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Characterization of autocatalytic decomposition reactions is important
for the safe handling and storage of energetic materials. Isothermal differential
scanning calorimetry (DSC) has been widely used to detect autocatalytic decomposition
of energetic materials. However, isothermal DSC tests are time consuming and
the choice of experimental temperature is crucial. This paper shows that an
automatic pressure tracking calorimeter (APTAC) can be a reliable and efficient
screening tool for the identification of autocatalytic decomposition behavior
of energetic materials.
Hydroxylamine nitrate (HAN) is an important
member of the hydroxylamine family. High concentrations of HAN are used as
liquid propellants, and low concentrations of HAN are used primarily in the
nuclear industry for decontamination of equipment. Because of its instability
and autocatalytic decomposition behavior, HAN has been involved in several
incidents. 相似文献
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P. J. M. Peters M. Trentelman Q. C. Mei W. J. Witteman 《Applied physics. B, Lasers and optics》1994,59(5):533-535
The discharge characteristics of the XeF* (BX) laser are investigated. The NF3 and Xe partial pressure of the laser gas mixture and the total gas pressure have been varied. A highest specific output energy of 4.7 J/l with an efficiency of 0.5% was obtained from a X-ray preionized Ne/Xe/NF3 gas mixture at 6 bar with single-pulse excitation through a multichannel spark gap. 相似文献
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S. N. Tskhai Yu. B. Udalov P. J. M. Peters W. J. Witteman V. N. Ochkin 《Applied physics. B, Lasers and optics》1996,62(1):11-14
A radiofrequency excited atomic Xe slab laser with an active volume of 2 × 10 × 300 mm3 using a quartz envelope containing the laser-gas mixture shows a stable cw performance with an output power of almost 1 W. The free-running system oscillates, depending on gas composition and density, on several lines between 1.73 and 3.51 m. Line competition phenomena are observed. Single-line oscillation yields more than 500 mW. 相似文献
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In order to study the kinetic mechanism of the e-beam pumped Ar/Xe laser, the temporal profiles of individual laser lines during multiline oscillation have been measured as a function of power deposition (1–12MW/cm3) and gas laser pressure (2–14 bar) using a short pulse (30 ns) coaxial electron beam as excitation source. It was found that the optimum output energy at each pressure was obtained at the same specific power deposition.Strong line competition has been observed between the 2.65 and 1.73 m transitions. In order to explain our results we suggest that besides electron collision mixing (ECM) between the 5d and 6p levels of Xe, there is also a redistribution between all 6p levels which strongly favours the lower levels at higher pumping densities. 相似文献
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Several magnetic and optical processes contribute to the magneto-optical response of nickel thin films after excitation by a femtosecond laser pulse. We achieved a first complete identification by explicitly measuring the time-resolved Kerr ellipticity and rotation, as well as its temperature and magnetic field dependence in epitaxially grown (111) and (001) oriented Cu/Ni/Cu wedges. The first hundreds of femtoseconds the response is dominated by state filling effects. The true demagnetization takes approximately 0.5-1 ps. At the longer (sub-ns) time scales the spins are found to precess in their anisotropy field. Simple and transparent models are introduced to substantiate our interpretation. 相似文献
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P. J. M. Peters H. M. J. Bastiaens W. J. Witteman T. Gerber 《Applied physics. B, Lasers and optics》1987,43(4):253-261
Measurements of the output energy, the optical pulse length and the build-up time of the laser pulse, obtained with a coaxially e-beam pumped KrF* laser, were performed varying the total gas fill pressure, the F2 content and the e-beam current from 1–5 bar, 0.1–0.8% and 13.3–26.6 kA, respectively. The maximum specific extraction energy amounts to 64 J/l. The large range of measurements, especially at low F2 concentrations, reveals the necessity to extend the kinetics of the F2 chain in the usual computer model. With the introduction of electron quenching of KrF* and ArF* by dissociative attachment the predictions are also for low F2 concentration in agreement with experiments. 相似文献