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通过Wittig-Horner反应合成了两个含有均二苯乙烯发色团, 一端为N,N-双(2-乙酰氧乙基)氨基受体, 另一端分别为N,N-二甲氨基(DMDE)或N,N-二苯氨基(DPDE)的荧光探针分子. 进行了NMR和MS表征. 测试了加入不同金属离子时探针分子的吸收和荧光光谱变化. 加入Ag+和Zn2+, DMDE在420 nm处出现强的荧光峰, 在600 nm的荧光峰先增强后减弱, 认为发生了分子间的荧光共振能量转移. 而DPDE在加入Ag+和Zn2+, 420 nm处无荧光发射, 600 nm处的荧光红移并减弱. 相似文献
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A third harmonic superconducting niobium cavity has been proposed for installation in the Shanghai Synchrotron Radiation Facility (SSRF) storage ring to improve the Touschek lifetime. In order to investigate the feasibility of the superconducting cavity fabrication indigenously and the possibility to master the fabrica tion techniques, cavities were fabricated from copper and niobium sheets by deep drawing and electron-beam welding, and a series of measurements, such as resonant frequency, shape dimensions and wall thickness, were carried out during this process. After analysis of various problems existing in the fabrication process, technique improvements were proposed, and finally the precise shape as designed and resonant frequency within 1.2 MHz were achieved for the new completed cavities. In addition, full annealing was finally proved to be a good cure for niobium sheets' tearing up during deep drawing. By fabricating niobium cavities successfully, some problems to the next step were cleared. This paper introduces the process of cavity fabrication and its technique improvements towards forming, and the initial vertical test result of niobium cavity is also presented. 相似文献
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含二氯丙烯的亚硫酸酯类化合物的合成及杀虫活性测定 总被引:1,自引:0,他引:1
为了寻找和发现高效、广谱、低毒、低生态风险并与现有杀虫剂无交互抗性的新型杀虫剂,以对苯二酚为原料,经多步反应制得11个新型含二氯丙烯的亚硫酸酯类化合物,其结构经核磁共振氢谱、碳谱、元素分析确证.室内生物活性测定结果表明,目标化合物对小菜蛾(Plutella xylostella L.)具有较好的杀虫活性,其中3-[2,6-二氯-4-(3,3-二氯烯丙氧基)苯氧基]丙基正己基亚硫酸酯(7h)在10 mg/L下对小菜蛾的致死率可达到80%,优于对照药三氟甲吡醚. 相似文献
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于海波 《数学物理学报(B辑英文版)》2022,(1)
This paper concerns the global existence of strong solutions to the 3 D compressible isothermal Navier-Stokes equations with a vacuum at infinity.Based on the special structure of the Zlotnik inequality,the time uniform upper bounds for density are established through some time-dependant a priori estimates under the assumption that the total mass is suitably small. 相似文献
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