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研究建立了ICP—AES同时测定TiNi形状记忆合金中Co、Cu、Cr、Fe、Nb5元素的方法。进行了必要的条件试验,选择了分析线及其他仪器工作参数;考察了方法检出限、H2SO4酸度及基体钛、镍对测定的影响、工作曲线线性。进行了准确度和精密度试验,各元素的加标回收率为Co98.4%。99.6%、Cu98.0%~103%、Cr98.9%~99.6%、Fe94.6%~95.8%、Nb99.8%。102%。5种元素的相对标准偏差范围为4.2%-10%。 相似文献
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ICP-AES法测定丹参中的镉和铅 总被引:3,自引:0,他引:3
建立了利用电感耦合等离子体原子发射光谱(ICP-AES)法测定丹参中重金属元素Cd和Pb的方法,比较了干灰化法和湿化法两种样品处理方法对分析结果的影响,并测定了山东一些地区丹参中的Cd和Pb含量。结果表明:采用电感耦合等离子体原子发射光谱法检测丹参中的Cd和Pb,最低检出限(DL)分别为1.92和1.07 ng·mL-1;相对标准偏差(RSD)分别为3.14%和1.83%;回收率分别为103.05%和96.24%。利用湿法消解样品,精密度好,回收率高,优于干灰化法。干灰化法适合测定丹参中Pb,但不适合测定Cd,其回收率仅为0.1%。用湿法消解样品,测定不同产地丹参的Cd和Pb含量,结果表明:所测地区丹参的Cd, Pb含量大大低于《中华人民共和国药典》(2005)规定的中药材重金属含量标准,符合GAP生产的要求。 相似文献
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合成了丙烯酸/丙烯酰胺/马来酸酐(AA/AM/MA)三元共聚物,并探讨了共聚物与聚环氧琥珀酸(PESA)物理复配后的阻垢效果.研究了共聚物分子量、阻垢剂用量以及钙离子浓度、溶液pH值等因素对阻垢性能的影响.实验结果表明,AA/AM/MA共聚物与PESA复配后具有良好的阻垢效率. 相似文献
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刘春晓 《青海师范大学学报(自然科学版)》1998,(2):57-59
晚发性VK缺乏是婴儿期常见的出血性疾病,以颅内出血多见,起病急,病情进展迅速,病死率高,后遗症严重。本文对48例晚发性VK缺乏致颅内出血患儿采用常规静脉注射VK进行了治疗观察,酌情输鲜血,使用甘露醇及抗生素。对其中10例病情危重儿进行了腰穿放液治疗。经随访对照观察,腰穿放液治愈率明显提高,表明晚发性VK缺乏除常规应用VK等综合治疗外,早期采用腰穿放液治疗是控制病情进展的有效措施,可防止和减少后遗症 相似文献
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本文根据直接转矩控制的原理构造了一种直接转矩控制系统,该系统在动态和稳态时采用不同的控制策略,使转矩、转速的快速性和控制精度得到满足。仿真结果证明了该方法的有效性。 相似文献
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Visible and near-infrared optical properties of Nd:CLNGG crystal waveguides formed by proton implantation 下载免费PDF全文
A Nd:CLNGG waveguide structure operated at wavelengths of both 632.8 nm and 1539 nm was demonstrated for the first time to our knowledge, which was produced by the 480-keV H~+ion implantation with a dose of 1.0×10~(17)protons/cm~2.Its propagating modes at 632.8 nm and 1539 nm were measured by the well-known prism coupling technique. The refractive index profile at either 632.8-nm wavelength or 1539-nm wavelength was optical barrier type in the proton-implanted Nd:CLNGG crystal optical waveguide, which was calculated by using the reflectivity calculation method. The near-field light intensity distributions were also simulated by the finite-difference beam propagation method in the visible and nearinfrared bands. 相似文献
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Planar waveguides in neodymium-doped calcium niobium gallium garnet crystals produced by proton implantation 下载免费PDF全文
In this work, the fabrication and optical properties of a planar waveguide in a neodymium-doped calcium niobium gallium garnet(Nd:CNGG) crystal are reported. The waveguide is produced by proton(H~+) implantation at 480 ke V and a fluence of 1.0×10~(17) ions/cm~2. The prism-coupling measurement is performed to obtain the dark mode of the waveguide at a wavelength of 632.8nm. The reflectivity calculation method(RCM) is used to reconstruct the refractive index profile. The finite-difference beam propagation method(FD-BPM) is employed to calculate the guided mode profile of the waveguide.The stopping and range of ions in matter 2010(SRIM 2010) code is used to simulate the damage profile induced by the ion implantation. The experimental and theoretical results indicate that the waveguide can confine the light propagation. 相似文献