Nano-LC: An updated review

Low-flow chromatography has a rich history of innovation but has yet to reach widespread implementation in bioanalytical applications. Improvements in pump technology, microfluidic connections, and nano-electrospray sources for MS have laid the groundwork for broader application, and innovation in this space has accelerated in recent years. This article reviews the instrumentation used for nano-flow LC, the types of columns employed, and strategies for multidimensionality of separations, which are key to the future state of the technique to the high-throughput needs of modern bioanalysis. An update of the current applications where nano-LC is widely used, such as proteomics and metabolomics, is discussed. But the trend toward biopharmaceutical development of increasingly complex, targeted, and potent therapeutics for the safe treatment of disease drives the need for ultimate selectivity and sensitivity of our analytical platforms for targeted quantitation in a regulated space. The selectivity needs are best addressed by mass spectrometric detection, especially at high resolutions, and exquisite sensitivity is provided by nano-electrospray ionization as the technology continues to evolve into an accessible, robust, and easy-to-use platform.     

网格环境下基于本体的专家系统构建研究

对网格环境下基于本体的专家系统（Expert System）进行了研究，提出了构建在通用知识网格（Universal Knowledge Grid，UKG）和开放网格业务体系结构（Open Grid Services Architecture，OGSA）基础上的专家系统模型。为网格环境下创建大规模分布式基于本体知识库体系的专家系统提供了参考模型。     

USB数据传输中CRC校验码的并行算法实现

文章介绍了用于USB总线数据传输的CRC校验的原理和算法，并且采用并行电路实现USB2．0中的CRC产生和CRC校验，与传统的串行电路实现相比，并行电路实现方法虽然在芯片面积上大于串行电路实现，但由于降低了时钟频率，电路更容易综合实现，并且大大降低了功耗，有利于低功耗电路设计。     

FPGA在雷达信号跟踪器中的应用

雷达信号跟踪器是探测定位装置的重要组成部分。叙述了FPGA的结构特点和设计流程，讨论了利用FPGA设计雷达信号跟踪器的要点。模块化设计的系统，使其集成度和灵活性都有了很大的提高。     

On the Feasibility of Growing Pb[(Zn1/3Nb2/3)0.91Ti0.09]O3 Single Crystals

Pb[(Zn_1/3Nb_2/3)_0.91Ti_0.09]O₃ (PZNT91/9) single crystals were grown by two methods: from solution using PbO as a self‐fluxing agent (SC method) and directly from the melt without fluxing (MC method). In both growth methods, an allomeric Pb[(Mg_1/3‐Nb_2/3)_0.69Ti_0.31]O₃ (PMNT69/31) single crystal was used as a seed. X‐ray diffraction patterns of ground crystals showed that phase‐pure perovskite PZNT91/9 single crystals were successfully fabricated by the above two methods. The composition of the crystals obtained by both the SC and MC methods was analyzed using X‐ray fluorescence, which confirmed that the crystal composition is close to the nominal value, although volatilization of PbO and segregation during crystal growth are inevitable. The MC PZNT91/9 crystals exhibit excellent piezoelectric properties, with the piezoelectric constant, d₃₃, in the range of 1800–2200 pC N^–1. This value is comparable to that of the SC crystals. However, the MC crystals show an abnormal dielectric behavior. In contrast with the SC crystals, in the MC crystals a much broader dielectric peak appears in the dielectric response curves, accompanied by a much lower peak temperature of around 105 °C. Furthermore, frequency dispersion is apparent over a much wider temperature range (even more apparent than in pure relaxors), where a large, i.e., about 70 °C, full width at half maximum (FWHM) for the dielectric peaks is observed in the dielectric response. It is speculated that such an unusual phenomenon correlates with defects, microinhomogeneities, and polar regions in the as‐grown MC crystals. The origins of this abnormality have not been interpreted in detail until now. However, optical observation of the domain structure confirms that both the SC and MC crystals possess complex structural states.     

纵向泵浦Cr∶ Nd∶GSGG激光棒的热透镜效应研究

对纵向泵浦Cr∶Nd∶GSGG激光棒的热透镜效应进行了详细的理论分析。对温度分布的函数表达式 ,进行了讨论 ;分析了热引起的应力 ,得到了激光棒破裂的临界功率公式 ;最后对光学畸变进行了分析与讨论 ,推导了光程差计算公式     

一种基于混沌渐近同步的数字保密通信方法

根据驱动－响应混沌同步原理，提出了一种基于混沌渐近同步的数字保密通信方法。通过设计对发射信号进行多级单值非线性变换，使得通过预测法的攻击完全失效，因而这种通信方法具有较高的抗破译能力。理论分析和数值模拟结果证实了本方法的正确性与有效性。     

自动立体显示屏高亮度背光模块设计

使用自动立体显示器,用户不需要立体眼镜,裸眼就能看到立体图像.目前主流的液晶自动立体显示器的亮度不够,影响到使用.为了提高亮度,研究新的背光模块设计方法.采用高亮度发光二极管,用菲涅耳透镜和柱透镜使光线集中在用户眼睛上,大幅度提高图像亮度,由于左右眼看到的图像不一致,产生立体感.结合具体的显示器研制背光模块,选择二极管,设计光路和透镜,对光路仿真,探索出设计方法.该方法对自动立体显示器的设计有指导意义.