全文获取类型
收费全文 | 651篇 |
免费 | 57篇 |
国内免费 | 78篇 |
专业分类
化学 | 425篇 |
晶体学 | 6篇 |
力学 | 45篇 |
综合类 | 7篇 |
数学 | 88篇 |
物理学 | 215篇 |
出版年
2024年 | 4篇 |
2023年 | 16篇 |
2022年 | 13篇 |
2021年 | 20篇 |
2020年 | 34篇 |
2019年 | 30篇 |
2018年 | 29篇 |
2017年 | 23篇 |
2016年 | 36篇 |
2015年 | 36篇 |
2014年 | 49篇 |
2013年 | 34篇 |
2012年 | 64篇 |
2011年 | 54篇 |
2010年 | 32篇 |
2009年 | 38篇 |
2008年 | 40篇 |
2007年 | 49篇 |
2006年 | 31篇 |
2005年 | 26篇 |
2004年 | 19篇 |
2003年 | 12篇 |
2002年 | 6篇 |
2001年 | 12篇 |
2000年 | 11篇 |
1999年 | 12篇 |
1998年 | 8篇 |
1997年 | 9篇 |
1996年 | 5篇 |
1995年 | 6篇 |
1994年 | 3篇 |
1993年 | 5篇 |
1992年 | 8篇 |
1991年 | 2篇 |
1990年 | 2篇 |
1989年 | 2篇 |
1988年 | 3篇 |
1986年 | 2篇 |
1985年 | 1篇 |
排序方式: 共有786条查询结果,搜索用时 15 毫秒
1.
Yimei Wang Yi Qiao Xiaomin Xu Xiaohong Ding Weiwei Li Bo Yuan Haiyan Xu 《Biomedical chromatography : BMC》2019,33(8)
A sensitive and reliable LC–MS/MS method was developed and validated for simultaneous quantification of the major components of Huangqi–Honghua extact in rat plasma, including hydroxysafflor yellow A (HSYA), astragaloside IV (ASIV), calycosin‐7‐O‐β‐d ‐glucoside (CAG), calycosin, calycosin‐3′‐O‐glucuronide (C‐3′‐G) and calycosin‐3′‐O‐sulfate (C‐3′‐S). After extraction by protein precipitation with acetonitrile and methanol from plasma, the analytes were separated on a Hypersil BDS C18 column by gradient elution with acetonitrile and 5 mM ammonium acetate. The detection was carried out on a triple quadrupole tandem mass spectrometer equipped with electrospray ionization source switched between negative and positive modes. HSYA was monitored in negative ionization mode from 0 to 4.9 min, and ASIV, CAG, calycosin, C‐3′‐G and C‐3′‐S were determined in positive ionization mode from 4.9 to 10 min. The lower limits of quantification of the analytes were 6.25 ng/mL for HSYA, 0.781 ng/mL for CAG and 1.56 ng/mL for ASIV and calycosin. The intra‐ and inter‐assay precision (RSD) values were within 13.43%, and accuracy (RE) ranged from ?8.75 to 9.92%. The validated method was then applied to the pharmacokinetic study of HSYA, ASIV, CAG, calycosin, C‐3′‐G and C‐3′‐S in rat after an oral administration of Huangqi–Honghua extract. 相似文献
2.
YAN Xiaomin ZHAO Lin SHAO Jianhui TAN Xin SONG Zhengxiao School of Chemical Engineering Technology Tianjin University Tianjin China Slichem Liquid Material Co. Ltd. Shijiazhuang China 《Chinese Journal of Reactive Polymers》2004,(Z1)
1. INTRODUCTION Methionine, namely 2-amido-4-thiomethyl butyric acid with a structure of CH3SCH2CH2CHCOOH, is one of the essential amino acids and has two natural enantionmers, D and L-methionine. The mixture of L- and D-isomers can be used as analeptics or nutritive additives to maintain the equilibrium of amino acids of feed [1,2]. L-methionine can release active methyl and accelerate the synthesis of choline, which further speeds up the conversion of the lipid accumulated in liv… 相似文献
3.
4.
多目标半定规划的互补弱鞍点和G-鞍点最优性条件 总被引:1,自引:0,他引:1
对于含矩阵函数半定约束和多个目标函数的多目标半定规划问题,给出Lagrange函数在弱有效意义下的互补弱鞍点和Geofrrion恰当有效意义下的G-鞍点的定义及其等价定义.然后,在较弱的凸性条件下,利用含矩阵和向量约束的择一性定理,建立多目标半定规划的互补弱鞍点和G-鞍点充分必要条件. 相似文献
5.
进一步研究了具有三个cM公共值的亚纯函数的唯一性,改进了H.Ueda和仪洪勋等人的有关结果. 相似文献
6.
Traveling wave Ti:LiNbO3 Mach-Zehnder optical modulators with buried electrodes and etched grooves in the SiO2 buffer layer are analyzed by the finite element method. The tradeoff between the bandwidth BW and the half-wave voltage Vπ is discussed. The value of BW/Vπ is used to weight the total performance of the modulator. Taking a thick buffer layer and etching deep grooves in the buffer layer are demonstrated as two effective methods to improve the performance of the modulator. A 3-dB optical bandwidth of 18 GHz with half-wave voltage 5V at a wavelength of 1.55 pm could be obtained even though the electrode is not very thick. When the requirement of half-wave voltage is not very critical, a bandwidth of more than 100 GHz can be obtained. 相似文献
7.
All-optical wavelength conversion of 10-Gb/s signal based on four-wave mixing is experimentally demonstrated in a 30-m-long dispersion-flattened microstructure fiber with small positive dispersion. For an average pump power of 26 dBm, the conversion efficiency was around -19.5 dB with the fluctuation less than ±1.4 dB, covering a conversion bandwidth of 20 nm. The eye diagram of the converted signal shows good eye opening. 相似文献
8.
In this article,the Hausdorff dimension and exact Hausdorff measure function of any random sub-self-similar set are obtained under some reasonable conditions.Several examples are given at the end. 相似文献
9.
对于线性型多目标半定规划问题,引进加权中心路径的概念,并利用单目标半定规划的中心路径法,提出了求解多目标半定规划问题的加权中心路径法,先得型对一个叔向量的有效解,然后在此基础上,提出了通过一次迭代得到对应一定范围内其他任意权向量的有效解的一步修正方法. 相似文献
10.