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排序方式: 共有396条查询结果,搜索用时 468 毫秒
1.
Valiollah Mirkhani Majid Moghadam Shahram Tangestaninejad 《Tetrahedron letters》2006,47(13):2129-2132
Rapid and efficient preparation of 2-imidazolines and bis-imidazolines by reaction of ethylenediamine with nitriles in the presence of catalytic amounts of sulfur under ultrasonic irradiation is reported. The advantages of this system are short reaction times, high yields and the ability to carry out large scale reactions. 相似文献
2.
Real-time processing and compression of DNA microarray images. 总被引:1,自引:0,他引:1
Shadrokh Samavi Shahram Shirani Nader Karimi 《IEEE transactions on image processing》2006,15(3):754-766
In this paper, we present a pipeline architecture specifically designed to process and compress DNA microarray images. Many of the pixilated image generation methods produce one row of the image at a time. This property is fully exploited by the proposed pipeline that takes in one row of the produced image at each clock pulse and performs the necessary image processing steps on it. This will remove the present need for sluggish software routines that are considered a major bottleneck in the microarray technology. Moreover, two different structures are proposed for compressing DNA microarray images. The proposed architecture is proved to be highly modular, scalable, and suited for a standard cell VLSI implementation. 相似文献
3.
A new diamine monomer containing flexible sulfone, sulfide, and amide units was prepared via three steps. Nucleophilic chloro displacement reaction of 4‐aminothiophenol with 4‐nitrobenzoyl chloride in the presence of propylene oxide afforded N‐(4‐mercapto‐phenyl)‐4‐nitrobenzamide and subsequent reduction of the nitro intermediate led to 4‐amino‐N‐(4‐mercapto‐phenyl)benzamide. Two moles of this amino thiophenol compound was reacted with bis‐(4‐chloro phenyl)sulfone to provide a novel diamine monomer. The diamine was reacted with aromatic dianhydrides to form polyimides via a two‐step polycondensation method, formation of poly(amic acid)s, followed by chemical imidization. The resulting polymers were characterized and their physical properties including thermal behavior, thermal stability, solubility and inherent viscosity were studied. Copyright © 2007 John Wiley & Sons, Ltd. 相似文献
4.
A series of new poly(amide imide)s was prepared from new diacid containing sulfone, ether, amide and imide groups with various aromatic diamines. The diacid was synthesized via four steps, starting from reaction of 4-aminophenol with 4-nitrobenzoyl chloride in the presence of propylene oxide afforded N-(4-hydroxy phenyl)-4-nitrobenzamide. In the second step, reduction of nitro group resulted in preparation of 4-amino-N-(4-hydroxy phenyl) benzamide. In the next step for the preparation of diamine, the reaction of 4-amino-N-(4-hydroxy phenyl) benzamide with bis-(4-chlorophenyl) sulfone in the presence of K2CO3 was achieved. The prepared sulfone ether amide diamine was reacted with two moles of trimellitic anhydride to synthesize related sulfone ether amide imide diacid. The precursors and final monomer were characterized by FT-IR, H-NMR and elemental analysis. Direct polycondensation reaction of the sulfone ether amide imide diacid with different diamines in the presence of triphenyl phosphite afforded five different poly (sulfone ether amide imide amide)s. The obtained polymers were fully characterized and their physical properties including thermal behavior, thermal stability, solubility, and inherent viscosity were studied. 相似文献
5.
Valiollah Mirkhani Shahram TangestaninejadBahram Yadollahi Ladan Alipanah 《Tetrahedron》2003,59(41):8213-8218
Epoxides can be cleaved in a regio- and stereoselective manner under neutral conditions with alcohols and acetic acid in the presence of catalytic amounts of decatungstocerate(IV) ion, ([CeW10O36]8−), affording the corresponding β-alkoxy and β-acetoxy alcohols in high yields. In water, ring opening of epoxides occurs with this catalyst to produce the corresponding diols in good yields. 相似文献
6.
Shahram Mehdipour-Ataei 《European Polymer Journal》2005,41(1):65-71
Terephthalic acid bis(carboxydiphenyl methyl)ester (TBE) as a new monomer for the preparation of polyamides was synthesized through the nucleophilic substitution reaction of benzilic acid with terephthaloyl chloride. This diester-diacid (TBE) was characterized using conventional spectroscopic methods. Polycondensation reactions of TBE with different aromatic and semi-aromatic diamines via Yamazaki method resulted different poly(ester amide)s. All the polymers were characterized and their physical and thermal properties were studied. 相似文献
7.
Xiaoning Qi Gyure A. Yansheng Luo Lo S.C. Shahram M. Singhal K. 《Electron Device Letters, IEEE》2006,27(8):696-698
The on-chip inductive impact on signal integrity has been a problem for designs in deep-submicrometer technologies. The inductive impact increases the clock skew, max timing, and noise of bus signals. In this letter, circuit simulations using silicon-validated macromodels show that there is a significant inductive impact on the signal max timing (/spl sim/ 10% pushout versus RC delay) and noise (/spl sim/2/spl times/RC noise). In nanometer technologies, process variations have become a concern. Results show that device and interconnect process variations add /spl sim/ 3% to the RLC max-timing impact. However, their impact on the RLC signal noise is not appreciable. Finally, inductive impact in 65- and 45-nm technologies is investigated, which indicates that the inductance impact will not diminish as technology scales. 相似文献
8.
9.
In this paper, a new voltage-mode (VM) first-order phase shifter (all-pass filter) employing only four NMOS transistors and
minimum number of passive elements (i.e. one resistor and one capacitor) is proposed. The proposed VM phase shifter has high
input impedance and does not require passive element matching constraints. Moreover, since only two NMOS transistors are stacked
between positive and negative supply voltages, the proposed circuit is suitable for low-voltage operation. Electronic tunability
can be provided easily by replacing the employed resistor with an NMOS transistor operating in triode region. Simulation results
based on 0.18 μm TSMC CMOS parameters with ±0.9 V supply voltages are given to demonstrate the performance of the proposed
phase shifter. 相似文献
10.
Soltanolkottabi Fariba Talaie M R Aghamiri Seyedfoad Tangestaninejad Shahram 《Journal of the Iranian Chemical Society》2020,17(1):17-24
Journal of the Iranian Chemical Society - The primary objective of the present work was to investigate the effect of fluid movement on synthesized chromium-benzenedicarboxylate, MIL-101(Cr),... 相似文献