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用RF溅射制备厚度为200 nm的Fe-N薄膜在250℃, 12000 A/m磁场下真空热处理后,当N含量在5%~7%(原子百分数)范围内形成α′+α″相时,4πMS可达2.4 T, Hc<80 A/m, 2~10 MHz下高频相对导磁率μr=1500,可满足针对10 Gb/in2存储密度的GMR/感应式复合读写磁头中写入磁头的需要. Fe-N系薄膜中α′相的形成机理和点阵常数与块状试样按Bain机理形成的α′相有明显的差别,得到了薄膜中α′相的a,c与Cα′N之间的线性关系式. 相似文献
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本文用电化学方法研究了稀土元素Nd和La对工业纯铁中氢的渗透过程和扩散系数的影响。实验结果表明,随着铁中Nd或La含量的增加,氢的渗透过程减慢、扩散系数下降。固溶Nd和La原子是铁中氢的可逆浅陷井。固溶Nd原子与氢的结合能为4.4kcal/mol。当钕含量在0.082wt.%以下时,氢在铁中的扩散过程激活能为6.1kcal/mol。实验还测定了含Nd铁中氢的渗透过程激活能为8.7kcal/mol。 相似文献
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用抛光的WOL型恒位移试样跟踪观察了各种低合金钢在H_2S中应力腐蚀裂纹产生和扩展的规律。结果表明:当钢的强度和K_I均大于临界值之后,在裂纹前端将会发生滞后塑性变形,即裂纹前端塑性区的大小及其变形量将随时间延长而逐渐增加,当这种滞后塑性变形发展到临界状态时就会导致应力腐蚀裂纹的产生和扩展。 对超高强钢来说,当这个滞后塑性区闭合后应力腐蚀裂纹就在其端点形核,随着滞后塑性变形的发展,这些不连续的应力腐蚀裂纹逐渐长大并互相连接。对强度较低的钢,随滞后塑性变形的发展,应力腐蚀裂纹沿着滞后塑性区边界向前扩展。 已经证明这个滞后塑性变形是由氢引起的,称作氢致滞后塑性变形。 利用WOL型试样测量了在H_2S气体以及H_2S饱和水溶液中的K_(ISCC)和da/dt研究了它们随强度变化的规律,以及阴极极化和阳极极化对超高强钢K_(ISCC)和da/dt的影响。 相似文献
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The structure and magnetic properties of Fe- N thin films 总被引:1,自引:0,他引:1
200 nm Fe-N thin films deposited on glass substrates by RF sputtering were vacuum annealed at 250-350℃ under 12000 A/m magnetic field. Heat treatment was effective in improving the soft magnetic properties of the Fe-N film. When the nitrogen content was in the range of 5-7 at. %,the thin films consisted of α′ + α" after heat treatment and had excellent soft magnetic properties of 4πMs = 2.4 T, Hc < 80 A/m, μr = 1500 under 2-10 MHz. The properties of the films meet the needs of a write head material used in the dual element GMR/inductive heads. The fromation mechanism and lattice constants of the α′ phase in Fe-N thin film are different from Jack's results obtained from γ→α′transformation in bulk samples. The linear relationship between a, c and Ca'N for thin film was obtained asc = 2. 866+ 1.559Ca'N,a = 2.866 + 0.181Ca'N.`` 相似文献
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CRYSTALLINE CARBON NITRIDE THIN FILMS DEPOSITED BY MICROWAVE PLASMA CHEMICAL VAPOR DEPOSITION
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The crystalline carbon nitride thin films have been prepared on Si (100) substrates using microwave plasma chemical vapor deposition technique. The experimental X-ray diffraction pattern of the films prepared contain all the strong peaks of α-C3N4 and β-C3N4, but most of the peaks are overlapped.The films are composed of α-C3N4 and β-C3N4. The N/C atomic ratio is close to the stoichiometric value 1.33. X-ray photoelectron spectroscopic analysis indicated that the binding energies of C 1s and N 1s are 286.43eV and 399.08 eV respectively. The shifts are attributed to the polarization of C-N bond. Both observed Raman and Fourier transform infrared spectra were compared with the theoretical calculations. The results support the existence of C-N covalent bond in α- and β-C3N4 mixture. 相似文献