异溴丁酸羟乙酯为引发剂、溴化亚铜和2,2′-联吡啶为催化剂和配体,引发丙烯酸琥珀酰胺酯(NAS)进行原子转移自由基聚合,得到的聚丙烯酸琥珀酰胺酯(PNAS)的分子量可以通过配比和转化率预测.进一步与单端氨基苯胺四聚体(TA)在50℃下反应,得到的聚合物用1H-NMR和FT-IR的测试,结果表明,当TA/NAS的摩尔比为3∶1时,PNAS上的琥珀酰胺酯可以完全被取代,从而得到侧链为苯胺四聚体的导电高分子.聚合物的结构和分子量以及分布用核磁共振氢谱、FT-IR和GPC进行表征;电化学性质用循环伏安法进行了测试. 相似文献
4.
A general method has been proposed for synthesizing 3-(3-acetyl-5-aroyl-1,3,4-oxadiazolyl-2)-chromones that has been based on conversion of 3-formylchromones to acylhydrazones and of theacylhydrazones into the heterocyclic chromones. 相似文献
5.
CTD data from two oceanographic survey cruises, conducted by “Shiyan No. 3” R/V during two reversing monsoons, were employed
to calculate and analyze the distributions of temperature, salinity and geopotential anomaly in the southern South China Sea
(SSCS). Based on these distributions, the horizontal structures of the SSCS circulation are described systematically. Study
results show that the SSCS circulation structure could be classified as a two-layer (the upper and the lower) pattern, and
that the main circulation in the upper layer (0–400 m) is driven by the South China Sea monsoons and is opposite in direction
to the reversal of the monsoons. The distributions of principal current systems and their features are presented. Two important
local phenomena, local eddy and oceanic front, were observed. 相似文献
6.
Yulong Bai Wang Wan Yanan Huang Wenhan Jin Haochen Lyu Qiuxuan Xia Xuepeng Dong Zhenming Gao Yu Liu 《Chemical science》2021,12(24):8468
Co-aggregation of multiple pathogenic proteins is common in neurodegenerative diseases but deconvolution of such biochemical process is challenging. Herein, we developed a dual-color fluorogenic thermal shift assay to simultaneously report on the aggregation of two different proteins and quantitatively study their thermodynamic stability during co-aggregation. Expansion of spectral coverage was first achieved by developing multi-color fluorogenic protein aggregation sensors. Orthogonal detection was enabled by conjugating sensors of minimal fluorescence crosstalk to two different proteins via sortase-tag technology. Using this assay, we quantified shifts in melting temperatures in a heterozygous model protein system, revealing that the thermodynamic stability of wild-type proteins was significantly compromised by the mutant ones but not vice versa. We also examined how small molecule ligands selectively and differentially interfere with such interplay. Finally, we demonstrated these sensors are suited to visualize how different proteins exert influence on each other upon their co-aggregation in live cells.A little leak will sink a great ship! We prepared a series of multi-color protein aggregation sensors and developed a dual-color thermal shift assay to simultaneously and quantitatively report on protein co-aggregation of two different proteins. 相似文献
7.
Separations of small ions were carried out under nonequilibrated conditions using capillaries treated with NaOH, HCl, or tris(hydroxymethyl)aminomethane (Tris) prior to analysis. For separations of benzoic acid isomers or acids and amines under weakly acidic conditions, capillaries flushed with 0.1 M NaOH and subsequently with running buffers prior to analysis were used. Separations of six benzoic acid isomers were accomplished in 4 min in 1 mM phosphate buffers, pH 4.01, containing 2.5 mM hydroxypropyl-beta-cyclodextrin. Without additives, the separation of biological amines and acids were also achieved in 10 min at pH 4.01. Capillaries treated with 0.1 M HCl prior to analysis were tested in separations of six phenols in 5 mM Tris solutions at pH 7.0. As a result of small electrophoretic mobilities of phenols against a small electroosmotic flow, resolution was optimized. We also found that reproducibility was improved using capillaries treated with HCl. The relative standard deviations of migration mobility of phenols were less than 1%, which were smaller than those obtained using capillaries treated with 0.1 M NaOH or Tris. 相似文献
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10.
提出将MEMS矢量水听器应用于潜标系统,并进行了大量实验验证其可行性。MEMS矢量水听器是一种新型水下声学传感器,它具有体积小、成本低、一致性高和高灵敏度等优点。将水听器应用于潜标系统,可以大幅降低阵列孔径,进而有效地监测海洋声场的矢量信息。矢量水听器矢量通道的指向性与频率无关,在低频和甚低频同样可以获得良好的空间增益,应用在低频和甚低频领域中,可以有效地解决声纳设备体积庞大的问题。经过对系统样机进行多次室内驻波桶调试和外场湖试与海试,结果表明,该系统能有效检测海底20~1000 Hz范围内的声场矢量信号,水听器此时的灵敏度可达-176 dB,且具有良好的8字型指向性。实验结果证明了MEMS矢量水听器应用在潜标系统中进行海洋声场矢量信息探测的可行性,为MEMS 矢量水听器在水下目标探测领域的研究提供了良好的试验平台,并为其工程化应用奠定了基础。 相似文献