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同步荧光法测定食品中维生素B1 总被引:7,自引:0,他引:7
本文研究了食品中维生素B1的同步荧光法测定条件,采用氯化钾-乙醇作柱层析洗脱液,碱性介质中氧化后立即调为中性,并加入表面活性剂OP对体系增稳增敏,取代丁醇萃取,经济方便,用于几种粮食样品的测定,结果满意。 相似文献
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The classical perturbation theory is extended to the weighted Kronecker product linear systems W(A? B)Wx =h. Upper bounds are derived for the normwise condition number. 相似文献
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Yiming Huai Mahendra PakalaZhitao Diao Dmytro ApalkovYunfei Ding Alex Panchula 《Journal of magnetism and magnetic materials》2006
Spin-transfer driven switching was observed in MgO based magnetic tunnelling junctions (MTJ) with tunnelling magnetoresistance ratio of up to 160% and the average intrinsic switching current density (Jc0) down to 2 MA/cm2, which are the best known results reported in spin-transfer switched MTJ nanostructures. Based on a comparison of results both from MgO and AlOx MTJs, further switching current decrease via MgO dual structures with two pinned layers is discussed. 相似文献
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Polymerizable lipopeptides with two hydrophobic chains were synthesized and transformed into comb-like polymers by radical polymerization. The structure of dry polymerizable lipopeptides and comb-like polymers and of their aqueous solutions was determined by X-ray diffraction. Comb-like polymers exhibit both thermotropic and lyotropic properties. Three types of mesomorphic structure were resolved: smectic B, smectic A and cylindrical hexagonal. The domains of stability of the mesophases and the values of their structural parameters were established. 相似文献
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采用激发样品表层和样品中心两种激发方式,在300K和77K温度下研究叶绿素A(Chla)的较高激发行为,观测到峰值位于493、520和580nm三条新的荧光发射带.分别测量它们的荧光激发光谱,证明这三条新的荧光带属于Chla的第二激发单线态向基态的不同振动能级的辐射跃迁发光.最后提出电子跃迁模型,同时进行了讨论. 相似文献
8.
Wang Yongqian Liao Xianbo Diao Hongwei Cheng Wenchao Li Guohua Chen Changyong Zhang Shibin Xu Yanyue Chen Weide Kong Guanglin 《中国科学A辑(英文版)》2002,45(10):1320-1328
A set of a-SiOx:H (0.52 <x< 1.58) films are fabricated by plasma-enhanced-chemical-vapor-deposition (PECVD) method at the substrate temperature
of 250°C. The microstructure and local bonding configurations of the films are investigated in detail using micro-Raman scattering,
X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FTIR). It is found that the films are
structural inhomogeneous, with five phases of Si, Si2O:H, SiO:H, Si2O3:H and SiO2 that coexist. The phase of Si is composed of nonhydrogenated amorphous silicon (a-Si) clusters that are spatially isolated.
The average size of the clusters decreases with the increasing oxygen concentration x in the films. The results indicate that
the structure of the present films can be described by a multi-shell model, which suggests that a-Si cluster is surrounded
in turn by the subshells of Si2O:H, SiO:H, Si2O3:H, and SiO2. 相似文献
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In this paper, a projection method is presented for solving the flow problems in domains with moving boundaries. In order to track the movement of the domain boundaries, arbitrary‐Lagrangian–Eulerian (ALE) co‐ordinates are used. The unsteady incompressible Navier–Stokes equations on the ALE co‐ordinates are solved by using a projection method developed in this paper. This projection method is based on the Bell's Godunov‐projection method. However, substantial changes are made so that this algorithm is capable of solving the ALE form of incompressible Navier–Stokes equations. Multi‐block structured grids are used to discretize the flow domains. The grid velocity is not explicitly computed; instead the volume change is used to account for the effect of grid movement. A new method is also proposed to compute the freestream capturing metrics so that the geometric conservation law (GCL) can be satisfied exactly in this algorithm. This projection method is also parallelized so that the state of the art high performance computers can be used to match the computation cost associated with the moving grid calculations. Several test cases are solved to verify the performance of this moving‐grid projection method. Copyright © 2004 John Wiley Sons, Ltd. 相似文献
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用等离子体增强化学气相沉积(PECVD)的方法,以固定的氢气(H2)流量和不同的硅烷(SiH4)和甲烷(CH4)流量比沉积了一系列的氢化非晶SiC(a-Si,C1-x-H)膜。用这种宽带隙的a-SixC1-x-H材料作为掺铒的基体材料,通过离子注入的方法得到掺铒的a-SixC1-x-H(a-SixC1-x-H:Er)膜。注入以后的样品经过不同温度的退火。用X射线光电子能谱(XPS)、红外吸收光谱(IR)、拉曼散射谱(Raman)等技术研究不同的SiH4/CH4流量比和退火温度对a-SixC1-x-H:Er发光强度的影响。结果表明,高温退火引起了膜中C的分凝,对饵的发光是不利的。通过低温和室温下铒发光强度的比较,表明这种材料具有较弱的温度猝灭效应。 相似文献