化学水浴沉积CdS薄膜晶相结构及性质

采用CBD法在醋酸镉溶液体系中制备CdS半导体薄膜，研究了溶液组份的浓度对CdS结晶结构的影响．增加乙酸胺的浓度、提高溶液的pH值有利于生成立方晶CdS，反之则易于生成六方晶CdS．无论立方相还是六方相CdS薄膜，电阻率均在10~4～10~5Ω·cm范围，结晶均匀细致．用六方晶为主和立方晶为主的CdS制备的CIGS太阳电池最高效率分别达到12.10%和12.17%．     

A Novel Dimeric Eremophilane from Ligularia virgaurea spp. oligocephala

A novel dimeric eremophilane, ligulolide B, was isolated from the alcoholic extract of the whole plant of Ligularia virgaurea spp. oligocephala. The structure was elucidated by various spectroscopic methods including intensive 2D NMR techniques （^1H-^1H COSY, gHMQC, gHMBC and ^1H-^1H NOESY） and HR-ESI-MS.     

高铁摩擦片表面裂纹检测方法研究

摩擦片的裂纹数目和长度是衡量高铁制动性能的核心评定标准之一,有效的裂纹检测对高铁的安全运行具有重要意义.提出基于CSPDarkNet53主干网络架构的改进算法,实现摩擦片裂纹的在线自动检测.一方面融合双路特征提取网络以增强对于裂纹特征检测的敏感度,有效提高摩擦片裂纹检测的准确率;另一方面在YOLO检测模块预测框的去冗余...     

一类齐次对称多项式上的切比雪夫不等式

本文借助于控制不等式及数学归纳法，将著名的切比雪夫不等式推广到m次一般齐次对称多项式上(如文中定理及引理7)，并将此结果用于对称平均等．旨在展示证明解析不等式的一些有效的方法和技巧，同时为数学研究特别是高维几何研究提供一些新的有趣而有用的解析不等式．     

基于可调谐光纤环形镜滤波器的多波长布里渊掺铒光纤激光器

通过使用非线性放大的光纤环形 镜滤波器(AFLMF),构造了一种新颖的多波长布里渊掺铒光纤激光器(E DFL)线形结构。非线性AFLMF由掺铒光纤放大器(EDFA,由980n m泵浦抽运 一段EDF构成)、偏振控制器(PC)和耦合器构成,减少了腔内基于波长的损耗,并且能够灵 活地控制反射 光以及激光腔内输入和输出光的强度。在布里渊泵浦功率为25mW、 980nm泵浦功率为200mW时,获得了波 长间隔为0.08nm的14个波长的激光输出以及50nm的可调谐范围。通过调节980nm抽运光功率、PC以及布里渊泵浦光波长,实现了可调谐的多波长输出。研究 了980nm抽运光功率以及PC对斯托克斯光波数的影响。     

以香豆素为基用以识别氟离子的新型比色化学传感器

以香豆素作为发色团,胺基为氢键供体,以—C=N键桥连设计合成了可裸眼识别氟离子的化学传感器1,吸收光谱结果表明在乙腈中它可以高选择性识别氟离子,光谱红移70 nm,溶液颜色由橙色变为蓝紫色,而其它离子如Cl~-、Br~-、I~-、H_2PO_4~-、NO_3~-、HSO_4~-、AcO~-等均不影响其对氟离子的识别.通过核磁共振氢谱考察其识别机制,表明传感分子通过与F~-间的质子转移反应,使整个体系电子离域,分子内电荷转移更加显著,从而导致吸收光谱大幅红移.     

化学水浴沉积CdS薄膜晶相结构及性质

采用CBD法在醋酸镉溶液体系中制备CdS半导体薄膜,研究了溶液组份的浓度对CdS结晶结构的影响.增加乙酸胺的浓度、提高溶液的pH值有利于生成立方晶CdS,反之则易于生成六方晶CdS.无论立方相还是六方相CdS薄膜,电阻率均在104～105Ω·cm范围,结晶均匀细致.用六方晶为主和立方晶为主的CdS制备的CIGS太阳电池最高效率分别达到12.10%和12.17%.     

Noncommutative Differential Calculus Approach to Discrete Symplectic Schemes on Regular Lattice

By means of a noncommutative differential calculus on function space of discrete Abelian groups and that of the regular lattice with equal spacing as well as the discrete symplectic geometry and a kind of classical mechanical systems with separable Hamiltonian of the type H(p, q) = T(p) + V(q) on regular lattice, we introduce the discrete symplectic algorithm, i.e., the phase-space discrete counterpart of the symplectic algorithm including original symplectic schemes and the jet-symplectic schemes in terms of the discrete time jet bundle formalism, on the regular lattice. We show some numerical calculation examples and compare the results of different schemes.     

Relationship between pretrial publicity and trial outcomes

Research suggests that pretrial publicity influences trials. Past research has relied heavily on experimental methods. Several commentators have questioned the ecological validity of the studies, and hence the value of the findings. The present study, one of the first to examine actual trials, focused on all federal murder trials over a 3-year period. The results suggested that (a) greater probability of conviction was associated with low rather than high levels of publicity; (b) defendants fared better under moderate rather than no publicity levels; and for defendants who were convicted, any degree of pretrial publicity was associated with longer sentences. In general, the results obtained from studying actual trials differed in important ways from the results obtained in laboratory research.